• Title/Summary/Keyword: coating properties

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Hard Coatings on Polycarbonate Plate by Sol-Gel Reaction of (3-glycidoxypropyl)trimethoxysilane (폴리카보네이트 판 위에 (3-glycidoxypropyl)trimethoxysilane의 졸-겔 반응을 이용한 하드 코팅)

  • Kim, Ju Youn;Shin, Young Jae;Shin, Youn Rok;Ji, Young Jon;Yoon, Yeo Seong;Shin, Jae Sup
    • Applied Chemistry for Engineering
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    • v.17 no.2
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    • pp.170-176
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    • 2006
  • The hard coatings on the polycarbonate plate were performed with the object of substitution the glass in the car to the polycarbonate plate. In this research, (3-glycidoxypropyl)trimethoxysilane (GPTMS), (3-aminopropyl)triethoxysilane (APS), and diethylenetriamine (DETA) were used to prepare the coatings by a sol-gel process. The optimum conditions and formulation to achiere the excellent physical properties of the coating were determined. In the case of using GPTMS and DETA, the smooth coating which had the 2 H class in pencil hardness was formed. In the case of using GPTMS and APS, the coating which had the 2 H class in pencil hardness was also formed. And the coatings with GPTMS and DETA showed an excellent abrasion resistant.

Development of Technology to Improve Maintenance Efficiency of Steel Corrosion using Zinc Powder (아연분말을 이용한 강재부식 유지보수 효율성 향상 기술 개발)

  • Kim, Dong-Ik
    • Journal of the Society of Disaster Information
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    • v.16 no.2
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    • pp.411-419
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    • 2020
  • Purpose: This study is intended to improve the performance of traffic signs corroded by aging, to ensure maintenance efficiency, a water-hardened coating solution was developed. Performance tests were then used to determine the optimal component scale. Method: For research purposes, the results were analyzed by conducting corrosion resistance assessment, physical properties evaluation, storage safety assessment, etc. on coating solutions of various magnifications. Results: The analysis results showed that there was little hearing in the cutting area in the liquid with added magnesium, so the method effect was excellent. And there was little blister occurrence, which was analyzed at the highest magnification. Conclusion: Enhancements to future new component scale experiments are needed for water-hardened coating solutions that have been recognized for their performance through this study. And institutional improvement efforts are needed to expand the enforcement of traffic sign maintenance using coating solutions.

Influence of Subsurface Layer on the Indentation Damage Behavior of YSZ Thermal Barrier Coating Layers Deposited by Electron Beam Physical Vapor Deposition (전자 빔 물리적 증착(EB-PVD)법으로 코팅된 YSZ 열차폐층의 압흔손상 거동에 대한 하부층의 영향)

  • Heo, Yong-Suk;Park, Sang-Hyun;Han, In-Sub;Woo, Sang-Kuk;Jung, Yeon-Gil;Paik, Un-Gyu;Lee, Kee-Sung
    • Journal of the Korean Ceramic Society
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    • v.45 no.9
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    • pp.549-555
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    • 2008
  • The thermal barrier coating must withstand erosion when subjected to flowing gas and should also maintain good stability and mechanical properties while it must also protect the turbine component from high temperature, hot corrosion, creep, and oxidation during operation. In this study we investigated the influence of subsurface layer, $Al_2O_3$ or NiCrCoAIY bond coat layer, on the indentation damage behavior of YSZ thermal barrier coating layers deposited by electron beam physical vapor deposition (EB-PVD). The bond coat is deposited using different process such as air plasma spray (APS) or spray of high velocity oxygen fuel (HVOF) and the thickness is varied. Hertzian indentation technique is used to induce micro damages on the coated layer. The stress-strain behaviors are characterized by results of the indentation tests.

Luminescent Properties of $SrTiO_3:Pr^{3+}$ Phosphor Coated with $SiO_2$ and $Al_2O_3$ by Sol-Gel Method (졸-겔법에 의한 $SrTiO_3:Pr^{3+}$ 형광체의 $SiO_2$$Al_2O_3$ 코팅에 따른 발광특성)

  • Lee, Dong-Kyu;Lim, Mun-Hyuk;Lee, Jin-Hwa;Kim, Tae-Young
    • Journal of the Korean Applied Science and Technology
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    • v.23 no.3
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    • pp.243-251
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    • 2006
  • Field emission display(FED) is actively investigated in view of the development of full color flat-panel display, which can replace some cathode-ray tube(CRT). Thus, the development of new phosphors appropriate for FED is urgently needed and has been actively investigated. In this work, $SrTiO_3:Pr^{3+}$ phosphor was prepared by sol-gel method and the coating was applied by sol-gel method combined with sonication on these phosphor's surface into diluted precursor solution. It was found that very fine particles of coating material were formed on phosphor's surface. The luminescent intensity of $SrTiO_3:Pr^{3+}$ phosphor coated with $SiO_2$ and $Al_2O_3$ was considerably increased without any noticeable change in color chromaticity. The optimum concentration of coating material was found to be 1wt% and the optimum pH value of the solution was 10.

Electrochemistry and Corrosion Characteristics of Polyaniline Dispersion Coating for Protection of Steels (강철보호를 위한 폴리아닐린 분산 코팅의 전기화학 및 부식특성)

  • Huh, Jae-Hoon;Oh, Eung-Ju;Cho, Jeong-Hwan
    • Journal of the Korean Electrochemical Society
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    • v.6 no.2
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    • pp.113-118
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    • 2003
  • Processible polyaniline (PAM) dispersions consisting of polyaniline micro-particles, cyclohexanone, and a polymeric surfactant were prepared in a micro-milling machine with various mixing conditions. The electrochemical properties of the dispersion film coated on Pt electrode were investigated by cyclic voltammetry (CV). The electrochemistry of the PAM dispersion coatings was basically similar to a pure PAM coating based on the results of CV. The results of polarization measurements and open circuit potential measurements carried out in $3\;wt.\%$ NaCI solution showed increase in corrosion potential when the PANI dispersion coatings applied on steel surface. Variation of open circuit potential $(OCP,\;V_{OC})$ of the dispersion coating/steel electrodes was observed, which differed with milling conditions. The results demonstrated practical use of the conducting polymer dispersion as a coating material for corrosion prevention of steel.

Characteristics of BGsome-Coated Illite as a Face Powder (BGsome이 코팅된 일라이트 및 이를 함유한 페이스 파우더의 특성)

  • Lim, Jin Kyong;Jin, Byung Suk
    • Applied Chemistry for Engineering
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    • v.24 no.2
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    • pp.126-131
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    • 2013
  • BGsome coating on the surface of illite powder was attempted to impart skin affinity and improve various characteristics of the powder for makeup cosmetics. BGsome is a type of hydrated liquid crystalline vesicles prepared by the hydration of 1,3-butylene glycol (BG) dissolved lecithin. BGsome droplets were coated through wet process and the coated powders were analyzed by TGA, SEM, and particle size measurements. Effect of BGsome coating on the physical properties, such as flow-ability, dispersibility, spreadability, and adhesion, were examined. The repose angle of BGsome-coated illite was decreased, which means that BGsome coating improves the flowability of the powder. Dispersibility, spreadability, and adhesion of the coated illite were also improved remarkably. The result of adhesion tests showed that the BGsome-coated illite was evenly adhered onto artificial leather surface with almost no lumps. The flowability, dispersibility, spreadability and adhesion of face powders containing the BGsome-coated illite were also improved.

Diamond Like Carbon Coating on WC Core Pin for Injection Molding of Zirconia Optical Ferrule (지르코니아 광페룰 사출성형용 WC 코아 핀의 Diamond Like Carbon 코팅)

  • Park, Hyun-Woo;Jeong, Se-Hoon;Kim, Hyun-Young;Lee, Kwang-Min
    • Korean Journal of Materials Research
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    • v.20 no.11
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    • pp.570-574
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    • 2010
  • A diamond-like carbon (DLC) film deposited on a WC disk was investigated to improve disk wear resistance for injection molding of zirconia optical ferrule. The deposition of DLC films was performed using the filtered vacuum arc ion plating (FV-AIP) system with a graphite target. The coating processing was controlled with different deposition times and the other conditions for coating, such as input power, working pressure, substrate temperature, gas flow, and bias voltage, were fixed. The coating layers of DLC were characterized using FE-SEM, AFM, and Raman spectrometry; the mechanical properties were investigated with a scratch tester and a nano-indenter. The friction coefficient of the DLC coated on the WC was obtained using a pin-on-disk, according to the ASTM G163-99. The thickness of DLC films coated for 20 min. and 60 min. was about 750 nm and 300 nm, respectively. The surface roughness of DLC films coated for 60 min. was 5.9 nm. The Raman spectrum revealed that the G peak of DLC film was composed of $sp^3$ amorphous carbon bonds. The critical load (Lc) of DLC film obtained with the scratch tester was 14.6 N. The hardness and elastic modulus of DLC measured with the nano-indenter were 36.9 GPa and 585.5 GPa, respectively. The friction coefficient of DLC coated on WC decreased from 0.2 to 0.01. The wear property of DLC coated on WC was enhanced by a factor of 20.

Optical Properties of Aspheric Glass Lens using DLC Coated Molding Core (성형용 코어면 DLC 코팅에 의한 비구면 Glass렌즈 광학적 특성에 관한 연구)

  • Kim, Hyun-Uk;Cha, Du-Hwan;Lee, Dong-Gil;Kim, Sang-Suk;Kim, Hye-Jeong;Kim, Jeong-Ho;Jeong, Sang-Hwa
    • Korean Journal of Optics and Photonics
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    • v.18 no.5
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    • pp.362-366
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    • 2007
  • In this research, the optimal grinding condition has been obtained by design of experiment (DOE) fur the development of aspheric lens for the 3 Mega Pixel, 2.5x optical zoom camera-phone module. Also, the tungsten carbide (WC) mold was processed by the method of ultra precision grinding under this optimal grinding condition. The influence of diamond-liked carbon (DLC) coating on form accuracy (PV) and surface roughness (Ra) of the mold was evaluated through measurements after DCL coating using ion plating on the ground mold. Also, aspheric glass lenses were molded, some before DLC coating of the mold and some after the DLC coating. The optical characteristics of each sample, molded by the different molds, were compared with each other.

Effect of Microstructure on the Environmentally Induced Cracking Behavior of Al-Zn-Mg-Cu-Zr Aluminum Alloy

  • Ghosh, Rahul;Venugopal, A.;Pradeep, PI;krishna, L. Rama;Narayanan, P. Ramesh;Pant, Bhanu;Cherian, Roy M
    • Corrosion Science and Technology
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    • v.17 no.3
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    • pp.101-108
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    • 2018
  • AA7010 is an Al-Zn-Mg-Cu alloy containing Zr, developed as an alternate to traditional AA7075 alloy owing to their high strength combined with better fracture toughness. It is necessary to improve the corrosion resistance and surface properties of the alloy by incorporating plasma electrolytic oxidation (PEO) method. AA7010-T7452 aluminum alloy has been processed through the forging route with multi-stage working operations, and was coated with $10{\mu}m$ thick $Al_2O_3$ ceramic aluminina coating using the plasma electrolytic oxidation (PEO) method. The corrosion, stress corrosion cracking (SCC) and nano-mechanical behaviours were examined by means of potentiodynamic polarization, slow strain rate test (SSRT) and nano-indentation tests. The results indicated that the additional thermomechanical treatment during the forging process caused a fully recrystallized microstructure, which lead to the poor environmental cracking resistance of the alloy in 3.5% NaCl solution, despite the overaging treatment. Although the fabricated PEO coating improved general corrosion resistance, the brittle nature of the coating did not provide any improvement in SCC resistance of the alloy. However, the hardness and elastic modulus of the coating were significantly higher than the base alloy.

Synthesis of Silica Aerogel and Thin Film Coating at Ambient (상입하에서의 실리카 에어로겔의 합성 및 박막코팅(I))

  • 양희선;최세영
    • Journal of the Korean Ceramic Society
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    • v.34 no.2
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    • pp.188-194
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    • 1997
  • Wet gel with surface modification by TMCS was redispersed in EtOH and redispersed silica sol for coat-ing was prepared. After spin coating of redispersed sol was conducted on silicon substrate, processes of drying(8$0^{\circ}C$) and heat treatment(>25$0^{\circ}C$) were, followed at ambient pressure. The influence of heat treat-ment of properties of film was observed, changing temperature at heat treatment. The optimum redisp-ersion condition for stable silica sol was wet gel:EtOH=1g:110$m\ell$ and the concentration and viscosity of redispersed silica sol with average particle size of 30nm were 0.11 M, 2.0-2.2 cP respectively. Crack-free thin film with the refractive index of 1.14 and thickness of 400 nm was obtained through drying at 8$0^{\circ}C$ and subsequent heat treatment at 45$0^{\circ}C$ for 2 hrs respectively after spin coating of 1500rpm, 10 times.

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