• 제목/요약/키워드: coating layer strength

검색결과 249건 처리시간 0.023초

Plasma spray 공정을 이용한 BCuP-5 filler 금속/Ag 기판 복합 소재의 제조, 미세조직 및 접합 특성 (Fabrication, Microstructure and Adhesive Properties of BCuP-5 Filler Metal/Ag Plate Composite by using Plasma Spray Process)

  • 윤성준;김영균;박재성;박주현;이기안
    • 한국분말재료학회지
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    • 제27권4호
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    • pp.333-338
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    • 2020
  • In this study, we fabricate a thin- and dense-BCuP-5 coating layer, one of the switching device multilayers, through a plasma spray process. In addition, the microstructure and macroscopic properties of the coating layer, such as hardness and bond strength, are investigated. Both the initial powder feedstock and plasma-sprayed BCuP-5 coating layer show the main Cu phase, Cu-Ag-Cu3P ternary phases, and Ag phase. This means that microstructural degradation does not occur during plasma spraying. The Vickers hardness of the coating layer was measured as 117.0 HV, indicating that the fine distribution of the three phases enables the excellent mechanical properties of the plasma-sprayed BCuP-5 coating layer. The pull-off strength of the plasma-sprayed BCuP-5 coating layer is measured as 16.5 kg/㎠. Based on the above findings, the applicability of plasma spray for the fabrication process of low-cost multi-layered electronic contact materials is discussed and suggested.

인쇄과정에서 코팅 용지의 국부적인 표면강도 변화에 관한 연구 (The Local Surface Strength Variation of Coated Papers during Printing)

  • 윤종태
    • 한국인쇄학회지
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    • 제22권2호
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    • pp.101-110
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    • 2004
  • The local surface strength variation of coated papers were measured at various speeds on a number of coated paper samples to study the effects of speed and ink tack on coating pick. Coating pick phenomenon is observed in an ink transfer variation curve as a decrease in the slope of the curve. On the other hand, it causes an actual decrease in net ink transfer to paper with an increase in speed. The effect of speed on coating pick depends on ink tack, ink film thickness and surface properties of coating layer formation of paper. A novel device to measure the surface strength can rate the coating paper in a different order. Comparison are made between dry test of coating paper pick and wet coating pick test of printing in IGT printability tester. Coating formulation is the main key to prevent from coating pick. The binder level increases, the coating pick and the slop decrease. The piling on blanket in printing is a problem when the coating pick is occur on a local area rather than average surface strength of coated papers.

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Failure and Phase Transformation Mechanism of Multi-Layered Nitride Coating for Liquid Metal Injection Casting Mold

  • Jeon, Changwoo;Lee, Juho;Park, Eun Soo
    • 한국재료학회지
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    • 제31권6호
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    • pp.331-338
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    • 2021
  • Ti-Al-Si target and Cr-Si target are sputtered alternately to develop a multi-layered nitride coating on a steel mold to improve die-casting lifetime. Prior to the multi-layer deposition, a CrN layer is developed as a buffer layer on the mold to suppress the diffusion of reactive elements and enhance the cohesive strength of the multi-layer deposition. Approximately 50 nm CrSiN and TiAlSiN layers are deposited layer by layer, and form about three ㎛-thickness of multi-layered coating. From the observation of the uncoated and coated steel molds after the acceleration experiment of liquid metal injection casting, the uncoated mold is severely eroded by the adhesion of molten metallic glass. On the other hand, the multi-layer coating on the mold prevents element diffusion from the metallic glass and mold erosion during the experiment. The multi-layer structure of the coating transforms the nano-composite structured coating during the acceleration test. Since the nano-composite structure disrupts element diffusion to molten metallic glass, despite microstructure changes, the coating is not eroded by the 1,050 ℃ molten metallic glass.

플라즈마 용사된 $ZrO_{2}$-단열 코팅층의 특성 및 열처리에 따른 접합강도변화 (Characteristic and Adhesive Strength Change by Heat Treatment of the Plasma Sprayed $ZrO_{2}$- Thermal Barrier Coatings(TBC))

  • 김병희;서동수
    • 한국재료학회지
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    • 제8권6호
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    • pp.505-512
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    • 1998
  • 플라즈마 용사법을이용하여 AISI 316 스테인레스 금속모재에 0.1mm 두께의 $NiCrAlCoY_{2}O_{3}$금속 결합층과 0.3mm 두께의 $ZrO_{2}(8wt%Y_{2}O_3$) 세라믹층으로 구성된 이층 단열코팅층을 제조하였다. 코팅층의 미세조직, 금속결합층의 산화를 고찰하였으며, $900^{\circ}C$에서 등은 시험과 열반복시험 후, 접합강도시험을 통하여 코팅층의 단사정 상은 열처리시간이 길어질수록 약간 증가하였다. 또한 비변태성 t'의 c/a는 용사상태에서 1.0099이였으며, 100시간 열처리 후에는 1.0115로 약간 증가하였다. 그리고 용사층의 접합강도는 열처리 시간이 길어질수록 감소하였다. 등온열처리 후에는 1.0115로 약간 증가하였다. 그리고 용사층 의 접합강도는 열처리 시간이 길어질수록 감소하였다. 등온열처리 후, 파괴는 주로 세라믹층에서 일어났으며, 반복 열처리되 시편에서는 10회 이후 대부분 금속결합층/세라믹층의 계면에서 일어났다.

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합금화용융아연코팅강판의 코팅층 접합강도 평가를 위한 단일 겹치기이음 시험의 적용 (Application of Single Lap-Shear Test for Extracting Adhesive Bonding Strength of Coating Layer on Galvannealed sheet)

  • 이정민;이찬주;이상곤;고대철;김병민
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2007년도 춘계학술대회A
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    • pp.238-243
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    • 2007
  • This paper is designed to estimate the adhesion strength of coating layer on galvannealed steel sheet using lap shear test. The single lap shear test is the most commonly used standard test for determining the strength of medium-strength and high strength bonds. The bond strength of bonded single lap joints on subjecting the substrates to loads is determined by lap shear forces in the direction of the bonded joint. In this study, specimen for adhesion strength test was made to attach coated sheet to cold rolled sheet and were heated in temperature of 180 for 20minutes. After test, detached parts of coatings on coated sheet were observed using SEM and EDX to identify substrate and complete detachment. The tested results showed that adhesive strength of coating is unrelated to anisotropy of sheet and is difficult to be extracted using conventional theory because of fine cracks of coating layers which were created during annealing process.

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친수성 고분자의 코팅을 통한 Poly(acrylonitrile) 나노복합중공사막의 제조 및 성능 연구 (Studies on Preparation and Performance of Poly(acrylonitrile) Nano-composite Hollow Fiber Membrane through the Coating of Hydrophilic Polymers)

  • 박철오;임지원
    • 멤브레인
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    • 제29권3호
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    • pp.140-146
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    • 2019
  • 본 연구에서는 다공성 Polyacrylonitrile (PAN) 중공사막을 지지체막으로 하여 Poly styrene sulfonic acid (PSSA)와 polyethyleneimine (PEI)을 이용하여 layer-by-layer법으로 선택층을 형성시켰다. 코팅용액에 Mg염을 첨가하여 염석법(salting out method)을 이용하였다. 코팅용액의 이온세기, 고분자 농도, 코팅시간 등을 달리하여 나노여과막을 제조하였으며 NaCl, $MgCl_2$, $CaSO_4$ 100 mg/L를 공급액으로 하여 2 atm의 구동 압력에서 투과도와 염 배제율을 평가하였다. PSSA 20,000 ppm, 코팅시간 3분, 이온세기 1.0, PEI 30,000 ppm, 코팅시간 1분, 이온세기 0.1의 조건으로 코팅한 막이 가장 우수한 성능을 보여 주었다. 100 ppm의 NaCl, $MgCl_2$, $CaSO_4$ 공급액에서 각각 20.4, 19.4, 18.7 LMH의 투과도와 67, 90, 66.6%의 염 배제율을 나타내었다.

분무건조법에 의한 용사용 WC-17%Co 복합분말제조 및 HVOF(High Velocity Oxy-Fuel) 용사특성 (Fabrication of WC-17%Co Composite Powder for Thermal Spray by Spray-Drying Method and HVOF Thermal Spray Characteristics)

  • 설동욱;김병희;임영우;정민석;서동수
    • Journal of Welding and Joining
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    • 제14권6호
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    • pp.101-108
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    • 1996
  • In this study, WC-l7wt% Co composite powder for thermal spray was fabricated by spray drying method. The agglomerated composite powder had spheroidal morphology and the particle size distribution was 20~60${\mu}{\textrm}{m}$. WC and Co were distributed homogeneously. However, the strength of the spray-dried agglomerate was low due to the pores within the agglomerate. Therefore, the spray-dried agglomerate was broken down during HVOF thermal spray and the microstructure was inhomogeneous with many pores within the coating layer. And the decomposition of WC to W and $W_{6}$ $C_{2.54}$ was accelerated. The strength and flowability of the agglomerate were greatly improved by sintering heat treatment(110$0^{\circ}C$, 1 hour, hi atmosphere), and then the coating layer showed dense and homogeneous microstructure with well-developed splats. The hardness of the coating layer was H $v_{300}$ = 1072.2.2.

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AIP 코팅법에서 코팅 시간이 고속도강의 TiN 코팅층 성질에 미치는 영향 (Effect of Coating Time on the Property of TiN-Coated Layer on High Speed Steel by Arc Ion Plating)

  • 김해지;전만수
    • 한국소성가공학회:학술대회논문집
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    • 한국소성가공학회 2006년도 춘계학술대회 논문집
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    • pp.308-313
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    • 2006
  • The effect of coating time on surface properties of the TiN-coated high speed steel(SKH51) by arc ion plating is and presented in this paper. Surface roughness, micro-hardness, coated thickness, atomic distribution of TiN and adhesion strength are measured for various coating times. It has been shown that the coating time has a deep influence more than 60 minites on the micro-hardness, coated thickness, atomic distribution of Ti and adhesion strength of the SKH51 steels, but that the coating time has little influence on the surface roughness.

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저탄소강의 알루미늄코팅조건에 따른 Nd:YAG 레이저 용접특성 (Welding Characteristics of Low Carbon Steel with Al Coating Condition by Nd:YAG Laser)

  • 김종도;이정한;김숙환;김기철
    • 대한기계학회:학술대회논문집
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    • 대한기계학회 2007년도 춘계학술대회A
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    • pp.1317-1321
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    • 2007
  • Aluminized steel sheet that Al coated on low carbon steel has a excellent heat resistance, thermal reflection and corrosion resistance. It has applied to fuel tank, automotive exhaust systems, etc. Laser weldability of the aluminized steel for the full penetration welding will be described in this paper. We focused on the effect of Al coating conditions on weld strength. For these objectives, aluminized steel sheets that has various thickness and coating weight were prepared for laser welding. And then, tensile-shear and hardness test were carried out. At that same time, Al content mixed in weld after laser welding was evaluated and investigated a correlation between the mixed Al and mechanical properties. Besides, as removing partially coating layer, weldability has been investigated according to position of coating layer. As a result of this study, as increasing Al content in weld, tensile-shear strength was decreased. Also it was identified that Al of coating layer caused grain growth.

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$Cr_2O_3$ 플라스마 용사 코팅된 유리의 입자충격에 의한 손상기구 (Damage Mechanism of Particle Impact in a $Cr_2O_3$ Plasma Coated Soda-lime Glass)

  • 서창민;이문환;김성호;장종윤
    • 한국해양공학회지
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    • 제12권3호통권29호
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    • pp.49-59
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    • 1998
  • The damage mechanism of $Cr_2O_3$ plasma coated soda-lime glass and uncoated glass by steel ball particle impact was analyzed in this study. And the shape variation of the cracks was investigated by stereo-microscope according to the impact velocity and steel ball diameter. In order to improve the damage reduction effect by $Cr_2O_3$ coating layer, crack size was measured and surface erosion state was observed for both of two kinds of specimen after impact experiment. And the results were compared with each other. The 4-point bending test was performed according to ASTM D790 testing method to evaluate the effect of coating layer for bending strength variation. As a result, it was found that the crack size of $Cr_2O_3$ coated specimen was smaller than that of uncoated one, because of the impact absorption by interior pores in the coating layer and the load dispersion by the structural characteristic of the coating layer. For the specimens subjected to the steel ball impact, the bending strength of coated specimen was higher than that of uncoated specimen.

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