• Corrosion Science and Technology
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• v.16 no.4
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• pp.209-225
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• 2017

Development of high strength steel requires proper understanding of hydrogen behavior since the higher the steel strength the greater the susceptibility of hydrogen assisted cracking. This paper provides a brief but broad overview on hydrogen entry and transport behavior of high-strength ferritic steels. First of all, hydrogen absorption, diffusion and trapping mechanism of the steels are briefly introduced. Secondly, several experimental methods for analyzing the physical/chemical nature of hydrogen uptake and transport in the steels are reviewed. Among the methods, electrochemical permeation technique utilized widely for evaluating the hydrogen diffusion and trapping behavior in metals and alloys is mainly discussed. Moreover, a modified permeation technique accommodating the externally applied load and its application to a variety of steels are intensively explored. Indeed, successful utilization of the modified permeation technique equipped with a constant load testing device leads to significant academic progress on the hydrogen assisted cracking (HAC) phenomenon of the steels. In order to show how the external and/or residual stress affects mechanical instability of steel due to hydrogen ingress, the relationship among the microstructure, hydrogen permeation, and HAC susceptibility is briefly introduced.

• KOREAN JOURNAL OF PACKAGING SCIENCE & TECHNOLOGY
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• v.15 no.1
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• pp.1-6
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• 2009

The impact absorption materials made of synthetic organic chemical product like Expanded Polystyrene(EPS), Expanded Polyethylene(EPE), Expanded Polyurethane(EPU), etc. have been used with general packaging material until the present. But nowadays, the use of these materials is intended to be decreased and to be recycled in connection with environmental pollution. In addition, it has been tried to substitute these materials with non-pollution materials(natural materials) like pulp mould, paper protectors, etc. At the same time, it is required to evaluate and analyze these cushioning materials for cushioning properties based on impact and vibration, in order to make an efficiency on the overall packaging system because they are generally being used by a random choice regardless of the properties of contents and cushioning materials. Therefore, this study provides analyzed data on cushioning properties of various cushioning materials against impact and vibration, and is intended to provide more efficient model for packaging system by minimizing their using amount through choosing an optimal cushioning material as well as intended to lead to the use of nonpollution materials in case these cushioning materials have same cushioning properties.

• Polymer(Korea)
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• v.32 no.1
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• pp.85-89
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• 2008

Acrylate polymer gel electrolytes containing N-methoxymethyl-N-methylpyrrolidium bis (trifluoro - methansulfonyl) imide (MPSI) as an ionic liquid were synthesized by solution polymerization in the presence of carbonate solvent. ionic conductivity and mechanical properties of the polymer gel electrolytes were investigated by impedance analyzer and universal testing machine as a function of the amount of polymer, and ionic liquid and type of crosslinker. The maximum ionic conductivity of polymer gel electrolytes was 0.8 mS/cm at $25^{\circ}C$ with 15 wt% of polymer, 30 wt% of ionic liquid and 5 wt% of crosslinker. The mechanical analysis showed that the tensile strength of polymer gel electrolytes increased with additional polymer contents and had the maximum value of 0.5 MPa with a reasonable ionic conductivity.

• Food Science of Animal Resources
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• v.34 no.6
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• pp.749-756
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• 2014

A rapid and simple analytical method for L-carnitine was developed for infant and toddler formulas by liquid chromatography tandem mass spectrometry (LC-MS/MS). A 0.3 g of infant formula and toddler formula sample was mixed in a 50 mL conical tube with 9 mL water and 1 mL 0.1 M hydrochloric acid (HCl) to chemical extraction. Then, chloroform was used for removing a lipid fraction. After centrifuged, L-carnitine was separated and quantified using LC-MS/MS with electrospray ionization (ESI) mode. The precursor ion for L-carnitine was m/z 162, and product ions were m/z 103 (quantitative) and m/z 85 (qualitative), respectively. The results for spiked recovery test were in the range of 93.18-95.64% and the result for certified reference material (SRM 1849a) was within the range of the certificated values. This method could be implemented in many laboratories that require time and labor saving.

• Membrane Journal
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• v.22 no.5
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• pp.301-308
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• 2012

Phosphazene diagnostic membranes were prepared to measure blood glucose level of diabetics. Final absorbances at 680nm through activated phosphazene membranes were measured at various temperature and humidity by varing concentration of glucose in blood. Measuring temperature and humidity did not seriously affected the end-point results of varing absorbance values as time (K/S). The effects of storage temperatures on the measurements of glucose concentration were studied after activated phosphazene diagnostic membranes were stored at various temperatures for 3 days, 1 week, 3 weeks, and 5 weeks. The stabilities of phosphazene dianostic membranes were confirmed even at RH 80%.

• Journal of the Korean Applied Science and Technology
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• v.6 no.1
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• pp.51-57
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• 1989

A series of four sodium ${\alpha}-sulfo$ fatty vinyl ester oligomers including sodium ${\alpha}-sulfo$ lauric acid vinyl ester oligomer, sodium ${\alpha}-sulfo$ myristic acid vinyl ester oligomer, sodium ${\alpha}-sulfo$ palmitic acid vinyl ester oligomer and sodium ${\alpha}-sulfo$ stearic acid vinyl ester oligomer were examined for surface activities such as surface tension, foaming power, foam stability, emulsifying power, dispersion effect, solubilization of orange OT. The critical micelle concentration(CMC) was also evaluated. Consequently, these sodium ${\alpha}-sulfo$ fatty acid vinyl ester oligomers were shown to have a good cohesive power and dispersion effect.

• Composites Research
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• v.18 no.3
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• pp.1-6
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• 2005

Carbon nanofiber exhibits superior and of ien unique characteristics of mechanical, electrical, chemical and thermal properties. Despite of the excellent properties of carbon nanofiber, the properties of carbon nanofiber filled polymer composites were not increased largely. The reason is that it is still difficult to ensure the uniform dispersion of carbon nanofiber in a polymer matrix. In this study, for improvement of the mechanical properties of composites, carbon nanofiber reinforced hybrid composites was investigated. For the dispersion of carbon nanofiber. solution blending method using ultrasonic was used. Dispersion of carbon nanoifiber was observed by scanning electron microscope (SEH). Mechanical properties were measured by universal testing machine(UTM).

• Archives of Pharmacal Research
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• v.29 no.2
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• pp.135-139
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• 2006

Activity-guided fractionation of the ethanol extract of the whole plant from Solanum lyratum resulted in the isolation of a new pregnane derivative glycoside, 16-dehydropregnenolone 3-O-${\alpha}$-L-rhamnopyranosyl-($1{\to}2$)-${\beta}$-D-glucopyranosid uronic acid (2), as well as other six known compounds: 16-dehydropregnenolone (1), allopregenolone (3), protocatechuic acid (4), vanillic acid (5), caffeic acid (6), and scopoletin (7). The structures of the isolated compounds were elucidated on the basis of their spectral data and chemical evidences. Compounds 1, 3, 4 were isolated for the first time from this plant. Cytotoxic activities of the isolated compounds were evaluated. Compound 1 exhibited significant cytotoxic activity against A375-S2, HeLa, SGC-7901, and Bel-7402 with $IC_{50}$ values of $13.1{\pm}0.9,\;21.5{\pm}1.0,\;40.2{\pm}0.7$, and $49.8{\pm}1.2\;{\mu}g/mL$, respectively.

• Journal of the Korean Ceramic Society
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• v.55 no.5
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• pp.480-491
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• 2018

Calcium phosphates (CaP) were prepared by a wet chemical method. Micro-crystalline dicalcium phosphate (DCPD) was precipitated at $37^{\circ}C$ and pH 5.0 using $Ca(OH)_2$ and $H_3PO_4$. The precipitated DCPD solution was kept at $37^{\circ}C$ for 96 h. Artificial bone cement was composed of DCPD, $Ca(H_2PO_4)_2{\cdot}H_2O$ (MCPM), and $CaSO_4{\cdot}1/2H_2O$, $H_2O$ and aqueous poly-phosphoric acid solution. The wet prepared CaP powder was used as a matrix for the bone cement recipe. With the addition of aqueous poly-phosphoric acid, the cement hardening reaction was started and the CaP bone cement blocks were fabricated for the mechanical strength measurement. For the tested blocks, the mechanical strength was measured using a universal testing machine, and the microstructure phase analysis was done by field emission scanning electron microscopy and X-ray diffraction. The cement hardening reaction occurred through the decomposition and recrystallization of MCPM and $CaSO_4{\cdot}1/2H_2O$ added on the surface of the wet prepared CaP, and this resulted in grain growth in the bone cement block.

• Proceedings of the Korean Institute of Building Construction Conference
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• 2018.11a
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• pp.189-190
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• 2018

KS standards mostly relate to single component material evaluation, so in cases of underground structure environments, most cannot predict the existing composite forms of deterioration, resulting in the applied waterproofing materials becoming unable to respond to these damaging factors. Current domestic waterproofing market in Korea mainly uses single-ply waterproofing materials comprised of coatings or waterproof sheets and two or more-ply composite waterproofing methods. In order to evaluate these types of composite waterproofing systems, a new test equipment and method that incorporates various deterioration conditions (joint displacement, chemical exposure, water pressure etc) was developed. In a comparison testing, the results showed that flexible type materials have higher response performance towards joint displacement than the hardened material.