The purpose of this study was to evaluate the effect of wetting condition made by drying time on bonding of resin cement to dentin. Freshly extracted bovine teeth were grinded to expose flat dentin surfaces. After the exposed dentin surfaces were treated with pretreatment agents and water rinse, each wetting condition of dentin surfaces was made according to drying times and methods including slight blow bry for I-second by air syringe, blow dry for 20-second by air syringe, and 12-hour dry in desiccator respectively. and then, previously made composite resin specimens were bonded onto each conditioned dentin surface of the specimen using Panavia-21(Kuraray Co.), Bistite(Tokuso Co.), and Choice(use with All bond-2, Bisco Inc.) resin cement according as manufacturer's instruction. Bonded specimens were stored in $37^{\circ}C$ distilled water for 24 hours, then the tensile bond strength was measured, cohesive failure rate was calculated, and fractured dentin surfaces and acrylic rod sides were examined under scanning electron microscope. The result were as follows ; In the group of bonding with Panavia-21 resin cement, higher tensile bond strength was seen in 12-hour dry group than in I-second and 20-second dry group(p<0.01). In the group of bonding with Bistite resin cement, higher tensile bond strength was seen in 1-second dry group than in 20-second and 12-hour dry group(p<0.01). In the group of bonding with Choice resin cement, no significant differences of bond strength under given drying time were seen. Cohesive failure rates derived from the groups of bonding with Panavia-21 and Choice resin cement were increased with the increase of tensile bond strength in each drying time. On SEM examination of fractured surface, adhesive failure mode with fractured resin tags was mostly seen in wet condition with I-second drying time in the group of bonding with Panavia-21 resin cement, mixed failure mode with shortened and fractured resin tag was seen in the group of bonding with Bistite resin cement, and regardless of drying time, and cohesive-adhesive mixed failure mode with fracture of 'Hollow' typed resin tags was mainly seen in the group of bonding with Choice resin cement.
Kim, Hyun-Wook;Park, Gye-Young;Han, Jin-Gu;Han, Young-Sun;Hwang, Bum-Gu;Lee, Jun-Hyuk
Journal of Korean Society of Occupational and Environmental Hygiene
/
v.20
no.2
/
pp.88-93
/
2010
To confirm and quantify asbestos fibers released from the asbestos-cement slate roofs due to weathering, three houses, selected based on the year of built - 60's, 70, and 80's, were investigated. All of them were located in the downtown of Seoul. Rain or snow-melt water was collected from the roof in a 3.5 liter plastic bottle. A known amount of collected water was filtered on the 37 mm membrane filter, ashed in a muffle furnace, and subsequently treated with HCl to remove organic material. The treated remaining was refiltered on a 25mm membrane filter for PLM and PCM analyses. The NIOSH 7400 method was utilized for PCM counting. In addition, SEM/EDX was used to confirm the asbestos types. The results of this study showed that chrysotile fibers were confirmed by PLM in all samples analyzed. A significant amount of asbestos fibers were found in the water samples. The ranges of asbestos fibers counted from the samples collected in the 60's, 70's, and 80's were; 10,406.3~55,575.6 f/L, 5,218.8~38,126.2 f/L, and 2,906.3~7,798.6 f/L, respectively. As anticipated, concentrations of asbestos fibers increased with time of installment of the roofing material. We conclude that weathering can be a significant factor on the release of asbestos fibers from the asbestos cement products. Since asbestos fibers released into environment can be a source of significant health hazard, countermeasures, such as replacement, removal, and encapsulation of weathered asbestos slate, should be initiated immediately.
The purpose of this study was to evaluate the bond strength of glassionomer cement against cut dentin surface which was treated with various surface cleaning agents. 48 freshly extracted human 3rd molars were ground flat through the enamel into the dentin using 600 grit silicone carbide paper under a flow of water. The were divided into four groups by the following cleaning procedure on cut dentin surface; Group I : No surface treatment after grinding with 600 grit silicone carbide paper as control group Group II : Surface treatment with 50% citric acid for 30 seconds. Group III : Surface treatment with 37% phosphoric acid for 30 seconds. Group IV : Surface treatment with 10% poly acrylic acid for 30 seconds. The specimens in 4 groups were immersed in distilled water at $37^{\circ}C$ for 24 hours before testing after cleanising with water-spray and drying with air. Bond strength was measured with Instron Universal Testing Machine (Autograph S-100, Shimadzu, Kyoto, JAPAN). The results were as follows: 1. The bond strengths of group II, III & IV were not seemed to be shown more significant improvement than a group I. 2. The bond strengths in groups which were treated with 50% citric acid, 37% phosphoric acid and 10% polycrylic acid, were ranked 24.70kg/$cm^2$, 22.02kg/$cm^2$ and 31.13kg/$cm^2$, but its difference was not significant, statistically.
Kim, Jun-Young;Jang, Eui-Ryong;Chung, Choong-Ki;Jang, Soon-Ho
Journal of the Korean Geotechnical Society
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v.27
no.5
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pp.5-15
/
2011
Recent increase of large scale construction near costal area has also increased the application of soft ground treatment. As a result, solidification with cement and lime which increases stability and durability of soils, is frequently used for surface layer stabilization in soft ground site. While stabilization of very soft clay with high plasticity and compressibility has widely been studied, studies on silty clay with low plasticity and compressibility are relatively rare. In this study, after stabilizing low plasticity silty clay of Songdo area with cement and lime under various water contents, mixing ratio, and curing time, uniaxial compression test and plate load test were performed. Strength properties from both tests were considerably consistent. And trackability of construction equipment on the treated surface layer of dredged land was estimated. Finally, optimum mixing condition for Songdo silty clay was proposed.
This study was performed to reuse the dyeing wastewater sludge treated by Fenton process through the solidification/stabilization technique. To solidify the dyeing sludge the industrial by-products such as blast furnace slag, fly ash and waste sand with cement were used. The laboratory scale and pilot scale test were conducted at room temperature to make construction brick which has high compressive strength and low leaching of heavy metals. The experimental results showed that blast furnace slag and fly ash could be used instead of cement and the products satisfied the regulation of Korean Standards. The blast furnace slag increased the compressive strength and the optimum ratio of slag/dyeing sludge on dry basis was found 0.4. The solidifying agent of SB series could increase rapidly the compressive strength and the optimum ratio of solidifying agent/sludge on dry basis was 0.26 at which the strength was two times compared with non-added condition. The portion of waste and industrial by-products in matrix was over 80%. From the pilot test the optimum pressure in molding was 100kg/$\textrm{cm}^2$ at which the compressive strength was over 100kg/$\textrm{cm}^2$. And the strength increased continuously to 160kg/$\textrm{cm}^2$ until 120 days curing time due to pozzolanic reaction. When SB-20 as a solidifying agent was used, the unconfined compressive strength of dyeing sludge could be obtained 110kg/$\textrm{cm}^2$ which satisfied the regulation of cement brick in Korea Standard(KS).
Post and core is used to restore endodontically treated teeth, and it is a very important part which supplies retention and support to the prosthesis. But occasionally, caries occured due to the microleakage at the post and core and tooth interface, the failure of prosthesis has happened. In this study, the microleakage of cast gold post and core, amalgam core, and composite resin core was investigated and compared. The coronal part of the extracted upper anterior teeth were removed and endodontically treated with conventional method. The teeth were divided into three groups. In group 1, cast gold post and core was cemented with resin cement and in group 2, ready-made post was cemented with resin cement and amalgam core was built. In group 3, ready-made post was cemented with resin cement and composite resin core was built. All specimens were thermocycled between $5^{\circ}C\;and\;55^{\circ}C$ with dwell time of 15 seconds, and immersed in 0.5% aqueous solution of basic fuchsin dye for 24 hours. After embedded in the epoxy resin, the specimens were sectioned longitudinally and observed with stereomicroscope with the magnification of 25. From the findings of this study, the following conclusions were obtained. 1. There was microleakage at the core/tooth interface of all specimens. 2. The microleakage of gold post and core was significantly less than those of the other two groups. 3. There was no significant difference between the microleakage of amalgam core and that of composite resin core.
Expansive soil is the most predominant geologic hazard which shows a large amount of shrinkage and swelling with changes in their moisture content. This study investigates the macro-mechanical and micro-structural behaviours of dredged natural expansive clay from coal mining treated with ordinary Portland cement or hydrated lime addition. The stabilised expansive soil aims for possible reuse as pavement materials. Mechanical testing determined geotechnical engineering properties, including free swelling potential, California bearing ratio, unconfined compressive strength, resilient modulus, and shear wave velocity. The microstructures of treated soils are observed by scanning electron microscopy, x-ray diffraction, and energy dispersive spectroscopy to understand the behaviour of the expansive clay blended with cement and lime. Test results confirmed that cement and lime are effective agents for improving the swelling behaviour and other engineering properties of natural expansive clay. In general, chemical treatments reduce the swelling and increase the strength and modulus of expansive clay, subjected to chemical content and curing time. Scanning electron microscopy analysis can observe the increase in formation of particle clusters with curing period, and x-ray diffraction patterns display hydration and pozzolanic products from chemical particles. The correlations of mechanical properties and microstructures for chemical stabilised expansive clay are recommended.
Joh, Ju Yeon;Bae, Young Gon;Kim, Yang Hyun;Lee, Eun Hyung;Lee, Chul Joong;Lee, Sang Chul;Kim, Yongn Lak
The Korean Journal of Pain
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v.18
no.2
/
pp.204-207
/
2005
Background: Transpedicular percutaneous vertebroplasty, along with kyphoplasty of the thoracic vertebrae, is technically more difficult than those of the lumbar vertebrae due to the anatomical differences. During the last four years, all the percutaneous vertebroplasty and kyphoplasty of the thoracic vertebrae carried out at our institution were performed using a transpedicular approach; therefore, we tried to find if there were any problems or complications associated with the process. Methods: The medical records of all the patients who had undergone thoracic percutaneous vertebroplasty or kyphoplasty were retrospectively reviewed. The following were looked up: the procedure name, unipedicular or bipedicular, the level of the thoracic vertebrae treated, and the pre- and postoperative changes in the Visual Analog Scales (VAS), the volume of cement injected and complications. Results: In the last four years, 58 vertebral bodies in 58 patients were treated. Twelve and 46 vertebral bodies were treated by kyphoplasty and vertebroplasty, respectively. A total of 58 mid and lower thoracic levels were treated: T5 (n=1), T6 (n=1), T7 (n=3), T8 (n=4), T9 (n=1), T10 (n=4), T11 (n=14) and T12 (n=30). The mean preoperative and postoperative VAS scores were $8.1{\pm}1.4$ and $5.2{\pm}1.7$, respectively. The mean volume of cement injected was $4.01{\pm}1.85ml$; $3.18{\pm}0.60ml$ at T5-8 and $4.22{\pm}2.27ml$ at T9-12. There were no clinical complications, such as pedicular fracture or cement leakage. Conclusions: Although transpedicular vertebroplasty and kyphoplasty at the mid to lower thoracic vertebral bodies is technically difficult compared to that at the lumbar region, the procedures can be performed safely.
Journal of Dental Rehabilitation and Applied Science
/
v.22
no.3
/
pp.221-230
/
2006
Recently, the need for esthetic results has increased the interest for all-ceramic crown prosthesis. Furthermore, the development of zirconium core via CAD/CAM system has allowed the all ceramic restorations to be applied to almost all fixed prosthesis situations. But, the increased strength has been reported to increase in proportion with the bond strength of cement, and recently, the tribochemical system which increases the bond strength through, silica coating and silanization has been introduced. The purpose of this study was to compare the $Rocatec^{TM}$ system and $CoJet^{TM}$ system with the traditional acid etching and silanization method of the irconium based ceramic. The surface character was observed via SEM(X2000), and the bond strength with the resin cement were measured. 50 In-Ceram Zirconia (Adens, Korea) discs were fabricated and embedded in resin, group 1 was treated with glass-bead blasting and cleaning, group 2 was treated with 20% HF for 10 minutes and silanized, group 3 was treated with the $Rocatec^{TM}$ system, and group 4 was treated with the $CoJet^{TM}$ system. Each group was comprised of 10 specimens. The specimens were cemented to a $3mm{\times}5mm$ resin block with Super-Bond C&B. The shear bond strength was measured with the $Instron^{(R)}$ 8871 at a crosshead speed of 0.5mm/min. The results were as follows. 1. According to SEM results, there were little difference between group 1 & group 2, but in group 3 and 4, silica coating was detected and there was increase in surface roughness. 2. The shear bond strength decreased in the order of group 3(46.28MPa), group 4(42.04MPa), group 2(31.56MPa), and group 1(27.46MPa). 3. There was significant differnce between group 1&2 and group 3&4(p<0.05). From the results above, it can be considered that the conventional method of acid etching and silane treatment cannot increase the bond strength with resin cements, and that by applying the tribochemical system of $Rocatec^{TM}$ system and $CoJet^{TM}$ system, we can achieve a stronger all ceramic restoration. Further studies on surface treatments to increase the bond strength are thought to be needed.
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