• Title/Summary/Keyword: borax

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Preparation of Low Density Ceramic Supporter from Fly Ash with Borax and Glass Powder (붕사 및 유리분말을 첨가한 석탄회로부터 저밀도 세라믹 담체의 제조)

  • Hwang, Yeon;Lee, Hyo-Sook;Lee, Woo-Chul;Bae, Kwang-Hyun;Jeong, Yong-Dae;Lee, Won-Kwon
    • Resources Recycling
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    • v.9 no.2
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    • pp.40-45
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    • 2000
  • Low density ceramic supporter was prepared by using fly ash as a starting mterial with borax or glass powders. Also the wheat powders were used by 30 wt% to increase the initial porosity of the supporter. The density of the supporter decreased as the amount of borax increased. The bulk density of $0.79g/\textrm{cm}^3$ and the apparent density of $1.10g/\textrm{cm}^3$ were obtained when the fly ash with 15% of borax was sintered at $1160^{\circ}C$ for 15 minutes. The density also decreased as the plate glass powders past through $212\mu\textrm{m}$ size were mixed. When the fly ash with 12% of glass powder was sintered at $1280^{\circ}C$ for 10 minutes, the bulk and apparent density were $0.90g/\textrm{cm}^3$ and $1.00g/\textrm{cm}^3$, respectively.

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A Study on the Toughness of Die Steel Coated with VC (vanadium carbide) by Immersing in Molten Borax Bath (용융염 침적법에 의한 VC Coating 금형강의 인성에 관한 연구)

  • Lee, B.K.;Nam, T.W.
    • Journal of the Korean Society for Heat Treatment
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    • v.6 no.2
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    • pp.59-69
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    • 1993
  • Bending fracture strength test and impact strength test were made for VC coated die steels treated by immersing in molten borax bath and for hardened steels which were quenched and tempered, in order to clarify the effect of VC coating at $1000^{\circ}C$. The material used in this investigation was representative cold and hot work die steels STD11, STD61. The results obtained are as follows. 1) The bending fracture strength of VC coated die steel (STD11, STD61) was lessened with increasing the thickness of the VC coated layer. 2) With increasing the immersing time (imcreasing the thickness of the VC coated layer) the maximum hardness was obtained at 480 minutes holding, after that holding time hardness was decreased. 3) The impact strength of the VC coated die steel was not decreased. In the casse of STD11, it was higher than that of the quenched condition especially at low tempering temperature, and vice versa at high tempering temperature. However in the case of STD61 shows the result to the contrary.

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Adsorptive Stripping Voltammetrical Determination of Zirconium (흡착벗김 전압전류법적 지르코늄의 정량)

  • Choi, Won Hyung;Lee, Jin Sik;Kim, Do Hoon;Kim, Jong Cheol
    • Analytical Science and Technology
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    • v.6 no.5
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    • pp.425-433
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    • 1993
  • Adsorptive stripping voltammetric determination method of trace zirconium using oxine as a ligand was studied. Optimal conditions found to be $2.5{\times}10^{-3}M$ borax buffer solution(pH 8.5) containing oxine concentration of $4{\times}10^{-8}M$. Accumulation potential was -0.2V, accumulation time was 400sec and scan rate was 4mV/sec. Calibration plots for zirconium are linear over the range of $1{\sim}100{\mu}g/L$ in optimal condition.

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Development of Phase Change Thermal Energy Storage System (상변화 물질을 이용한 고효율 축열시스템 개발)

  • 장진택;유영선;윤진하;김영중;장유섭;강금춘
    • Proceedings of the Korean Society for Bio-Environment Control Conference
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    • 1998.05a
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    • pp.77-82
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    • 1998
  • 현재 온실 난방에 주로 이용되고 있는 난방기는 대부분이 화석에너지를 연료로 사용하고 있다. 따라서 생산비의 가중이 불가피하며, 또한 연소 과정에서 발생하는 배기 가스로 인하여 환경 오염이 문제시되고 있다. 따라서 태양에너지를 보다 더 적극적으로 활용할 수 있는 기술의 개발이 요구된다. 태양에너지를 시설 농업에 적극적으로 이용하기 위해서는 주간에 밀도가 낮은 태양에너지를 고밀도로 축열하여 기온이 급강하하는 야간의 보온에 활용하여야 한다. 주간의 온실내 잉여 태양에너지를 축열할수 있는 상변화 온도 3$0^{\circ}C$ 수준의 잠열축열재를 개발하기 위하여 수행한 본 연구의 결과를 요약하면 다음과 같다. 1. SCD에 Borax를 0.0~5.0wt% 첨가하여 과냉도를 25.$0^{\circ}C$에서 $1.5^{\circ}C$ 이하로 조절하였으며, Borax의 적정 함량은 3.0wt%였다. 2. SCD에 Carbopol을 0.0~3.0wt% 첨가하여 상분리량을 70.0%에서 0.0%로 조절하였으며, Carbopol의 적정 함량은 1.5wt%였다.3. 축열재 내구성 검증을 위하여 0~1,500회의 상변화 사이클을 수행하였다. 이때 상변화 온도의 변화량이 $\pm$1.$0^{\circ}C$ 이하, 잠열량 변화가 $\pm$2.0 kacl/kg 이하로서 안정된 값을 보였다. 이상의 결과로 볼 때 축열재의 수명을 10년까지는 보장할 수 있는 것으로 판단되었다.

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A study on Adhesion and Wear Resistance of Vanadium Carbide Coating on Die Steels by Immersing in Molten Borax Bath (용융 붕사욕 침지법에 의해 금형용 강에 형성된 VC coating층의 밀착성과 내마모성에 관한 연구)

  • Lee, B.K.;Nam, T.W.
    • Journal of the Korean Society for Heat Treatment
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    • v.13 no.2
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    • pp.71-84
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    • 2000
  • A study on adhesion and wear resistance of VC(vanadium carbide) coating on die steels, STD11 and STD61, has been carried out. The VC coating on the die steels was made by immersing them in molten borax bath, a kind of TRD(thermo-reactive deposition and diffusion). Adhesion strength and wear resistance were investigated using scratch test, indentation test and plate-disc test(Ogoshi type) respectively. The influence of sliding distance on the amount of wear has been determined and dominant wear mechanisms has been characterized using optical microscopy, scanning electron microscopy and EDS spectroscopy. The critical adhesion strength($L_c$) between VC coating layer and substrate(STD11) was increased to 60N($L_c$) in the scratch test. In the case of STD61, the strength increased to 24N. The wear resistance of VC coated die steels was excellent because the diffusion layer formed just below the coating layer. The dominant wear mechanism was identified as adhesive wear for VC coating die steels which were worn by combination of cracking and plucking of VC fragments and disc.

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Nonlinear response of complex fluids under LAOS(large amplitude oscillatory shear) flow

  • Ahn, Kyung-Hyun;Kyu Hyun;Nam, Jung-Gun;Manfred Wilhelm;Lee, Seung-Jong
    • Korea-Australia Rheology Journal
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    • v.15 no.2
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    • pp.97-105
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    • 2003
  • In the previous paper (Hyun et al.,2002), we have investigated the shape of storage modulus (G') and loss modulus (G") of complex fluids under large amplitude oscillatory shear (LAOS) flow. As the strain amplitude increases, owever, the stress curve becomes distorted and some important information may be smothered during data processing. Thus we need to investigate the stress data more precisely and systematically. In this work, we have obtained the stress data using high performance ADC (analog digital converting) card, and investigated the nonlinear response of complex fluids, 4wt% xanthan gum (XG), 2 wt% PVA/ 1 wt% Borax, and 1 wt% hyaluronic acid (HA) solutions, using Fourier transformation (FT) rheology. Comparing the strain signals in time domain with FT parameters in frequency domain, we could illustrate the sensitivity and importance of FT rheology. Diverse and unique stress patterns were observed depending on the material system as well as flow environment. It was found that they are not the outcome of experimental deficiency like wall slip but characteristics of the material system. When nonlinear response of complex fluids is analyzed, the intensity and phase angle of higher harmonic contributions should be considered together, and the shape of the stress signal was found to be strongly dependent upon phase angle.ngle.

Reliability of the Impregnated Boron Compounds, Citric Acid- and Heat-Treated Samama (Anthocephalus macrophyllus) Wood against the Fungal and Termite Attacks

  • Trisna PRIADI;Guruh Sukarno PUTRA;Tekat Dwi CAHYONO
    • Journal of the Korean Wood Science and Technology
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    • v.51 no.1
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    • pp.49-57
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    • 2023
  • This research aimed to evaluate the durability of Samama (Anthocephalus macrophyllus) wood treated with boron preservatives, citric acid (CA), and heating against termites. Wood samples were impregnated firstly with 5% boron solutions, such as boric acid, borax and boric acid + borax combination at 1:1 (w/w). The second impregnation used 5% CA. The impregnations were conducted in a pressure tank at 7 kg/cm2 for 4 hours. After impregnation, the samples were heat treated at 80℃ or 160℃. All the treated and control samples were exposed to decay fungi, drywood termites and subterranean termites based on SNI 7207:2014 standard. The results showed that boron preservatives reduced fungal attacks on Samama wood. The combination treatment of boric acid, CA and heat treatment at 160℃ was also effective to increase the resistance of Samama wood against white- and brown rot fungi, and drywood termites. Heat treatment consistently improved the resistance of Samama wood from decay fungi.

Evaluation of the Potential of Wood Preservatives Formulated with Okara (두부비지를 이용한 목재 방부제의 사용가능성 평가)

  • Kim, Ho-Yong;Choi, In-Gyu;Ahn, Sye-Hee;Oh, Sei-Chang;Hong, Chang-Young;Min, Byeong-Cheol;Yang, In
    • Journal of the Korean Wood Science and Technology
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    • v.36 no.1
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    • pp.110-123
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    • 2008
  • The use of CCA as a wood preservative was recently inhibited due to its environmental pollution and human harmfulness. Instead of CCA, copper azole (CuAz) and alkaline copper quaternary (ACQ) have been used as alternative wood preservatives, but the price of the preservatives is much more expensive than that of CCA. As a substitute for high-priced CuAz and ACQ, environmentally friendly wood preservatives were formulated with okara, which is an organic waste from the production of tofu. Prior to formulating the preservatives, okara was hydrolyzed by three levels of sulfuric acid concentration (1, 2.5 and 5%) to easily penetrate the effective components of the preservatives into wood blocks. Final preservative solutions were formulated with the hydrolyzed okara and metal salts, such as copper sulfate, copper chloride and borax. The preservatives were treated into wood blocks by vacuum-pressure method to measure the treatability of the preservatives, and the treated wood blocks were placed in hot water for three days to measure the leachability of the preservatives. The effective components of the preservatives might be successfully penetrated into wood blocks through the uses of hydrolyzed okara and ammonia water. However, the leached amount of effective components was increased as the concentration of acid used for the hydrolysis of okara increased. The treatability and leachability of the preservatives were not affected by hydrolysis temperature but negatively affected by the addition of borax. Based on the results above, the optimal conditions for formulating okara-based wood preservatives cost-effectively and environmentally might be 1% acid hydrolysis of okara and the use of $CuCl_2$ as a metal salt. In addition, the treatability and leachability of okara-based wood preservatives were superior or no differences comparing with those of CuAz. Therefore, it is concluded that okara-based wood preservatives might have a potential to be used as an environmentally friendly wood preservative.

Combustion Characteristics of Hinoki Cypress Louver after Pressure Impregnation with Boric Acid, Borax and Ammonium Phosphate (붕사, 붕산 및 인산암모늄을 가압 함침한 편백 루버의 연소특성)

  • Park, Hyung-Ju
    • Fire Science and Engineering
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    • v.29 no.6
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    • pp.1-5
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    • 2015
  • In this study, the combustion characteristics of Hinoki Cypress Louver were measured after performing pressure impregnation with aqueous solution of boric acid, borax, and ammonium phosphate. The characteristics measured include ignition time, critical heat flux, and mass loss rate by incident hear flux (25, 30 and $50kW/m^2$). The samples used for the test were $100{\times}100{\times}10mm$, and the 5 min variation for each incident heat flux was measured 3 times. The results show that the ignition time for incident heat flux of $25kW/m^2$ showed a delay effect of 17.4 to 21.3% except for Type C-H. There was no significant difference at 35 and $50kW/m^2$ in the average mass loss rate in Types A-H and D-H, which had lower rates than Type N-H, which was predicted to be higher than that of Type N-H ($10.7kW/m^2$) by 38.22 to 60.46%. It is thus expected that at the time of initial primary fire, there would be a delay effect against fire spread.

An experimental study on the preparation and property of the sintering aggregate using fly ash (플라이애쉬를 이용한 소성골재의 제조 및 특성에 관한 연구)

  • 박대영;김도수;박종현;임채영;노재성
    • Proceedings of the Korea Concrete Institute Conference
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    • 1998.10a
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    • pp.239-244
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    • 1998
  • Fusion temperature of fly ash was determined with wasted glass wool and borax using ash fusion determinator, 0.5wt% of bentonite and water glass used as binder, 50wt% of wasted glass wool added to fly ash, fusion temperature of fly ash was 1, 156$^{\circ}C$. Pellet was prepared, and then sintered at 1, 00$0^{\circ}C$ and 1, 10$0^{\circ}C$. Water-absorption rate, specific gravity, porosity and pore structure of sintering aggregate was determined.

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