• Title/Summary/Keyword: bonding material

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REMOVAL TORQUE OF BICORTICALLY STABILIZED RBM(RESORBABLE BLAST MEDIA) PIN IMPLANTS IN RABBIT TIBIA

  • Kim, Kwon-Sik;Suh, Kyu-Won;Lee, Richard Sung-Bok;Ryu, Jae-Jun
    • The Journal of Korean Academy of Prosthodontics
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    • v.44 no.6
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    • pp.722-733
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    • 2006
  • Statement of problem. The use of small diameter implants having less than 3 mm in diameter were restricted because of lack of bonding strength to bone. Purpose. The purpose of this study was to observe how much resorbable blast media pin implants increase the binding force to the bone compared to machined transitional pin implants by measuring removal torque, and whether they can be used as final implants for replacement of small diameter teeth. Material and method. Fifteen rabbits were used in this study. Two kinds of implants (resorbable blast media pin implants and machined transitional pin implants) were inserted in each tibia bicortically. After healing time of 2, 4 and 8 weeks, the removal torque values were recorded and the rabbits were sacrificed for histological analysis. Linear finite element method analyses were conducted to compare bicortical fixation with monocortical fixation. Result and conclusion. Within the limitation of this in vivo study, the following conclusions were drawn: 1) The removal torque value of RBM pin implants showed statistically significant increase compared to machined pin implants at 2, 4, and 8 weeks respectively (p<0.05). 2) The removal torque value of RBM pin implants at 2, 4, and 8 weeks was increased statistically significantly with time (p<0.05). 3) Bicortical fixation showed better stress distribution compared with monocortical fixation in a linear finite element method analysis. 4) RBM pin implants are not recommended as transitional implants because they showed a lot of bone fracture in histologic specimens.

A Study on Iron Compounds Accompanied in Korean Kaolin Minerals (국산 Kaolin 광물에 수반된 철화합물의 종류 및 존재상태 구명에 관한 연구)

  • 박금철;최석진;박영갑
    • Journal of the Korean Ceramic Society
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    • v.11 no.2
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    • pp.22-30
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    • 1974
  • This study was carried out to investigate the species of iron compounds in kaolin mineral and the bonding relation between the major kaolin and its subordinate iron compound existing as incidental mineral in common clay by means of chemical composition, X-ray diffraction, thermal differential and thermogravimetrie analysis for the application of clays in the field of ceramic raw material. The domestic clay are produced abounduntly in many places, but San-Cheong kaolin, Chu-An clay, and Yeong-Am clay were selected as samples in this experiment because of their frequent utilization in porcelain industry. Two kinds of samples with low and high iron content are picked up respectively from the place of production and elutriated under two micron size to determine the properties and concentration of iron compound very fine particles or colloidal substance of low crystalline grade. Therefore, hydrothermal treatment in autoclave was conducted considering the existence of low crystalline grade of iron compounds known as an amorphoue state in X-ray diffraction pattern furthermore, de-iron treatment of hydrothermal compound was done in order to identify the related iron compound before and after hydrothermal reaction and iron compound which is one of the samples was synthesized for the determination of their compounds state in more detail. The obtained results in this study are as follows: In San-Cheong kaolin, Chu-An clay and Yeong-Am clay 1) It is proved that species accompanying iron compound is $\alpha$-FeOOH form. 2) Iron compound is composed of very fine particles or colloidal substance. 3) The iron substance encircles the fine parts of clay minerals under 2 micron and acts as cementizing agent.

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The Analysis on Properties of Epoxy/MWCNT for Bonding CFRP to Steel Plates (CFRP와 금속 재료의 접합을 위한 epoxy/MWCNT의 특성 분석)

  • Yoo, Sung-Hun;Kwon, Il-Jun;Shin, Dong-Woo;Park, Sung-Min;Yeum, Jeong-Hyun
    • Composites Research
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    • v.30 no.3
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    • pp.215-222
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    • 2017
  • The effect of a multi walled carbon nanotubes (MWNCT) on the adhesive properties and thermal properties of epoxy were studied by double lap-shear tests. Epoxy/MWCNT resins were prepared from a different amount of the MWCNT incorporated into the epoxy resins (araldite 2011). Steel plates and carbon fiber reinforced plastics (CFRP) were chosen as materials. Mechanical tests were performed by a universal testing machine (UTM). The analysis of thermal properties were conducted by a thermogravimetric analyzer (TGA) and a differential scanning calorimetry (DSC). The fracture surface morphology was examined using a scanning electron microscopy (SEM) and optical microscope. Compared to neat epoxy, it was found that the mechanical properties of epoxy/MWCNT resins are increased.

Characteristics of bending strength and residual stress distribution on high thermal cycle of ceramic and metal joint (세라믹/금속접합재의 고온 열사이클에 따른 잔류응력분포 및 굽힘강도 특성)

  • Park, Young-Chul;Hue, Sun-Chul;Boo, Myoung-Hwan;Kim, Hyun-Su;Kang, Jae-Wook
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.21 no.10
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    • pp.1541-1550
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    • 1997
  • Since the ceramic/metal joint material is made at a high temperature, the residual stress develops when it is cooled from bonding temperature to room temperature due to remarkable difference of thermal expansion coefficient between ceramic and metal. As residual stress at ceramic/metal joints influences the strength of joints, it is important to estimate residual stress quantitatively. In this study, it is attempted to estimate joint residual stress of Si$_3$N$_4$STS304 joints quantitatively and to compare the strength of joints. The difference of residual stress is measured when repeated thermal cycl is loaded, under the conditions of the practical use of the ceramic/metal joint. The residual stress increases at 1 cycle of thermal load but decreases in 3 cycles to 10 cycles of thermal load. And 4-point bending test is performed to examine the influence of residual stress on fracture strength. As a result, it is known that the stress of joint decreases as the number of thermal cycle increases.

Modeling of RC shear walls strengthened by FRP composites

  • Sakr, Mohammed A.;El-khoriby, Saher R.;Khalifa, Tarek M.;Nagib, Mohammed T.
    • Structural Engineering and Mechanics
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    • v.61 no.3
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    • pp.407-417
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    • 2017
  • RC shear walls are considered one of the main lateral resisting members in buildings. In recent years, FRP has been widely utilized in order to strengthen and retrofit concrete structures. A number of experimental studies used CFRP sheets as an external bracing system for retrofitting of RC shear walls. It has been found that the common mode of failure is the debonding of the CFRP-concrete adhesive material. In this study, behavior of RC shear wall was investigated with three different micro models. The analysis included 2D model using plane stress element, 3D model using shell element and 3D model using solid element. To allow for the debonding mode of failure, the adhesive layer was modeled using cohesive surface-to-surface interaction model at 3D analysis model and node-to-node interaction method using Cartesian elastic-plastic connector element at 2D analysis model. The FE model results are validated comparing the experimental results in the literature. It is shown that the proposed FE model can predict the modes of failure due to debonding of CFRP and behavior of CFRP strengthened RC shear wall reasonably well. Additionally, using 2D plane stress model, many parameters on the behavior of the cohesive surfaces are investigated such as fracture energy, interfacial shear stress, partial bonding, proposed CFRP anchor location and using different bracing of CFRP strips. Using two anchors near end of each diagonal CFRP strips delay the end debonding and increase the ductility for RC shear walls.

Electron Microscopic Study of Osseointegration between Bone and Smooth Machined Implants (선반가공 임플란트와 골조직의 유착에 관한 전자현미경적 연구)

  • Chang, Byung-Soo
    • Applied Microscopy
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    • v.34 no.4
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    • pp.277-283
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    • 2004
  • This paper reports that the ultrastructural nature of the interface process between the implants and surrounding bone has been studied after in vivo 1, 4, 8, 12 weeks of implantation of smooth machined implants into rabbit tibias. There was no indication of the fibrous connective tissue formation around the implant that imply intolerance of the bone tissue towards the implant after 1 week of implantation. The regions showing direct bone tissue bonding to the smooth machined implant contained osteoblast activating across the interface in the direction after 4 weeks of implantation. The reaction of a smooth machined implant caused in the first instance formation of an amorphous woven bone, which transformed into a mineralized bone containing collagen fibers. After 8 weeks of implantation, the activities of osteoblast initiated osseointegration forming bone matrix at the interface. During this period, the osteoblast surrounded with a matrix consisting of collagen bundles running in various directions. In the interface area between newly formed bone tissue and implants which has been inserted in rabbit tibias for 12 weeks, the implant and mineralized bone was separated by an amorphous electron dense material layer about $1{\sim}1.5{\mu}m$ in thickness.

Re-Repair Method for Deterioration of Partial Depth Repair Section in Portland Cement Concrete Pavement (콘크리트 포장 부분단면보수 재파손 구간의 적정 보수 방안)

  • Lee, Yong Hyeon;Kim, Hyun Seok;Jung, Won Kyong;Oh, Han Jin;Kim, Hyung Bae
    • International Journal of Highway Engineering
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    • v.19 no.5
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    • pp.33-42
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    • 2017
  • PURPOSES : The purpose of this study is to suggest the construction and quality control method for the re-repair of a deteriorated partial depth repair for sections of Portland cement concrete pavement. METHODS : An experimental construction was conducted to extend the repair width for removing an existing repair section. A removal method was used to ensure early performance for a deteriorated partial depth repair section. Bond strength and split tensile strength were measured at the near vertical interface layer between the existing pavement and repair material. The area was analyzed for various conditions such as the extended repair area and the removing method of the existing repair section. RESULTS : As a result of analysis of bond strength and split tensile strength, the bonding performance of a milling removed section was improved over a cutting and hand breaker removed section. The bond strength was analyzed to increase slightly as the extended repair width for removing the existing repair section increased. The split tensile strength did not show a clear relationship to an increased extended repair width of an existing removed repair section. CONCLUSIONS : The milling removal method should be applied in the removal of existing deteriorated partial depth repair sections. The extended repair width for a re-repair section should be wider than the existing partial depth repair with at least a 75-mm length and width for the bond strength and the split tensile strength.

Brazing of Aluminium Nitride(AlN) to Copper with Ag-based Active Filler Metals (은(Ag)계 활성금속을 사용한 질화 알미늄(AlN)과 Cu의 브레이징)

  • Huh, D.;Kim, D.H.;Chun, B.S.
    • Journal of Welding and Joining
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    • v.13 no.3
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    • pp.134-146
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    • 1995
  • Aluminium nitride(AlN) is currently under investigation as potential candidate for replacing alumium oxide(Al$_{2}$ $O_{3}$) as a substrate material for for electronic circuit packaging. Brazing of aluminium nitride(AlN) to Cu with Ag base active alloy containing Ti has been investigated in vacuum. Binary Ag$_{98}$ $Ti_{2}$(AT) and ternary At-1wt.%Al(ATA), AT-1wt.%Ni(ATN), AT-1wt.% Mn(ATM) alloys showed good wettability to AlN and led to the development of strong bond between brate alloy and AlN ceramic. The reaction between AlN and the melted brazing alloys resulted in the formation of continuous TiN layers at the AlN side iterface. This reaction layer was found to increase by increase by increasing brazing time and temperature for all filler metals. The bond strength, measured by 4-point bend test, was increased with bonding temperature and showed maximum value and then decreased with temperature. It might be concluded that optimum thickness of the reaction layer was existed for maximum bond strength. The joint brazed at 900.deg.C for 1800sec using binary AT alloy fractured at the maximum load of 35kgf which is the highest value measured in this work. The failure of this joint was initiated at the interface between AlN and TiN layer and then proceeded alternately through the interior of the reaction layer and AlN ceramic itself.

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A Study on the Prediction Model of Shear Strength of RC Beams Strengthened for Shear by FRP (섬유보강재로 전단보강된 RC보의 전단강도예측을 위한 해석모델에 대한 연구)

  • 심종성;오홍섭;유재명
    • Journal of the Korea Concrete Institute
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    • v.12 no.5
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    • pp.35-46
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    • 2000
  • In this paper, an analytical model is proposed to predict the shear strenth of RC beams strengthened by FRP. This predictional model is composed of two basic models-the upper bound theorem for shear failure (shear tension or shear compression criteria) and a truss model based on the lower bound theorem for diagonal tension creteria. Also, a simple flexural theory based on USD is used to explain flexural failure. The major cause of destruction of RC beams shear strengthened by FRP does not lie in FRP fracture but in the loss of load capacity incurred by rip-off failure of shear strengthening material. Since interfacial shear stree between base concrete and the FRP is a major variable in rip-off failure mode, it is carefully analyzed to derive the shear strengthening effect of FRP. The ultimate shear strength and failure mode of RC beams, using different strengthening methods, estimated in this predictional model is then compared with the result derived from destruction experiment of RC beams shear strengthened using FRP. To verify the accuracy and consistency of the analysis, the estimated results using the predictional model are compared with various other experimental results and data from previous publications. The result of this comparative analysis showed that the estimates from the predictional model are in consistency with the experimental results. Therefore, the proposed shear strength predictional model is found to predict with relative accuracy the shear strength and failure mode of RC beams shear strengthened by FRP regardless of strengthening method variable.

A design of silicon based vertical interconnect for 3D MEMS devices under the consideration of thermal stress (3D MEMS 소자에 적합한 열적 응력을 고려한 수직 접속 구조의 설계)

  • Jeong, Jin-Woo;Kim, Hyeon-Cheol;Chun, Kuk-Jin
    • Journal of the Institute of Electronics Engineers of Korea SD
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    • v.45 no.2
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    • pp.112-117
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    • 2008
  • Vertical interconnection scheme using novel silicon-through-via for 3D MEMS devices or stacked package is proposed and fabricated to demonstrate its feasibility. The suggested silicon-through-via replaces electroplated copper, which is used as an interconnecting material in conventional through-via, with doped silicon. Adoption of doped silicon instead of metal eliminates thermal-mismatch-induced stress, which can make troubles in high temperature MEMS processes, such as wafer bonding and LP-CVD(low pressure chemical vapor deposition). Two silicon layers of $30{\mu}m$ thickness are stacked on the substrate. The through-via arrays with spacing $40{\mu}m$ and $50{\mu}m$ are fabricated successfully. Electrical characteristics of the through-via are measured and analyzed. The measured resistance of the silicon-through-via is $169.9\Omega$.