• Title/Summary/Keyword: bonding agent

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A STUDY OF THE DURABILITY OF DENTINAL TUBULE SEALING EFFECTS OF DENTIN BONDING AGENTS (상아질 접착제의 상아세관 밀봉지속효과에 관한 연구)

  • Kim, Eui-Seong;Park, Dong-Soo
    • Restorative Dentistry and Endodontics
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    • v.19 no.1
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    • pp.180-193
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    • 1994
  • The purpose of this study was to observe the sealing ability and durability of All-Bond 2, Gluma Bonding System, Scotch bond 2 and Superbond D-liner which are dentin bonding agents used as desensitizing agents. The durability of the sealing ability of the materials were compared after 0, 140, 420, 840 tooth brushing strokes. 120 extracted teeth were divided into 5 groups and the agents were applied to the exposed dentin. No agents was applied on group I, the control group. Each specimen went through thermocycling from $5^{\circ}$ to $55^{\circ}C$, 200 times. Each group was devide into 4 subgroups and artificial tooth brushing strokes were done for 0, 140, 420, 840 times. Finally the specimens were stored in 0.5 % methylene blue solution for 24 hours in a incubator set at $37^{\circ}C$. The tooth were sectioned perpendicular to the long axis and the dye penetration ratio to the pulp was measured. The following results were obtained. 1. All four dentin bonding agents initially showed excellent sealing ability. 2. All-bond 2, Gluma Bonding System and Superbond D-liner showed durability of dentinal tubule sealing effect after 840 strokes(6-week) artificial tooth brushing. 3. Scotchbond 2 showed a significant decrease in sealing ability after 420 strokes(3-week) artificial tooth brushing. (P<0.05).

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A STUDY OF SEALING ABILITY OF DENTIN BONDING AGENT AS ROOT CANAL SEALER (Dentin Bonding Agent의 근관폐쇄(根管閉鎖) 효과(效果)에 관(關)한 실험적(實驗的) 연구(硏究))

  • Min, Hyo-Kie;Min, Byung-Soon;Choi, Ho-Young;Park, Sang-Jin
    • Restorative Dentistry and Endodontics
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    • v.13 no.1
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    • pp.103-111
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    • 1988
  • The purpose of this study was to, examine the sealing ability of the denting bonding agent, when used with gutta percha cone, as a root canal sealer. Seventy two upper and lower extracted human teeth with single root were randomly selected and instrumented in a conventional method with K-file. After instrumentation and dry the canal with paper point, there were divided into three groups and twenty four teeth in each group were filled with the following material; In group I: Scotchbond in combination with gutta percha cone. In group II: AH 26 in combination with gutta percha cone. In group III: Tubli-Seal in combination with gutta percha cone. All specimens were immersed in Indian Ink, decalcified, and cleared. The depth of dye penetration into the canals were evaluated by caliper at the intervals of 1 day, 1 week, 2 weeks. The results were as follows; 1. Depth of dye penetration for all groups increased with time. 2. As to difference in mean dye penetration at time interval of 1 day and 14 days, Scotchbond group exhibited the smallest value as 0.53mm and Tubli-Seal group exhibited the largest value as 0.70mm. 3. There was the difference of dye penetration between each group, but its difference was not significant, statistically.

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Handsheet Property Changes by Internal Addition of Surface Strength Agent (표면강도 향상제 내첨에 따른 수초지 특성 변화)

  • Lim, Jong-Hyck;Jung, Chul-Hun;Chae, Hee-Jae;Park, Chang-Soon;Park, Jong-Moon
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.42 no.2
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    • pp.41-45
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    • 2010
  • This study was performed to evaluate the effect of paper property changes by internal addition of surface strength agent on printability. Advances in printing technique has required the development of paper qualities in many aspects. Basically paper structure is composed of hydrogen bonds which induce many problems in high speed printing machine because of weak bonding strength. One of the important printing problems is surface picking when mechanical pulp or recycled pulp are used. It was caused by the ink-stained blanket in printing process because accumulations of pollutant in white water and other elements which are bonded weakly or do not have hydrogen bonds. Debris at paper surface adheres to blanket which deteriorates printing efficiency and causes various problems. To complement these problems, Pennocel 5137 of polysaccharide structure was used as an agent to improve paper's surface property, strength and printability. Paper surface picking was analyzed by RI-1 test. As the dosage amount increased tensile strength, fiber bonding strength and ZDT strength were improved. Further more formation, smoothness and surface picking resistance were improved. It was confirmed that when adding polysaccharide structure polymers to improve surface strength such as surface picking resistance, it was also possible to improve tensile strength, fiber bonding strength, formation and smoothness.

The influence of hemostatic agent contamination on bond strengths on dentin bonding agents (지혈제가 상아질과 레진 결합력에 미치는 영향)

  • Cho, Jeong-Hyun;Lee, Eun-Jeong;So, Kyung-Mo;Kim, Won;Oh, Nam-Sik;Han, Sang-Hyun;Song, Kyung-Hwa
    • The Journal of Korean Academy of Prosthodontics
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    • v.46 no.4
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    • pp.351-358
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    • 2008
  • Purpose: This study examined the recovery of the dentin-resin bonding strength, and the difference in the bonding strength after applying pH hemostatic agents at various pH. Materials and methods: Bosmin, Hemodent, Astregedent, and Visine were used as the hemostatic agents in this study. The Bosmin, Hemodent, and Astrigedent hemostatic agents are acidic, and the Visine hemostatic agent is neutral and is used as a decongestant. Ninety human molar teeth were used as the specimen. The teeth were sectioned using a diamond wheel until the dentin was exposed and wet ground by silica paper. The specimens were divided into two groups according to the hemostatic agent used. The specimens were then subdivided into 9 groups according to the application of re etching (R group) or rinsing only (N group). A commonly used resin bonding procedure was used in the control group. The resin bonding procedure was managed dentin using celluloid capsule. In addition, the shear bond strength was measured using an Instron. Results: In general, samples with the applied hemostatic agent, with the exception of Visine, had a slightly weak bond that was similar to the control group. In addition, the rinsing only (N) group had slightly weak bond that was similar to the re etching (R) group. Conclusion: The application of a hemostatic agent on the dentin surface does not affect the shear bond strength after application for a short time. In addition, rinsing only can recover the shear bond strength making other management procedures redundant, particularly re etching.

Evaluation of Microleakage and Penetration Ability of Flowable Resin in Occlusal Fissure (유동성 레진의 교합면 열구내 침투도와 미세누출 평가)

  • Cheong, Hyeran;Im, Sungok;Lee, Sangho;Lee, Nanyoung
    • Journal of the korean academy of Pediatric Dentistry
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    • v.44 no.1
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    • pp.89-98
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    • 2017
  • The aim of this study was to compared the penetration scores and microleakage levels of flowable resin in comparison to resin-based pit and fissure sealant. A total 120 extracted premolars were used and classified with group I (resin-based pit and fissure sealant), group II (flowable resin), group III (bonding agent + flowable resin), IV (fissurotomy + bonding agent + flowable resin) depending on the materials and the application methods. The penetration scores of the group treated with flowable resin following fissurotomy were similar to those of the group treated with resin-based sealant, but higher compared to those of the other groups treated with flowable resin without fissurotomy or bonding agent. The group treated with flowable resin following fissurotomy also exhibited the lowest microleakage levels. The group treated with resin-based sealant and the one treated with a bonding agent prior to the application of flowable resin showed similar microleakage levels. In conclusion, flowable resin may be applied as a pit and fissure sealant, and its application along with fissurotomy could increase the penetration scores.

A STUDY ON THE EFFECTS OF THE TEMPERATURE AND HUMIDITY TO THE TENSILE BOND STRENGTH BETWEEN GLASS-IONOMER CEMENT AND COMPOSITE RESIN (온도 및 습도가 Glass-ionomer cement와 Composite resin의 접착강도에 미치는 변화에 관한 연구)

  • Chung, Inn-Gyo;Min, Byung-Soon
    • Restorative Dentistry and Endodontics
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    • v.16 no.1
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    • pp.60-73
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    • 1991
  • The purpose of this study is to evaluate the effects of etching time, environmental temperature and humidity on the adhesion of composite resin to glass-ionomer cement. Two chemical cure composite resins (Clearfil F II and Microrest AP) and two glass-ionomer cements (Fuji ionomer Type I and KET AC-CEM) were used as the experimental materials. The experiment is performed in 3 stages: The first stage is to bond composite resins to glass-ionomer cements, and the surface was not etched, and etched for 20 seconds, 40 seconds, and 60 seconds. Then specimens are stored in distilled water at $37^{\circ}C$ for 24 hours to measure tensile strength. The second stage is to choose the one group that had the highest tensile strength from the first stage and prepare two experimental groups: One group with composite resin bonded to glass-ionomer cement without etching and bonding agent application and the other with composite resin bonded to glass-ionomer cement with etching but without any bonding agent application. The specimens are stored in distilled water at $37^{\circ}C$ for 24 hours and tensile strength is measured. The third stage is to choose group that had the highest tensile strength from the first stage experiment, and bond composite resin to glass-ionomer cement at $24^{\circ}C$ 44%, $30^{\circ}C$ 44%, $30^{\circ}C$ 80%, and $32^{\circ}C$ 92%. The storage time of specimens is to bond immediately after storage, then changed to 30 sec., 60 sec., and 120 sec.. Specimens are stored in distilled water at $37^{\circ}C$ for 24 hours and their tensile strength are measured again. The following results were obtained: 1. As the etching time increases, the tensile bond strength between glass-ionomer cement and composite resin increase, and the tensile bond strength is the highest when acid etched for 60 minutes (P < 0.05). 2. After acid etching for 60 minutes, the tensile strength of the group with bonding agent was stronger than that without bonding agent application (P < 0.05). 3. The tensile strength of Clearfil F II was stronger than that of Microrest AP. 4. It was observed that the tensile bond strength is not affected by different storage time with different temperature and humidity. 5. As the humidity was increased, the tensile bond strength between glass-ionomer cement and composite resin decreased (P < 0.05).

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Effects of Resin Compositions and Additives on Gelation Properties and Bonding Characteristics of Urea-Melamine-Formaldehyde resin adhesives (요소·멜라민 수지 접착제의 겔화성 및 접착특성에 미치는 수지조성과 첨가물의 영향)

  • Roh, Jeang-Kwan
    • Journal of the Korean Wood Science and Technology
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    • v.27 no.1
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    • pp.72-78
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    • 1999
  • To accelerate the curing and to improve the bonding properties of urea-melamine-formaldehyde (UMF) resin adhesives for plywood, the effects of resin compositions and additives on gelation time and bonding strength were discussed. The gelation time of UMF resin prepared by simultaneous reaction with urea(U), melamine(M) and formaldehyde(F) at M/U molar ratio 0.2 was shortened as the molar ratio of formaldehyde to urea was increased. However, at F/U molar ratios higher than 2.5, the amounts of free fomaldehyde of resin could not satisfy with KS standard, Therefore, it was difficult to increase the amount of formaldehyde in resin composition for the purpose of fast gelation time. With increasing the molar ratio of melamine to urea(M/U) from 0.3 to 0.6 at constant F/U molar ratio 3.4, the gelation time of UMF resin was slightly decreased, while gradually increased at M/U molar ratio higher than 0.6. The gelation properties of UMF resin and bonding strength of UMF-bonded plywood could be enhanced by using ammonium chloride and p-toluene sulfonic acid as a curing-agent together with wheat flour and corngluten powder as a extender.

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Studies on Bonding Characteristics of Plywood by Kraft Black Liquor and Surface Activators (크라프트펄프 폐액(廢液)과 표면산화제(表面酸化劑)를 이용(利用)한 합판(合板)의 접착특성(接着特性)에 관(關)한 연구(硏究))

  • Chung, In-Ju;Lee, Phil-Woo
    • Journal of the Korean Wood Science and Technology
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    • v.16 no.3
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    • pp.5-16
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    • 1988
  • This experiment was executed to investigate the effect of activation of veneer surface by oxidizing agents, hydrogen peroxide and nitric acid, on bonding characteristics of Malas(Homalium foetidum Benth) plywood, in which the effects of these oxidizing agents amount, pretreatment time, and pressing time and temperatue on shear strength of the plywood were examined and discussed. In this research the activation of veneer surface by oxidants was effective in raising shear strength but the difference in shear strength was not observed between hydrogen peroxide and nitric acid treatment. Hydrogen peroxide treatment, however, seemed to be more profitable to industrial application because of its lower concentration and easier handling than nitric acid. The bonding method by lignin-phenol adhesive through surface activation revealed inferior shear strength to phenol- and urea-formaldehyde adhesive but superior water resistance to urea-formaldehyde adhesive and this bonding method, in addition, have the advantage of lower cost compared with phenol-formaldehyde adhesive, Therefore, this bonding method by lignin-phenol adhesive through surface activation seemed to economical in manufacturing of water-resistant wood panel materials in future.

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