• Title/Summary/Keyword: bond failure surface

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THE EFFECT OF $CO_2$ LASER IRRADIATION ON ENAMEL SURFACE AND THE BOND STRENGTH OF SEALANT MATERIAL (탄산가스 레이저 조사가 법랑질 표면구조와 치면열구 전색재의 결합강도에 미치는 효과)

  • Yun, Dong-Sik;Kim, Yong-Kee;Kim, Jong-Soo
    • Journal of the korean academy of Pediatric Dentistry
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    • v.25 no.4
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    • pp.761-771
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    • 1998
  • In this study, attempt has been made to evaluate the effect of $CO_2$ laser irradiation on enamel surface structure and the bond strength of sealant material. Conventional acid etching was used as a control technic for comparison. The results obtained from this experiment were as follows; 1. The highest mean shear bond strength value was observed in samples of Group I (acid-etching) with the statistical significance(p<.05) between all the other groups. 2. The shear bond strength in Group IV was the lowest among laser etching groups. but there were no significant difference between them(p>.05). 3. Scanning electron microscopic observation showed that the rough and irregular surface was created by $CO_2$ laser treatment with the formation of numerous pores, micro-cracks, and small bubble-like inclusion. Increasing the energy density induced localized surface melt with a thin smooth glaze-like appearance. 4. In acid-etched control specimen cohesive failure predominated, whereas adhesive failure was the main mode in laser-treated group. Based upon the above-mentioned results, it can be assumed that the $CO_2$ laser is not an adequate substitute for the acid-etch technique in enamel preconditioning. More studies are required to explore the effective condition of laser irradiation which could attain the better bond strength of restorative materials.

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A STUDY OF SHEAR BOND STRENGTH AND SURFACE CONDITION BETWEEN SURFACE TREATED PORCELAIN AND RESIN CEMENT (도재의 표면처리에 따른 레진시멘트와의 전단결합강도 및 표면상태에 관한 연구)

  • Park, Sang-Hyuck;Park, Sang-Jin
    • Restorative Dentistry and Endodontics
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    • v.22 no.1
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    • pp.144-155
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    • 1997
  • This study evaluated shear bond strength between porcelain and resin cement according to various surface treatments of porcelain, and surface condition of debonded porcelain. 50 porcelain specimens(Celay block A2M7) and composite resin specimens(Clearfil Photo-Bright) were prepared, and divided into 5 experimental groups according to the treatment method of porcelain surface. 5 experimental groups by surface treatments were as follows; CONTROL Group : No surface treatment was done on the surface of porcelains. SAND Group : The surface of porcelains were sandblasted with $50{\mu}m$ aluminum oxide for 5 seconds. HF Group: The surface of porcelains were etched with 8% Hydrofluoric acid for 4 minutes. SIL Group: The surface of porcelains were coated with silane coupling agent and heated at $100^{\circ}C$ for 5 minutes. SAND+HF+SIL Group : The surface of porcelains were sandblasted with $50{\mu}m$ aluminum oxide for 5 seconds and etched with 8% Hydrofluoric acid for 4 minutes, and coated with silane coupling agent and heated at $100^{\circ}C$ for 5 minutes. After surface treatments on the prepared porcelain surface two pastes of Panavia 21$^{(R)}$ were mixed, they were applied between composite resin block and porcelain surface, and then excessive resin cements were removed, and its margin was surrounded with Oxyguard II. All specimens were stored for 24 hours in water at $37^{\circ}C$ and tested with Instron testing machine between porcelains and resin cements, and debonded porcelain surfaces were observed under Scanning Electon Microscope(Hitachi S-2300) at 20kvp. The values from each group were compared statistically by Student's t-test. The obtained results were as follows; 1. The shear bond strength without surface treatment of porcelain was the lowest among all experimental groups(p<0.05). 2. The detached porcelain surface with sandblasting alone had more remarkable cracks than with only Hydrofluoric Acid or Silane coupling 2gent, but showed the lowest value of shear bond strength among surface treated groups(p<0.05), 3. When porcelain surface was treated by hydrofluoric acid, it affected shear bond strength more than silane coupling agent, but there were no significant statistical differences(p>0.05). 4. When three methods were combined to increase shear bond strength between porcelains and resin cements, its value was the highest than the others(p<0.05). 5. In Scannig Electron Micrograph of detached porcelain surface with no treatment, the sample revealed adhesive failure between the porcelain and resin cement whereas detached porcelain surface with combination of three method cohesive failure on the porcelain.

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Shear bond strength between CAD/CAM denture base resin and denture artificial teeth when bonded with resin cement

  • Han, Sang Yeon;Moon, Yun-Hee;Lee, Jonghyuk
    • The Journal of Advanced Prosthodontics
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    • v.12 no.5
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    • pp.251-258
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    • 2020
  • PURPOSE. The bond strengths between resin denture teeth with various compositions and denture base resins including conventional and CAD/CAM purposed materials were evaluated to find influence of each material. MATERIALS AND METHODS. Cylindrical rods (6.0 mm diameter × 8.0 mm length) prepared from pre-polymerized CAD/CAM denture base resin blocks (PMMA Block-pink; Huge Dental Material, Vipi Block-Pink; Vipi Industria) were bonded to the basal surface of resin teeth from three different companies (VITA MFT®; VITA Zahnfabrik, Endura Posterio®; SHOFU Dental, Duracross Physio®; Nissin Dental Products Inc.) using resin cement (Super-Bond C&B; SUN MEDICAL). As a control group, rods from a conventional heat-polymerizing denture base resin (Vertex™ Rapid Simplified; Vertex-Dental B.V. Co.) were attached to the resin teeth using the conventional flasking and curing method. Furthermore, the effect of air abrasion was studied with the highly cross-linked resin teeth (VITA MFT®) groups. The shear bond strengths were measured, and then the fractured surfaces were examined to analyze the mode of failure. RESULTS. The shear bond strengths of the conventional heat-polymerizing PMMA denture resin group and the CAD/CAM denture base resin groups were similar. Air abrasion to VITA MFT® did not improve shear bond strengths. Interfacial failure was the dominant cause of failure for all specimens. CONCLUSION. Shear bond strengths of CAD/CAM denture base materials and resin denture teeth using resin cement are comparable to those of conventional methods.

Evaluation of Bond Performance for AC overlay on PCC Pavement (AC / PCC 복합포장 경계면 재료의 부착 성능 평가)

  • Kim, Dong kyu;Hwang, Hyun sik;Christopher, Jabonero;Ryu, Sung woo;Cho, Yoon ho
    • International Journal of Highway Engineering
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    • v.18 no.5
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    • pp.1-9
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    • 2016
  • PURPOSES : This study focuses on the evaluation of interface performance with varying surface texture and tack coat application in an asphalt overlay. METHODS : The evaluation is carried out in two phases: tracking test and interface bond strength test. Using an image processing tool, tracking test is conducted to evaluate the susceptibility of the tack coat material to produce excessive tracking during application. Using the pull-off test method, the bond strength test is performed to determine the ability of the interface layer to resist failure. RESULTS : Results show that the underseal application yields less tracking compared to other applications. However, the bond strength is barely within the minimum acceptable value. On the other hand, RSC-4 produces higher bond strength for all surface types, but the drying time is long, which produces excessive tracking. CONCLUSIONS : While underseal application may be suitable for a trackless condition, the bond strength is less appealing compared to the rest of the tack applications available. RSC-4 demonstrated a high and consistent bond strength performance, but more time is required for drying to avoid excessive tracking. Tack coat application and surface type combination produce varying results. Therefore, these should be considered when selecting suitable future tack coat application options.

Probabilistic analysis of anisotropic rock slope with reinforcement measures

  • Zoran Berisavljevic;Dusan Berisavljevic;Milos Marjanovic;Svetlana Melentijevic
    • Geomechanics and Engineering
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    • v.34 no.3
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    • pp.285-301
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    • 2023
  • During the construction of E75 highway through Grdelica gorge in Serbia, a major failure occurred in the zone of reinforced rock slope. Excavation was performed in highly anisotropic Paleozoic schist rock formation. The reinforcement consisted of the two rows of micropile wall with pre-stressed anchors. Forces in anchors were monitored with load cells while benchmarks were installed for superficial displacement measurements. The aim of the study is to investigate possible causes of instability considering different probability distributions of the strength of discontinuities and anchor bond strength by applying different optimization techniques for finding the critical failure surface. Even though the deterministic safety factor value is close to unity, the probability of failure is governed by variability of shear strength of anisotropic planes and optimization method used for locating the critical sliding surface. The Cuckoo search technique produces higher failure probabilities compared to the others. Depending on the assigned statistical distribution of input parameters, various performance functions of the factor of safety are obtained. The probability of failure is insensitive to the variation of bond strength. Different sampling techniques should yield similar results considering that the sufficient number of safety factor evaluations is chosen to achieve converged solution.

COMPARISON OF THE SHEAR BOND STRENGTH OF GLASS IONOMER CEMENTS AND COMPOMER ACCORDING TO DENTIN SURFACE TREATMENT (상아질표면처리에 따른 글래스아이오노머 및 Compomer의 전단결합강도의 비교)

  • Jeong, Hyun-Suk;Lee, Hea-Joo;Hur, Buck
    • Restorative Dentistry and Endodontics
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    • v.24 no.2
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    • pp.416-425
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    • 1999
  • The purpose of this study was to evaluate shear bond strength of glass ionomer cements and compomer according to dentin surface treatment method. The materials used in this study were dentin conditioner and cavity conditioner for dentin treatment: Ketacfil, Fuji II LC, and Dyract for restoration. In this study, 90 sound bovine teeth were selected and then the teeth were embeded in improved stone and were grounded with 400 to 600 grit silicon carbide paper to create a flat dentin surfaces. The teeth were divided into nine groups as follows ; Group 1A : Samples bonded to dentin surface with Ketacfil after no treatment Group 1B : Samples bonded to dentin surface with Ketacfil after applicating dentin conditioner Group 1C : Samples bonded to dentin surface with Ketacfil after applicating cavity conditioner Group 2A : Samples bonded to dentin surface with Fuji II LC after no treatment Group 2B : Samples bonded to dentin surface with Fuji II LC after applicating dentin conditioner Group 2C : Samples bonded to dentin surface with Fuji II LC after applicating cavity conditioner Group 3A : Samples bonded to dentin surface with Dyract after no treatment Group 3B : Samples bonded to dentin surface with Dyract after applicating dentin conditioner Group 3C : Samples bonded to dentin surface with Dyract after applicating cavity conditioner Treated dentin surfaces were observed under SEM. After filling of each materials, shear bond strenth was evaluated and then debonded surfaces were observed under SEM. The following results were obtained; 1. The shear bond strengths obtained were decreased as Fuji II LC, Dyract, Ketacfil in that order and there was statistically significant difference(p<0.05). 2. About Group 1. the shear bond strengths were decreased as 1C, 1B and 1A in that order. But there was no significant difference between group 1B and 1C (p<0.05). 3. About Group 2, the shear bond strengths were decreased as group 2B, 2A and 2C in that order. And there was significant difference between group 2B and 2C (p<0.05). 4. About Group 3, the shear bond strengths were decreased as group 3A, 3C and 3B in that order. And there was signicant difference between group 3A and 3B (p<0.05). 5. As a result of observation under SEM, the fracture patterns of Fuji II LC and Dyract were adhesive failures, but those of Ketacfil were cohesive failure of material and mixture of cohesive and adhesive failure.

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An Evaluation on High Temperature Oxidation Resistance of EB-PVD Thermal Barrier Coatings (전자빔 증착법에 의한 열차폐코팅의 고온 내산화성 평가)

  • Kim, Jong-H.;Jeong, Se-I.;Lee, Ku-H.;Lee, Eui-Y.
    • Journal of Surface Science and Engineering
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    • v.39 no.4
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    • pp.147-152
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    • 2006
  • Failure mechanisms of electron beam physical vapor deposited thermal barrier coatings(EB-PVD TBCs) that occur during thermal cyclic oxidation were investigated. The investigations include microstructural degradation of NiCrAIY bond coat, thermally grown oxides(TGOs) along the ceramic top coat-substrate interface and fracture path within TBCs. The microstructural degradation of the bond coat during cyclic oxidation created Al depleted zones, resulting in reduction of NiAl and ${\gamma}$-Ni solid solution phase. It was observed that the fracture took placed primarily within the TGOs or at the interfaces between TGOs and bond coat.

THE EFFECT OF ADHESIVE PROPERTY ON MICROTENSILE BOND STRENGTH TO HUMAN DENTIN (상아질 접착제의 성상이 미세인장결합강도에 미치는 영향)

  • Kim, Hyoun-Jin;Hur, Bock;Kim, Hyun-Cheol
    • Restorative Dentistry and Endodontics
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    • v.29 no.3
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    • pp.281-287
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    • 2004
  • The purposes of this study were to evaluate the effect of adhesive property on microtensile bond strength and to determine the failure mode. Flat occlusal dentin surfaces were prepared using low-speed diamond saw. The dentin was etched with 37% phosphoric acid. The following adhesives were applied to the etched dentin to manufacturer's directions: Scotchbond Multi-Purpose in group SM, Prime&Bond NT in group NT, Scotchbond Multi-Purpose followed by Tetric-flow in group TR. After adhesive application, a cylinder of resin-based composite was built up on the occlusal surface. Each tooth was sectioned vertically to obtain the $1{\;}{\times}{\;}1\textrm{mm}^2$ "sticks". Microtensile bond strength were determined. Each specimen was observed under stereomicroscope and scanning electron microscope (SEM) to examine the failure mode. Data were analyzed using one way ANOVA. The results of this study were as follows:1. The microtensile bond strength value were:group SM ($18.98{\pm}3.01MPa$). group NT ($16.01{\pm}4.82MPa$) and group TR ($17.56{\pm}3.22MPa$). No significant statistical differences were observed among the groups (P>0.05). 2. Most of specimens showed mixed failure. In group TR, there was a higher number of specimens showing areas of cohesive failure in resin.

Shear bond strength of indirect composite material to monolithic zirconia

  • Sari, Fatih;Secilmis, Asli;Simsek, Irfan;Ozsevik, Semih
    • The Journal of Advanced Prosthodontics
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    • v.8 no.4
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    • pp.267-274
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    • 2016
  • PURPOSE. This study aimed to evaluate the effect of surface treatments on bond strength of indirect composite material (Tescera Indirect Composite System) to monolithic zirconia (inCoris TZI). MATERIALS AND METHODS. Partially stabilized monolithic zirconia blocks were cut into with 2.0 mm thickness. Sintered zirconia specimens were divided into different surface treatment groups: no treatment (control), sandblasting, glaze layer & hydrofluoric acid application, and sandblasting + glaze layer & hydrofluoric acid application. The indirect composite material was applied to the surface of the monolithic zirconia specimens. Shear bond strength value of each specimen was evaluated after thermocycling. The fractured surface of each specimen was examined with a stereomicroscope and a scanning electron microscope to assess the failure types. The data were analyzed using one-way analysis of variance (ANOVA) and Tukey LSD tests (${\alpha}$=.05). RESULTS. Bond strength was significantly lower in untreated specimens than in sandblasted specimens (P<.05). No difference between the glaze layer and hydrofluoric acid application treated groups were observed. However, bond strength for these groups were significantly higher as compared with the other two groups (P<.05). CONCLUSION. Combined use of glaze layer & hydrofluoric acid application and silanization are reliable for strong and durable bonding between indirect composite material and monolithic zirconia.

Analysis on the Interfacial Bond-Slip Relationship between ear Surface-Mounted FRP Plate and Concrete (콘크리트내 표면매입 보강된 FRP 판과 콘크리트 사이의 착-미끄러짐 관계 해석)

  • Seo, Soo-Yeon
    • Journal of the Korea Concrete Institute
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    • v.26 no.1
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    • pp.79-86
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    • 2014
  • In this paper, a stress transfer mechanism between near surface-mounted (NSM) fiber reinforced polymer (FRP) plate and concrete was investigated and a reliable analytical procedure for it was presented by using bilinear bond-slip model simulating the bond behavior of NSM FRP plate. As a result, critical values in the bi-linear model such as maximum shear strength, slip at that time and failure slip at the initiation of softening de-bonding were suggested for being used in the differential equation considering he interfacial characteristic between NSM FRP and concrete. Also, it was found that the bond-slip behavior could be suitably redicted by using the proposed procedure even in the case of various bond lengths from the comparison with bond test result.