• Title/Summary/Keyword: base-metal

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Brazing of Aluminium Nitride(AlN) to Copper with Ag-based Active Filler Metals (은(Ag)계 활성금속을 사용한 질화 알미늄(AlN)과 Cu의 브레이징)

  • Huh, D.;Kim, D.H.;Chun, B.S.
    • Journal of Welding and Joining
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    • v.13 no.3
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    • pp.134-146
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    • 1995
  • Aluminium nitride(AlN) is currently under investigation as potential candidate for replacing alumium oxide(Al$_{2}$ $O_{3}$) as a substrate material for for electronic circuit packaging. Brazing of aluminium nitride(AlN) to Cu with Ag base active alloy containing Ti has been investigated in vacuum. Binary Ag$_{98}$ $Ti_{2}$(AT) and ternary At-1wt.%Al(ATA), AT-1wt.%Ni(ATN), AT-1wt.% Mn(ATM) alloys showed good wettability to AlN and led to the development of strong bond between brate alloy and AlN ceramic. The reaction between AlN and the melted brazing alloys resulted in the formation of continuous TiN layers at the AlN side iterface. This reaction layer was found to increase by increase by increasing brazing time and temperature for all filler metals. The bond strength, measured by 4-point bend test, was increased with bonding temperature and showed maximum value and then decreased with temperature. It might be concluded that optimum thickness of the reaction layer was existed for maximum bond strength. The joint brazed at 900.deg.C for 1800sec using binary AT alloy fractured at the maximum load of 35kgf which is the highest value measured in this work. The failure of this joint was initiated at the interface between AlN and TiN layer and then proceeded alternately through the interior of the reaction layer and AlN ceramic itself.

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A Study on the Behavior Characteristics of Residual Stress of the Thin Butt Weldment by Mechanical Tensioning Method (인장법에 의한 박판 판계 용접부의 잔류 응력 거동 특성에 관한 연구)

  • Kim, Ha-Keun;Kim, Kyung-Ku;Shin, Sang-Beom
    • Proceedings of the KWS Conference
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    • 2010.05a
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    • pp.57-57
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    • 2010
  • For thin panel welded structure, the various welding distortions were found due to the low resistance against welding deformation. Especially, buckling distortion induced in the thin panel welded structure produce severe problems related to cost in production stage and safety in service life. So, many researches including mechanical and thermal tensioning method for preventing the occurrence of buckling distortion in the production stage have been performed. The purpose of this study is to identify the behavior of longitudinal residual stress at the SA butt weldment with thin plate of 6mm thickness under tension load by 3 dimensional FEA. For it, mesh design for 3D FEA was constructed with 20 nodes brick element for butt weldment and 8 nodes shell element for base metal. According to FEA results, the longitudinal compressive strain inducing tensile residual stress at the butt weldment decreased. It was because the compressive thermal strain in way of weldment was reduced by tension load. The control effect of residual stress increased with an increase in tension load. So, if the amount of tension load applied to the weldment exceeds 1.5 times of longitudinal shrinkage force, the amount of longitudinal residual stress decreased below the critical value inducing the buckling distortion at the SA butt weldment. Its validity was verified by experiment.

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Mechanical Behavior of Weldbond Joint of 1.2GPa Grade Ultra High Strength TRIP Steel for Car Body Applications (차체용 1.2GPa급 초고장력 TRIP강의 Weldbond 접합부의 기계적 거동)

  • Lee, Jong-Dae;Lee, So-Jeong;Bang, Jung-Hwan;Kim, Dong-Cheol;Kang, Mun-Jin;Kim, Mok-Soon;Kim, Jun-Ki
    • Journal of Welding and Joining
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    • v.32 no.5
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    • pp.44-49
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    • 2014
  • The effect of weldbond hybrid joining process on the mechanical behavior of single lap and L-tensile joints was investigated for the newly developed 1.2GPa grade ultra high strength TRIP(transformation induced plasticity) steel. In the case of single lap shear behavior, the weldbond joint of 1.2GPa TRIP steel showed lower maximum tensile load and elongation than that of the adhesive bonding only. It was considered to be due to the reduction of real adhesion area, which was caused by the degradation of adhesive near the spot weld, and the brittle fracture behavior of the spot weld joint. In the case of L-tensile behavior, however, the maximum tensile load of the weldbond joint of 1.2GPa TRIP steel was dramatically increased and the fracture mode was change to the base metal fracture which is desirable for the spot weld joint. These synergic effect of the weldbond hybrid joining process in 1.2GPa TRIP steel was considered to be due to the stress dissipation around the spot weld joint by the presence of adhesive which resulted in the change of crack propagation path.

Fatigue Strength For The Butt Welded Joint Of High Strength Steel (고강도강(高强度鋼) 맞대기 용접연결부(鎔接連結部)의 피로강도(疲勞强度))

  • Kim, Sung Hoon;Bae, Doo Byong;Kim, Myeong Kwan
    • Journal of Korean Society of Steel Construction
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    • v.14 no.2
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    • pp.385-394
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    • 2002
  • Currently, high strength steel is not used for steel bridges in Korea, except for the SM570 high strength steel in very isolated cases. The study aimed to promote the active adaptation of high strength steel for long-span steel bridges. Thus, the fatigue behavior of SM570 and POSTEN80 high strength steel was investigated. For the experimental study, the butt welded joints samples were manufactured. Likewise, regular amplitude tensile fatigue tests were conducted. Test results, e.g., location of fatigue cracks and their propagation were compared with the findings of other researchers. After analyzing the effects of fatigue strength, e.g., static tensile strength and plate thickness of base metal, basic data for fatigue design criteria of SM570 and POSTEN80 high strength steel were presented.

DC/RF Magnetron Sputtering deposition법에 의한 $TiSi_2$ 박막의 특성연구

  • Lee, Se-Jun;Kim, Du-Soo;Sung, Gyu-Seok;Jung, Woong;Kim, Deuk-Young;Hong, Jong-Sung
    • Proceedings of the Korean Vacuum Society Conference
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    • 1999.07a
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    • pp.163-163
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    • 1999
  • MOSFET, MESFET 그리고 MODFET는 Logic ULSIs, high speed ICs, RF MMICs 등에서 중요한 역할을 하고 있으며, 그것의 gate electrode, contact, interconnect 등의 물질로는 refractory metal을 이용한 CoSi2, MoSi2, TaSi2, PtSi2, TiSi2 등의 효과를 얻어내고 있다. 그중 TiSi2는 비저항이 가장 낮고, 열적 안정도가 좋으며 SAG process가 가능하므로 simpler alignment process, higher transconductance, lower source resistance 등의 장점을 동시에 만족시키고 있다. 최근 소자차원이 scale down 됨에 따라 TiSi2의 silicidation 과정에서 C49 TiSi2 phase(high resistivity, thermally unstable phase, larger grain size, base centered orthorhombic structure)의 출현과 그것을 제거하기 위한 노력이 큰 issue로 떠오르고 있다. 여러 연구 결과에 따르면 PAI(Pre-amorphization zimplantation), HTS(High Temperature Sputtering) process, Mo(Molybedenum) implasntation 등이 C49를 bypass시키고 C54 TiSi2 phase(lowest resistivity, thermally stable phase, smaller grain size, face centered orthorhombic structure)로의 transformation temperature를 줄일 수 있는 가장 효과적인 방법으로 제안되고 있지만, 아직 그 문제가 완전히 해결되지 않은 상태이며 C54 nucleation에 대한 physical mechanism을 밝히진 못하고 있다. 본 연구에서는 증착 시 기판온도의 변화(400~75$0^{\circ}C$)에 따라 silicon 위에 DC/RF magnetron sputtering 방식으로 Ti/Si film을 각각 제작하였다. 제작된 시료는 N2 분위기에서 30~120초 동안 500~85$0^{\circ}C$의 온도변화에 따라 RTA법으로 각각 one step annealing 하였다. 또한 Al을 cosputtering함으로써 Al impurity의 존재에 따른 영향을 동시에 고려해 보았다. 제작된 시료의 분석을 위해 phase transformation을 XRD로, microstructure를 TEM으로, surface topography는 SEM으로, surface microroughness는 AFM으로 측정하였으며 sheet resistance는 4-point probe로 측정하였다. 분석된 결과를 보면, 고온에서 제작된 박막에서의 C54 phase transformation temperature가 감소하는 것이 관측되었으며, Al impuritydmlwhswork 낮은온도에서의 C54 TiSi2 형성을 돕는다는 것을 알 수 있었다. 본 연구에서는 결론적으로, 고온에서 증착된 박막으로부터 열적으로 안정된 phase의 낮은 resistivity를 갖는 C54 TiSi2 형성을 보다 낮은 온도에서 one-step RTA를 통해 얻을 수 있다는 결과와 Al impurity가 존재함으로써 얻어지는 thermal budget의 효과, 그리고 그로부터 기대할 수 있는 여러 장점들을 보고하고자 한다.

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Assessment of Fracture Characteristics of Natural Gas Pipeline Weldment According to the Change of Microstructures (천연가스 배관 용접부의 미세조직의 변화에 따른 파괴특성 평가)

  • Ju Jang-Bog;Lee Jung-Suk;Jang Jae-il;Kim Cheol-man;Kim Woo-sik;Kwon Dongil
    • Journal of the Korean Institute of Gas
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    • v.5 no.3 s.15
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    • pp.15-22
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    • 2001
  • Reliability evaluation of welded structures by mechanical testing of weld heat-affected zones (HAZs) has become general practice throughout the world. HAZs of steel welded Joints show a gradient of microstructure from the fusion line to the unaffected base metal. This study is concerned a correlation between the microstructural change and the fracture characteristics in HAZs of both seam and girth welds of API 5L X65 pipeline steel, which is generally used for natural gas transmission pipelines in Korea. The focus in this study is the investigation of macroscopic fracture behavior of the various regions within HAZ. Changes in microstructure and toughness were observed using actual HAZ specimens. To evaluate the macroscopic toughness of actual HAZ, Charpy V-notch impact test and CTOD test were performed.

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A Study on Comparing Characteristics of Le Corbusier′s Furniture Design with Alvar Aalto′s (르 꼬르뷔지에와 알바 알토의 가구디자인 특성 비교 연구)

  • 이진영
    • Korean Institute of Interior Design Journal
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    • v.13 no.5
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    • pp.162-172
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    • 2004
  • Architects and designers of the 20th Century made various efforts to establish new design languages reflecting the changes of society, the times, and environment. They used furniture, especially chairs, as controversial items of aesthetic value, society and ideology. Le Corbusier and Alvar Aalto are furniture designers as well as architects, who adopted this ‘spirit of the times’ actively and have greatly contributed to modernism. This study will help us to understand the diversity of design since modernism, by comparing these two designers' furniture design. It also covers the common factors In modern furniture design, and analyses their individuality and likeness In design. The following is a comparison of furniture design by Le Corbusier and Alvar Aalto. Le Courbusier linked International design and Aalto linked Rational design and Organic concept design to their furniture, just as they did in their architecture. They were able to establish the base of modern furniture design by adapting new concepts and pursuing humanism. In structure, Le Corbusier's furniture Is simple and proportional. It demonstrates a sophisticated geometric composition, mechanical beauty. On the other hand, Aalto rationally linked nature with human requirements and his furniture is organic and in harmony with geometric structure. In function, Le Corbusier's furniture is standardized and prefabricated. He designed for the user so they could choose to use the furniture efficiently to suit their needs. In comparison with Le Corbusier, Aalto Invented the ‘Stacking Chair’ which allows a more effective use of space and reflected the structure of the human body to improve the user's comfort. In materials and techniques, Le Corbusier used new materials like metal or leather, and attempted new ways such as welding, prefabrication, and standardization for production. On the contrary, Alto mainly used birch, which is the traditional material in Finland, and tried new bent wood techniques and joining methods.

A COMPARATIVE STUDY ON THE FLEXIBILITY OF THE WROUGHT WIRE CLASPS (가공선 크라스프의 가요성에 관한 비교 연구)

  • Eom, Tae-Wan;Chang, Ik-Tae;Kim, Kwang-Nam
    • The Journal of Korean Academy of Prosthodontics
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    • v.27 no.2
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    • pp.261-270
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    • 1989
  • Bend test is one of the methods comparing the physical properties of the clasp wires. The type of bend test used in this investigation was the cantilever loading of a wrought wire. The purpose of this study was to compare the flexibility of a number of commonly used clasp wires, in according to gauge, alloy and heat treatment, under specific condition of load and deflection. Seven noble and one base metal wires were tested under three conditions as follows: (1) as received, (2) quenched (placed in an over at $700^{\circ}C$ for ten minutes and immediately quenched in water at room temperature.), (3) oven cooled (quencned as described, then placed in an oven at $450^{\circ}C$ for two minutes and uniformly slowly cooled to $250^{\circ}C$ in thirty minutes.) The basic test specimen consists of a sample 25 mm in length and 19, 18 gauge in diameter (17 gauge also in two alloys), and the wire was loaded in the form of straight cantilever beams. Force at 0.25 mm (0.01 inch) and 0.5 mm (0.02 inch) deflections for all samples were recorded. The results were as follows ; 1. Ticonium was least flexible and No. 2 was most flexible in according to gauge, alloy and heat treatment. 2. In most of precious wrought wire, the flexibility was increased, but there was no statistically significant differences between as-received and softened condition. 3. There was no statistically differences between as-received and hardened condition. 4. For each alloy, there were statistically significant differences in flexibility due to clasp diameter.

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A Study on the Simplified Estimating Method of Off-site Consequence Analysis by Concentration of Hydrochloric Acid (염산수용액의 농도별 간이 영향 평가 방법 연구)

  • Jung, Y.k.;Kim, B.;Heo, H.;Yoo, B.;Sin, C.;Yoon, Y.;Yoon, J.;Ma, B.
    • Journal of the Korean Society of Safety
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    • v.32 no.2
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    • pp.52-58
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    • 2017
  • One of the most important elements of the management of chemical accident is threat zone estimation of fires, explosions and toxic gas dispersion based on chemical releases. The threat zone estimation is going to be standard of emergency response for the first defender and base line data of off-site risk assesment (hereinafter referred to as "ORA") and risk management plan (hereinafter referred to as "RMP"). Generally, ALOHA form EPA(U.S.) and Kora(from KOREA MINISTRY OF ENVIRONMENT) has been used for the off-site consequence analysis in Korea. However it is hard to predict accurate consequences rapidly in case of emergency. Hydrochloric acid is a multipurpose raw material used in many industrial applications such as chemical, metal and food industries. It is usually treated in concentrations from 10 ~ 35 %, and release accident have occurred frequently. In this study, we have developed a simplified estimating method and equation to calculate threat zone easily in case of emergency due to release accident of hydrochloric acid.

The Effect of Age Heat-treatment to the Electro-Chemical Corrosion Behavior on Ti-6Al-4V (Ti-6Al-4V재의 전기화학적부식 거동에 미치는 시효열처리의 영향)

  • 백신영
    • Journal of Advanced Marine Engineering and Technology
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    • v.24 no.6
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    • pp.70-77
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    • 2000
  • In this paper, the effect of solution and age heat treatment to the corrosion behavior for the Ti-6Al-4V alloy were studied by cyclic polarization methods. Ti-6Al-4V was solution heat treated at $1,066^{\circ}C$ and $966^{\circ}C$ for 5 hours, and followed by age heat treated at $650^{\circ}C$, $600^{\circ}C$ and $550^{\circ}C$ with 1, 2, 4, 8 and 16 hours under vacuum environment. Test solution was 3.5% NaCl with temperature $25^{\circ}C$. The obtained results were as follows: 1. Base metal was exhibited higher electrical charge than that of solution and aged material. With decrease of solution-treatment temperature from 1066 to $966^{\circ}C$, the electrical charge was increased due to softening of micro structure. 2. The corrosion resistance of specimen that solution treated at $966^{\circ}C$ for 5 hours and age heat treated at 650, 660 and $550^{\circ}C$ were increased with increase of aging time to 4, 8 and 16 hours respectively, and then decreased. 3. In case of 316L stainless steel, measured charge and corrosion potential was 0.0627 coulomb and -614 mV respectively. Corrosion resistance of Ti-6Al-4V was higher than that of 316L.

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