• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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• pp.18-19
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• 2006

To improve the properties of fine metal powder, such as particle size distribution and geometric standard deviation, this work was done at various atomizing conditions. The new atomization mechanism and the correlation equation were proposed to estimate the mean particle diameter.

• 한국주조공학회지
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• 제7권2호
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• pp.133-139
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• 1987

The evolution of microstructures in two rapidly solidfied niobium microalloyed steels was studied. These alloys were rapidly solidified by two powder process techniques: nitrogen gas atomization and centrifugal atomization. It was found that in both powder processes, powder particles larger than $20{\mu}m$in diameter were martensitic, and that the nitrogen gas atomized particles solidified cellularly while those that were centrifugally atomized tended to solidify dendritically. Particles smaller than $1{\mu}m$ were not completely characterized because of wide variation in composition.

• 한국분말재료학회지
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• 제16권5호
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• pp.316-325
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• 2009

Fe based (Fe$_{68.2}$C$_{5.9}$Si$_{3.5}$B$_{6.7}$P$_{9.6}$Cr$_{2.1}$Mo$_{2.0}$Al$_{2.0}$) amorphous powder, which is a composition of iron blast cast slag, were produced by a gas atomization process, and sequently mixed with ductile Cu powder by a mechanical ball milling process. The experiment results show that the as-prepared Fe amorphous powders less than 90 $\mu$m in size has a fully amorphous phase and its weight fraction was about 73.7%. The as-atomized amorphous Fe powders had a complete spherical shape with very clean surface. Differential scanning calorimetric results of the as-atomized Fe powders less than 90 $\mu$m showed that the glass transition, T$_g$, onset crystallization, T$_x$, and super-cooled liquid range $\Delta$T=T$_x$-T$_g$ were 512, 548 and 36$^{\circ}C$, respectively. Fe amorphous powders were mixed and deformed well with 10 wt.% Cu by using AGO-2 high energy ball mill under 500 rpm.

• 대한기계학회논문집B
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• 제20권7호
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• pp.2267-2276
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• 1996

공정산업분야 및 분무연소분야에서 많이 사용되고 있는 2유체 분무기에서 출구 초음속유동의 가시화와 하류의 가스압력 측정 결과로부터 다음과 같은 결론을 얻었다. 1) 과소팽창 또는 과대팽창 초음속노즐 유동에서 출구 Mach수가 일정한 경우, 유동이 박리하지 않는다면 가스의 정체압력(유량)이 증가함에 따라 노즐출구에서 충돌정체점까지의 길이와 초음속 유동영역의 길이는 증가한다. 2) 스피팅 현상은 액체공급관 출구의 흡인압력은 분사가스압력이 증가함에 따라 단조증가하지만 분사가스압력이 0.5MPa이상이 되면 증감현상이 커지며 돌출형 노즐에서 유동박리시 급격히 증가한 다음 거의 일정하게 유지된다. 4) 액체공급관 하류축상의 압력변화는 출구의 음압에서 충돌정체점까지 상승한 다음 급강하하고 충격파 세포상의 구조에 따라 진동하면서 대기압에 도달한다.

• 한국분말재료학회지
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• 제23권5호
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• pp.391-396
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• 2016

In this study, ultra-fine soft-magnetic micro-powders are prepared by high-pressure gas atomization of an Fe-based alloy, Fe-Hf-B-Nb-P-C. Spherical powders are successfully obtained by disintegration of the alloy melts under high-pressure He or $N_2$ gas. The mean particle diameter of the obtained powders is $25.7{\mu}m$ and $42.1{\mu}m$ for He and $N_2$ gas, respectively. Their crystallographic structure is confirmed to be amorphous throughout the interior when the particle diameter is less than $45{\mu}m$. The prepared powders show excellent soft magnetic properties with a saturation magnetization of 164.5 emu/g and a coercivity of 9.0 Oe. Finally, a toroidal core is fabricated for measuring the magnetic permeability, and a ${\mu}_r$ of up to 78.5 is obtained. It is strongly believed that soft magnetic powders prepared by gas atomization will be beneficial in the fabrication of high-performance devices, including inductors and motors.

• 한국추진공학회지
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• 제21권5호
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• pp.88-96
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• 2017

재생냉각 기술을 적용한 스크램제트 엔진 개발의 일환으로 스크램제트 엔진에 사용될 공기 보조형 인젝터(Air-assist type injector)에 대한 연구를 수행하였다. 실험에 사용된 인젝터는 주 유동에 대해 $90^{\circ}$와 $60^{\circ}$의 각도로 분출되는 두 종류의 인젝터를 사용하였으며 측정 방법에는 미 산란(Mie-scattering)을 이용한 가시화 측정방법과 PDPA를 이용한 미립화 측정 방법을 사용하였다. 실험 결과, 공급되는 기체의 압력 증가와 노즐로부터의 거리가 증가할수록 더 좋은 미립화 특성을 보였으며 분출각도가 $60^{\circ}$인 인젝터가 $90^{\circ}$의 인젝터보다 더 좋은 미립화 특성을 보였다.

• 한국분무공학회지
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• 제11권2호
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• pp.59-68
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• 2006

Experimental results of the metal powder production with internal mixing, internal impinging and the atomizer coupled with substrate design are presented in this paper. In a test with internal mixing atomizer, mean powder size was decreased from $37{\mu}m\;to\;23{\mu}m$ for Pb65Sn35 alloy as the gas-to-melt mass ratio was increased from 0.04 to 0.17. The particle size further reduces to $16.01{\mu}m$ as the orifice area is increased to $24mm^2$. The micrograph of the metal powder indicates that very fine and spherical metal powder has been produced by this process. In a test program using the internal impinging atomizers, the mean particle size of the metal powder was decreased from $22{\mu}m\;to\;12{\mu}m$ as the gas-to-melt-mass ratio increased from 0.05 to 0.22. The test results of an atomizer coupled with a substrate indicates that the deposition rate of the molten spray on the substrate is controlled by the diameter of the substrate, the height of the substrate ring and the distance of the substrate from the outlet of the atomizer. This in rum determines the powder production rate of the spraying processes. Experimental results indicate that the deposition rate of the spray forming material decreases as the distance between the substrate and the atomizer increases. For example, the deposition rate decreases from 48% to 19% as the substrate is placed at a distance from 20cm to 40cm. On the other hand, the metal powder production rate and its particle size increases as the subsrate is placed far away from the atomizer. The production of metal powder with mean particle size as low as $3.13{\mu}m$ has been achieved, a level which is not achievable by the conventional gas atomization processes.

• 한국수소및신에너지학회논문집
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• 제20권6호
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• pp.505-511
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• 2009

The hydriding and electrochemical characteristics of Zr-based $AB_2$ alloy produced by gas atomization have been extensively examined. For the particle morphology of the as-cast and gas-atomized powders, it can be seen that the mechanically crushed powders are irregular, while the atomized powder particles are spherical. The increase of jet pressure of gas atomization process results in the decrease of hydrogen storage capacity and the slope of plateau pressure significantly increases. TEM and EDS studies showed the increase of jet pressure in the atomization process accelerated the phase separation within grain of the gas-atomized alloy, which brought about a poor hydrogenation property. However, the gas-atomized $AB_2$ alloy powders produced by jet pressure of 50 bar kept up the reversible $H_2$ storage capacity and discharge capacity similar to the mechanically crushed particles. In addition, the electrode of gas-atomized Zr-based $AB_2$ alloy of 50 bar showed improved cyclic stability over that of the cast and crushed particulate, which is attributed to the restriction of crack propagation by grain boundary and dislocation with ch/discharging cycling.

• 태양에너지
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• 제11권3호
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• pp.62-73
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• 1991

본 연구는 주어진 기름노즐의 분무특성을 실험적으로 조사하고 아울러 적정 가동조건을 설정하기 위하여 수행하였다. 실험에 공시한 노즐은 Delalvan과 Hago(압력분무 Simplex 1.25GPH)로서 각종 압력하에서 분무 각 $60^{\circ}$와 $80^{\circ}$에 대하여 조사하고 분무특성을 기술함에 있어서는 사우터 평균입경의 개념을 사용하였다. 포집된 모든 분무입자는 고감도 필름을 사용하여 50배로 확대 촬영하고, 이들을 Nukiyama-Tanazawa의 분포함수를 도입하여 해석하였다. 결론적으로 $80^{\circ}$의 경우가 $60^{\circ}$의 경우보다 분무특성이 양호하며, 적정 가동조건은 분무압 $8kg/cm^2$ 부근에서 정착됨을 알 수 있었다.

• 한국음향학회지
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• 제41권1호
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• pp.9-15
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• 2022

기존의 나노입자 현탁액의 분산과정의 한계를 극복하여 단분산된 나노입자만으로 이루어진 현탁액을 얻기 위하여, 기존의 방법으로 전분산 처리된 현탁액을 다시 초음파 무화효과 및 사이클론을 이용하여 여과하는 방법을 제안하였다. 평균직경 250 nm인 Al₂O₃나노입자로 0.5 wt%인 현탁액을 만들어 초음파세척기 및 호모지나이저를 이용하여 각각 전처리 분산된 현탁액에 대하여 제안한 여과법을 적용하였다. 그 결과 초음파세척기로 전처리 분산한 경우 단분산된 나노입자 현탁액으로 여과하기 위해서는 종속 연결된 사이클론이 3개가 요구되는 반면, 호모저나이저로 전처리 분산된 현탁액의 경우는 2개의 사이클론으로도 가능함을 확인 하였다. 초음파 무화기 주파수의 조정과 사이클론의 설계 변경에 의해 다양한 종류의 나노입자에 대한 여과가 가능할 것으로 기대된다.