For identification and apportionment of sources emitting particulate matters in environment, the multi-elemental characterization of size-density fractionated particulate matters was carried out. Eight types of samples were tested; soil, flyash released from burning of bunker-Coil, diesel oil, coal, and soft coal, urban road-way dust, urban dust fall, and airborne particulate matter. The fractions of particulate matters obtained by heavy liquid separation methos with a series of dichloromethane-bromoform were then analyzed using atomic absorption spectrophotometry for Ni, Cr, Cu, An, Fe, Al, and Mg. Each sample showed a different concentration profile as a function of density, and a number of useful conclusions concerning characterization of elemental distribution were obtained. From the density distributions of elements in soil, the maximum value was found for all elements in the density range of 2.2 ∼2.9g.cm−3∼2.9g.cm−3, including the density of SiO2SiO2. However, the distribution of metallic compounds with the density lower than 2.2g.cm−32.2g.cm−3 was prevalent in urban roadway dust, urban dust fall, and airborne particulate matter. And the density distribution curves of these urban dusts also have the higher distribution at the density of 2.2 - 2.9g.cm^{-3},includingthedensityofwind−blownsilica.Thistendencygenerallywasprevalentinthenaturalsourceelements,suchasAl,Fe,Mn,andMg.Themaximumvalueswerefoundinthedensityrangesof1.3,includingthedensityofwind−blownsilica.Thistendencygenerallywasprevalentinthenaturalsourceelements,suchasAl,Fe,Mn,andMg.Themaximumvalueswerefoundinthedensityrangesof1.3\sim 2.2g.cm^{-3}fromthedensitydistributionofelementsinoilfiredflyash.Thesedistributionsofanthropogenicsourceelements,suchasZn,Ni,Cu,andCrwerehigherpredominatelythanthoseofnaturalsourceelements.Andthehigherdistributionwasfoundinthedensityrangeoffromthedensitydistributionofelementsinoilfiredflyash.Thesedistributionsofanthropogenicsourceelements,suchasZn,Ni,Cu,andCrwerehigherpredominatelythanthoseofnaturalsourceelements.Andthehigherdistributionwasfoundinthedensityrangeof2.2 \sim 2.9g.cm^{-3}fromthedensitydistributionofelementsincoalandsoft−coalfiredflyash.Thesedistributionsshowedsimilarpatternstosoil.Butanthropogenicsourceelementssomewhatpredominatedatthedensityrangesoffromthedensitydistributionofelementsincoalandsoft−coalfiredflyash.Thesedistributionsshowedsimilarpatternstosoil.Butanthropogenicsourceelementssomewhatpredominatedatthedensityrangesof1.3 \sim 2.2g.cm{-3} and 2.9g.cm^{-3}tosoil.Thereforethehigherdistributionofanthropogenicsourceelementsinthedensityrangesoftosoil.Thereforethehigherdistributionofanthropogenicsourceelementsinthedensityrangesof1.3 \sim 2.2g.cm^{-3} and 2.9g.cm^{-3}$ was considered as anthropogenic origin.