• Title/Summary/Keyword: aqueous ethanol

Search Result 466, Processing Time 0.023 seconds

Applying Aqueous Two Phase Systems to Multi-layer Cosmetics (다중 층 화장료에서 수성 이상계의 응용)

  • Hong, Junki;You, Jaewon;Yoo, Jangyung;Nam, Seungok;Lee, Sanggil;Pyo, Hyeongbae
    • Journal of the Society of Cosmetic Scientists of Korea
    • /
    • v.39 no.2
    • /
    • pp.83-88
    • /
    • 2013
  • The aqueous two phase system has biocompatibility, because it is physically separated into an immiscible liquid multi-layer induced by incompatibility among hydrophilic components dissolved in the water phase. we have applied this principle to aqueous multi-layer liquid cosmetics and select two representative systems. What it was experimentally obtained was the phase diagrams including a binodal curve, a critical point, tie lines of concentration and tie curves of phase separating volume ratio and phase separating time. From the phase diagrams, we were able to observe existence of the optimum condition to prepare the aqueous multi-layer cosmetics for the systems.

Determination of Aloesin in Aloe Preparations by HPLC (고속액체크로마토그래피에 의한 알로에 제제 중의 알로에신의 정량)

  • Kim, Kyeong-Ho;Kim, Hyun-Ju;Park, Jeong-Hill;Shin, Young-Geun
    • YAKHAK HOEJI
    • /
    • v.40 no.2
    • /
    • pp.177-182
    • /
    • 1996
  • The contents of aloesin in aloe preparations were determined by HPLC. Aloesin was extracted 3 times with ethanol for 30 minutes. The ethanol extract was concentrated and suspend ed in saturated NaCl aqueous solution and successively partitioned with dichloromethane, n-butanol. Prepared samples were analyzed by HPLC on a reverse column(Inertsil ODS-2). In assay, internal standard was a puerarin and regression of calibration curve was 0.998. Recoveries of aloesin added to aloe preparation were 98~123(%).

  • PDF

Antioxidative Activity of Extrcts from Fruit of Curdrania tricuspidata (꾸지뽕나무 열매 추출물의 항산화 활성)

  • 차재영;조영수
    • Journal of the Korean Society of Food Science and Nutrition
    • /
    • v.30 no.3
    • /
    • pp.547-551
    • /
    • 2001
  • The comparative activities of acetone, ethanol, and aqueous fractions extracted from fruit powder of Cudrania tricuspidata by different temperature were tested by in vitro experimental models; peroxidation of linoleic acid and autooxidation of rat hepatic and renal microsomes by using thiobarbituric acid (TBA) for assay of free malondialdehyde production, and scavenging activities of free radicals by DPPH (α, α'-diphenyl-β-picrylhydrazyl). In DPPH method, acetone fraction extracted at 30℃ showed the highest free radical scavenging activities and acetone fractions extracted at 30℃ and 60℃ and ethanol fraction extracted at 30℃ showed stronger than BHT (butylated hydroxitoluene) although used ten-fold lower concentrations. In thiocyanate method used linoleic acid an inhibitory effects of all fractions showed higher than control treatment. TBA method used linoleic acid showed the highest antioxidative activity in acetone fraction extracted at 30℃ and 60℃. an inhibition activity against lipid peroxidation in hepatic microsomes of rats showed the highest at acetone faction extracted at acetone fraction among extracted fractions was shown to be the most potent antioxidative properties and this action was more potent in fractions extracted at 30℃ than those extracted at 60℃.

  • PDF

Release of Flurbiprofen from Poloxamer 407 Gel

  • Gil, Hyung-Jun;Kim, Hyun;Chi, Sang-Cheol
    • Archives of Pharmacal Research
    • /
    • v.17 no.4
    • /
    • pp.240-243
    • /
    • 1994
  • Release rates of flurbiprofen from transdermal gels made of poloxamer 407 were evaluated using a membraneless diffusion cell in order to study the effects of formulation variables on flurbiprofen release such as poloxamer 407 (17.5-25%) drug (0.1-1.0%), ethanol (10-20%), PG or PEF 300 (5-15%) concentrations and gel pH(3-7). Isopropyl myristate was employed as a receptor medium for the drug released from the gel. The diffusion coefficient of flurbiprofen decreased linearly as the amount of poloxamer 407 and the drug in the gel increased. The release rate of flurbiprofen was gel increased. The The addition of more ethanol in the gel increased the drug release, resulting from the increase of the thermodynamic activity of the drug in the aqueous phase of the gel. However, the concentration effects of PG and PEG 300 on the release rate of flurbiprofen were negligible over the concentration range used.

  • PDF

Reduction of Aromatic Nitro Group by Activated Cu-Zn-$NH_2NH_2{\cdot}H_2O$ in Ethanol (활성화시킨 Cu-Zn 과 히드라진을 이용한 방향족 니트로 화합물의 환원반응)

  • Byung Hee Han;Dae Hyun Shin;Hyun Ro Lee
    • Journal of the Korean Chemical Society
    • /
    • v.33 no.6
    • /
    • pp.577-581
    • /
    • 1989
  • Activated Cu-Zn by the reaction of aqueous cupric sulfate and excess Zn showed the exceptional catalytic activity for the reduction of aromatic nitro compounds to the corresponding amino compounds in the presence of hydrazine monohydrate in ethanol. But, aliphatic nitro compounds were not reduced to the amino compounds.

  • PDF

PHOTOCATALYTIC ISOQUINOLINE PRODUCTION AND N-ALKYLATION BY PLATINIZED TITANIUM(IV) OXIDE PARTICLES SUSPENDED IN ALCOHOLIC SOLUTION OF PHENETHYLAMINES

  • Bunsho Ohtani;Yoshiko Moriguchi;Nishimoto, Sei-Ichi;Tomoyuki Inui
    • Journal of Photoscience
    • /
    • v.1 no.2
    • /
    • pp.107-111
    • /
    • 1994
  • Photocatalytic ($\lambda$$_{ex}$ > 300 nm) reaction at room temperature by platinized titanium (IV) oxide particles produced 1-methyl-1, 2, 3, 4-tetrahydroisoquinolines (MIQ's) from phenethylamines in aqueous ethanol suspension under deaerated atmosphere. Among the phenethylamines, dopamine (2-(3, 4-dihydroxyphenyl) ethylamine) showed the highest reactivity to give MIQ almost selectively under the neutralized conditions. The other phenethylamines gave predominantly N-alkylated and N, N-dialkylated products in the methanol or ethanol solutions. The reaction mechanism includes a Schiff base intermediate to undergo either nucleophilic attack leading to MIQ or reduction to N-alkylated products.

  • PDF

The Antigastritic Effect of Taraxaci Herba (포공영의 항위염 작용)

  • Lee, Eun-Bang;Kim, Jung-Keun;Kim, Ok-Kyung
    • Korean Journal of Pharmacognosy
    • /
    • v.24 no.4
    • /
    • pp.313-318
    • /
    • 1993
  • The methanol extract of Taraxaci Herba was found to have inhibitory effect on the gastric lesion induced by HCl-ethanol. The systematic fractionation of the methanol extract resulted in positive action with water fraction in the gastric lesion. It also showed significant inhibition of gastric lesion induced by HCl-aspirin and absolute ethanol, but did not prevent indomethacin induced gastric lesion. This fraction did not affect basal gastric acid secretion but showed a decrease of pepsin activity in pylorus-ligated rats.

  • PDF

Coordinatively Polymerized Bilayer Membranes Prepared with an Amphiphilic Derivative of 2-Thiazolyazophenol in Water

  • 서정훈;신승훈;심현보
    • Bulletin of the Korean Chemical Society
    • /
    • v.18 no.2
    • /
    • pp.190-193
    • /
    • 1997
  • In search of new amphiphiles that form coordinatively polymerized bilayer membranes (CPBMs) in water, N-dodecyl-3-[2-hydroxy-3-(4-carboxymethyl-2-thiazolylazo)-5-methylphenyl]propanamide (5) was prepared. The bilayer membranes of 5 prepared in the presence of 2 equivalents of NaOH were further sonicated in the presence of transition metal ions such as Ni(Ⅱ), Cu(Ⅱ), Co(Ⅱ), or Co(Ⅲ) at > 80 ℃ to obtain CPBMs. The CPBMs of 5 were characterized by transmission electron microscopy, gel filtration, resistivity against disruption in aqueous ethanol, visible spectra, and release of entrapped 5(6)-carboxyfluorescein. Remarkable stabilization of the bilayer membranes through coordinative polymerization was evidenced by the resistivity of the Ni(Ⅱ)-CPBM of 5 against disruption in 40%(v/v) ethanol upon incubation for 20 hr.

Comparison of sericin produced through laboratory- and plant-scale extraction

  • Ye Eun Kim;Chun Woo Kim;In Chul Um
    • International Journal of Industrial Entomology and Biomaterials
    • /
    • v.47 no.1
    • /
    • pp.63-71
    • /
    • 2023
  • In this study, the structural characteristics of sericin recovered from wastewater released from the silk textile industry (Plant sericin) were comparatively analyzed with those of sericin extracted from a silkworm cocoon produced in a laboratory (Lab sericin). To prepare Plant sericin, ethanol was added to wastewater (i.e., a sericin aqueous solution) after the degumming process to remove nonprotein materials, affording a sericin precipitate. To prepare Lab sericin, nonprotein materials were removed from a silkworm cocoon and sericin was subsequently extracted from the cocoon. Lab sericin and Plant sericin exhibited similar solution viscosities, gel strengths, and crystallinity indices, indicative of the similar molecular weights (MWs) of the two sericin samples. In the case of sericin powder, Plant sericin was more crystalline than Lab sericin due to its treatment with ethanol. The findings of this study revealed that sericin recovered from industrial wastewater can be used equally as its MW is similar to that of sericin obtained through laboratory-scale extraction.

Preparation of Ultrafine Nickel Powders by Wet Reduction Process (습식 환원법에 의한 니켈 미분말의 제조)

  • Lee, Yoon-Bok;Moon, Young-Tae;Shin, Dong-Woo;Kim, Kwang-Ho
    • Korean Journal of Materials Research
    • /
    • v.12 no.10
    • /
    • pp.803-808
    • /
    • 2002
  • Nickel powders were prepared from nickel chloride solution by wet reduction process, and the size control of the particles was investigated with reactant concentration, dispersant agent, and the addition of ethanol as an organic solvent in NiCl$_2$ aqueous solution. The size of the particle decreased with the increase of nickel chloride concentration. Their average particle size were 1.9$\mu\textrm{m}$, 1.6$\mu\textrm{m}$ and $1.5\mu\textrm{m}$ with 0.5M, 0.8M and 1.0M of nickel chloride concentration respectively. The spherical particle was easily controlled by the addition of ethanol as an organic solvent. Especially, in 30 vol% of ethanol, the average particle size and specific surface area were about 0.2$\mu\textrm{m}$ and 8.98m$^2$/g, respectively.