• Title/Summary/Keyword: analytical values

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Analytical assessment of elevated tank natural period considering soil effects

  • Maedeh, Pouyan Abbasi;Ghanbari, Ali;Wu, Wei
    • Coupled systems mechanics
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    • 제5권3호
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    • pp.223-234
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    • 2016
  • The main purpose of current study is to find the soil effects on natural period of elevated tank. The coupled analytical method is used to assess in this study. The current study presented models which are capable to consider the soil dynamic stiffness changes and fluid- structure interaction effects on natural period of elevated tanks. The basic of mentioned models is extracted from elastic beam and lumped mass theory. The finite element is used to verify the results. It is observed that, external excitation can change the natural period of elevated tanks. Considering the increase of excitation frequency, the natural period will be decreased. The concluded values of natural period in case of soft and very soft soil are more affected from excitation frequency values. The high range of excitation frequency may reduce the natural period values. In addition it is observed that the excitation frequency has no significant effect on convective period compare with impulsive period.

동위원소희석 질량분석법에 의한 혈액 중 Cd, Pb 성분의 측정 : 국제공동분석 (Determination of Cd and Pb in Human Blood by Isotope Dilution Inductively Coupled Plasma Mass Spectrometry : International Comparison)

  • 박창준;서정기;이상화
    • 분석과학
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    • 제9권2호
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    • pp.145-160
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    • 1996
  • 한국표준과학연구원 무기분석그룹에서는 1994년과 1995년도에 카나다 퀘백주 독성센터에서 실시한 혈액시료의 국제공동분석프로그램에 참여하였다. 이 프로그램의 목적은 생체시료에 있는 미량의 독성원소에 대해 참여하는 각국 실험실의 재현성과 정확도의 평가이다. 본 실험실에서는 3개 농도수준의 Pb과 Cd이 함유된 혈액시료를 동위원소희석 유도결합플라스마 질량분석법으로 분석하였다. 0.5mL의 혈액시료에 농축 동위원소를 첨가하고 질산 2mL와 함께 마이크로파 가압분해장치에서 분해한 후 약 10mL로 묽힌 후 ICP-MS에 주입하였다. 각국 실험실에서 보고한 Pb과 Cd의 농도를 나타내고 서로 비교하였으며 본 실험실에서 보고한 값은 모두 목표값에 매우 가까운 값을 얻었다.

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Bond Analysis of Ribbed Reinforcing Bars

  • Park, Oan-Chul
    • KCI Concrete Journal
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    • 제13권2호
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    • pp.19-25
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    • 2001
  • A simple expression to predict bond strength of reinforcing bars with rib deformation to the surrounding is derived for the case of splitting bond failure. Finite element analysis is used to model the confining behavior of concrete cover. The roles of the interfacial properties, specifically, the friction coefficient, cohesion, the relative rib area and the rib face angle are examined. Values of bond strength obtained using the analytical model are in good agreement with the bond test results from the previous studies. The analytical model provides insight into interfacial bond mechanisms and the effects of the key variables on the bond strength of deformed bars to concrete. Based on the comparison between the analytical results and the test results, the values of cohesion, coefficient of friction, and the effective rib face angle are proposed.

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중수소 핵자기 공명을 이용한 외국 술과 국산 술의 비교 분석 (Application of Deuterium NMR Analysis for the Differentiation of Korean and Foreign Liquors)

  • 한기정;이석근
    • 분석과학
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    • 제13권1호
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    • pp.127-129
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    • 2000
  • The $^2H$ NMR analysis was used to determine the relative deuterium contents at the position of methyl and methylene in ethyl alcohols. Four different liquors manufactured in Korea clearly showed different R values from those of foreign liquors. These R values for the Korean liquors could be used to distinguish adulteration.

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Shrinkage-Induced Stresses at Early Ages in Composite Concrete Beams

  • Park, Dong-Uk;Lee, Chang-Ho
    • KCI Concrete Journal
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    • 제14권1호
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    • pp.15-22
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    • 2002
  • Stresses that develop due to differential shrinkage between polymer modified cement mortar (PM) and Portland cement concrete (PCC) in a repaired concrete beam at early ages were investigated. Interface delamination or debonding of the newly cast repair material from the base is often observed in the field when the drying shrinkage of the repair material is relatively large. This study presents results of both experimental and analytical works. In the experimental part of the study, development of the material properties such as compressive strength, elastic modulus, interface bond strength, creep constant, and drying shrinkage was investigated by testing cylinders and beams for a three-week period in a constant-temperature chamber. Development of shrinkage-induced strains in a PM-PCC composite beam was determined. In the analytical part of the study, two analytical solutions were used to compare the experimental results with the analytically predicted values. One analysis method was of an exact type but could not consider the effect of creep. The other analysis method was rather approximate in nature but the creep effect was included. Comparison between the analytical and the experimental results showed that both analytical procedures resulted in stresses that were in fair agreement with the experimentally determined values. It may be important to consider the creep effect to estimate shrinkage-induced stresses at early ages.

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ESTIMATION OF SUGAR AND REDUCING SUGAR IN MOLASSES USING NEAR INFRARED REFLECTANCE SPECTROSCOPY

  • Mehrotra, Ranjana;Gupta, Alka;Tewari, Jagdish;Varma, S.P.
    • 한국근적외분광분석학회:학술대회논문집
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    • 한국근적외분광분석학회 2001년도 NIR-2001
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    • pp.1258-1258
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    • 2001
  • Estimation of sugar and reducing sugar content in molasses is very important task in sugar refineries. Conventional methods of determination of sugar content in molasses samples are highly time consuming and employ hazardous chemicals. Due to the physical properties of molasses, probability of error in conventional analytical techniques is high. These methods have proven to be inefficient for a process control in any sugar industry. Hence development of a rapid, inexpensive, physical and also accurate method for sugar determination in molasses will be highly useful. Near Infrared spectroscopy is being widely used worldwide as an analytical technique in food industry. The technique offers the advantage of being non-destructive and rapid. The present paper highlights the potential of near infrared reflectance spectroscopy as a rapid and automated analytical technique for determination of sugar and reducing sugar content in molasses. A number of molasses samples were collected during and after the sugar season from Havana Sugar Industry, Havana. The samples were chosen so as to obtain a wide range of concentration of sugar and reducing sugars. This was done in order to achieve a good calibration curve with widely spread data points. These samples were scanned in the region of 1100 - 2500 nm in diffuse reflectance mode. An indigenous ELICO NIR spectrophotometer, modified according to the requirements of sugar industry was used for this purpose. Each sample was also analyzed simultaneously by standard chemical methods. Chemical values were taken as reference for near infrared analysis. In order to obtain the most accurate calibration for the set of samples, various mathematical treatments were employed. Partial Least Square method was found to be most suitable for the analysis. A comparison is made between the actual values (chemical values) and the predicted values (NIR values). The actual values agree very well with the predicted values showing the accuracy of the technique. The validity of the technique is checked by predicting the concentration of sugar in unknown molasses samples using the calibration curve. The present investigation assesses the feasibility of the technique for on-line monitoring of sugars present in molasses in sugar industries.

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중성자방사화분석법을 이용한 성인여성 혈청중의 무기 원소 분석 (Determination of Inorganic Elements in Women Blood Serum using Instrumental Neutron Activation Analysis)

  • 문종화;정용삼;이옥희
    • 분석과학
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    • 제15권6호
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    • pp.509-513
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    • 2002
  • 본 연구는 우리나라 성인여성의 혈청 내 미량 무기 원소의 농도를 조사하기 위해 중성자 방사화 분석법을 적용하였다. 혈청시료중의 나트륨과 염소의 높은 농도가 분석에 제헌을 주었으며 이들의 간섭을 최소화시킨 분석조건에서 Br, Ca, Cl, Co, Cr, Cs, Fe, K, Na, Rb, Se, Zn 와 같은 12종 원소의 분석이 가능하였다. 63명의 성인여성으로부터 채취한 혈청시료를 분석시료를 분석하여 각 원소의 농도수준과 범위 등을 결정하였으며 미국표준연구소의 표준물질들을 혈청시료와 동시에 분석하여 분석품질관리에 사용하였다. 혈청시료중의 무기질원소들의 평균값은 Na 과 Cl은 약 3000 mg/L, Ca은 약 100 mg/L, K은 200 mg/L, Br, Se 및 Zn은 각각 6.0, 0.1, 1.0 mg/L 등의 농도수준을 보였으며 지금까지 보고된 값과 비교한 결과 큰 차이를 보이지 않았다.

신뢰성이론을 이용한 철근 콘크리트 부재의 전단변형 해석에 관한 평가 (The estimation for Shear Deformation Analysis of Reinforced Concrete members using Reliability Theory.)

  • 최광진;장일영;송재호
    • 한국콘크리트학회:학술대회논문집
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    • 한국콘크리트학회 1998년도 가을 학술발표논문집(II)
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    • pp.559-564
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    • 1998
  • The object of this thesis is an analytical study on shear deformation of reinforced concrete members using monte carlo method. Using the established experimental data that has been presented in various documents the stress-strain relationships curves of reinforced concrete (300kgf/$\textrm{cm}^2$~400kgf/$\textrm{cm}^2$) models are proposed. Finally, the theoretical values calculated using the analytical method developed in this study have been investigated in comparison with the experimental ones which were carried out earlier in order to prove its validity. From the results it has been shown that theoretical values agree quite well with experimental ones, and it could be pointed out that the presented analytical method is widely acceptable for the practical analysis of shear displacement of reinforced concrete members.

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New Analytical Method with Curvature Based Kinematic Deflection Curve Theory

  • Tayyar, Gokhan Tansel
    • International Journal of Ocean System Engineering
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    • 제2권3호
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    • pp.195-199
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    • 2012
  • This paper reports a new analytical method to calculate the planar displacement of structures. The cross-sections were assumed to remain in plane and the deflection curve was evaluated using the curvature values geometrically, despite being solved with differential equations. The deflection curve was parameterized with the arc-length of the curvature values, and was taken as an assembly of chains of circular arcs. Fast and accurate solutions of complex deflections can be obtained easily. This paper includes a comparison of the nonlinear displacements of an elastic tapered cantilever beam with a uniform moment distribution among the proposed analytical method, numerical method of the theory and large deflection FEM solutions.

Time-dependent Material Properties in FCM Segment of Prestressed Concrete Box-Girder Bridge

  • Yoon, Young-Soo;Choi, Han-Tae;Kwon, Soon-Beom
    • KCI Concrete Journal
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    • 제11권3호
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    • pp.99-107
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    • 1999
  • In designing the Prestressed concrete box-girder bridge. dead load, prestressing force, creep and shrinkage of concrete are the main factors which influence the camber and deflection of segmental concrete structure under construction. Among these factors the creep and shrinkage are the functions of the time-dependent property which. therefore, must be considered with time. The prediction model for estimating creep and shrinkage of concrete has been suggested by ACI, CEB/FIP, JSCE and KSCE design code and EMM, AEMM, RCM, IDM and SSM has been suggested for analytical method in consideration of time-dependent characteristics. In this study the creep test was carried out for four different curing ages of concrete which were applied to the Prestressed concrete structure at the construction site, and the results of test were compared with the values of creep prediction proposed by the design code. Also the creep test was performed with step-wise incremental stresses and the results were compared to the analytical values.

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