• Title/Summary/Keyword: amorphous Fe

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Influence of Humidity Variation on the Surface Deffects and Soft Magnetic Properties in the Fabrication of Fe Based Amorphous Alloy Ribbon by the PFC Process (PFC프로세스 의한 Fe기 Fe78Si9B13 비정질 합금리본 제조에 있어서 습도변화가 표면결함 및 연자기적 특성에 미치는 영향)

  • Choi, Y.J.;Jang, S.J.;Kim, S.W.;Jeon, B.S.;Kim, S.M.;Song, C.B.;Kim, Y.C.;Namkung, J.
    • Journal of the Korean Magnetics Society
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    • v.25 no.1
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    • pp.4-9
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    • 2015
  • This study was carried out to investigate a influence of humidity variation (%) on the magnetic properties and the surface flaws in the fabrication of Fe-based $Fe_{78}Si_9B_{13}$ amorphous alloy ribbon by Planar Flow Casting process. As a result, the size of the air pocket and the droplet which is observed in the contact surface and the free face of the amorphous alloy ribbon becomes large when the humidity increases and the size highly increases with the surface roughness at the same time. Especially, the surface roughness value which is made in the 65 % of the humidity is the lowest in the contact surface ($Ra=0.60{\mu}m$, $Rz=3.11{\mu}m$) and the free face ($Ra=0.47{\mu}m$, $Rz=3.00{\mu}m$). Also, in case of the soft magnetic property of the magnetic core which is made with the toroidal core of $23(OD)^*20(ID)^*20(H)$ size, in the sample of the amorphous alloy ribbon which is made in 65% of the humidity, the most excellent value is gained as $B_s(B_{700})=1.055T$, $H_c=0.083Oe$, permeability = 1,197 and core loss = 0.276W/kg.

Magnetic Properties of Fe-System Thin Films with Non-equilibrium Phases (비평형 Fe계 박막의 자기 특성)

  • Kim, H.S.;Min, B.K.;Song, J.S.;Oh, Y.W.;Lee, W.J.;Lee, D.Y.;Kim, l.S.
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2000.05b
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    • pp.13-16
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    • 2000
  • In this study, we have fabricated nonequilibrium $Fe_{85.6}Zr_{3.3}B_{5.7}Ag_{5.4}$ thin film, which contains an additional insoluble element Ag, by using DC magnetron sputtering method. We have investigated the magnetic properties of amorphous $Fe_{85.6}Zr_{3.3}B_{5.7}Ag_{5.4}$ thin film as a function of rotational field annealing(RFA). After deposition, the amorphous $Fe_{85.6}Zr_{3.3}B_{5.7}Ag_{5.4}$ thin film annealed by rotational field annealing method at $350^{\circ}C$ for an hour was founded to have high permeability of 8680 of 100 MHz, 0.2 mOe, low coercivity of 0.86 De and very low core loss of 1.3 W/cc at 1 MHz, 0.1T.

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Microstructural Effects on DC Bias Characters in FeSiBNi Amorphous Ribbon (FeSiBNi 비정질 리본의 열처리 조건에 따른 미세구조가 직류중첩특성에 미치는 영향)

  • 장용익;김종렬;송용설
    • Journal of the Korean Magnetics Society
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    • v.10 no.1
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    • pp.1-6
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    • 2000
  • Amorphous Fe$_{79.7}$Si$_{9.3}$B$_{9.7}$Ni$_{1.4}$ ribbon alloys were fabricated by a single roll method. To enhance D. C. bias properties, the magnetic and micro-structural changes have been investigated as the variation of annealing time and condition. The D. C. bias properties were found to be directly related to micro-structural changes. Primary ${\alpha}$-Fe dendrites with 200∼300 nm showed the best D. C. bias properties, which resulted from the magnetic domain wall pinning effect. Due to the differences of cooling rate, the growth shape and distribution of the dendrites is divided into two areas.

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Magnetic and Magnetostrictive Properties of Amorphous Tb-Fe- and Tb-Fe-B Thin Films

  • Park, Y. S.;Lee, S. R.;S. H. Han;Kim, H. J.;S. H. Lim
    • Journal of Magnetics
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    • v.2 no.3
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    • pp.76-85
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    • 1997
  • Magnetic and magnetostrictive properties of Tb-Fe and Tb-Fe-B thin films are systematically investigated over a wide composition range from 40.2 to 68.1 at. % Tb. The films were fabricated by rf magnetron sputtering using a composite target which consists of an Fe plate and Tb chips. The microstructure, examined by X-ray diffraction, mainly consists of an amorphous phase and, at high Tb contents, a pure Tb phase also exists. A progressive change in the direction of anisotropy from the perpendicular to in-plane occurs as the Tb content increases and the boundary at which the anisotropy change occurs shifts significantly towards to higher Tb contents with the addition of B. The saturation magnetization exhibits maxima at the Tb contents of 42 and 48 at. % for Tb-Fe and Tb-Fe-B thin films, respectively, and it is decreased by the addition of B. The coercive force, measured in the easy direction, decreases monotonically with the Tb content. Excellent magnetostrictive characteristics, particularly at low magnetic fields, are achieved in both Tb-Fe and Tb-Fe-B thin films; for example, a magnetostriction of 138 ppm is obtained in a Tb-Fe-B thin film at a magnetic field as low as 30 Oe. The excellent magnetostrictive properties of the present thin films are supported by the equally excellent magnetic softness, the coercivity below 10 Oe and a typical squared-loop shape with the saturation field as low as 1 kOe. Due to the excellent low field magnetostrictive characteristics, the present Tb-Fe based thin films are thought to be suitable for Si based microdevices.

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Effects of Microbial Iron Reduction and Oxidation on the Immobilization and Mobilization of Copper in Synthesized Fe(III) Minerals and Fe-Rich Soils

  • Hu, Chaohua;Zhang, Youchi;Zhang, Lei;Luo, Wensui
    • Journal of Microbiology and Biotechnology
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    • v.24 no.4
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    • pp.534-544
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    • 2014
  • The effects of microbial iron reduction and oxidation on the immobilization and mobilization of copper were investigated in a high concentration of sulfate with synthesized Fe(III) minerals and red earth soils rich in amorphous Fe (hydr)oxides. Batch microcosm experiments showed that red earth soil inoculated with subsurface sediments had a faster Fe(III) bioreduction rate than pure amorphous Fe(III) minerals and resulted in quicker immobilization of Cu in the aqueous fraction. Coinciding with the decrease of aqueous Cu, $SO_4{^{2-}}$ in the inoculated red earth soil decreased acutely after incubation. The shift in the microbial community composite in the inoculated soil was analyzed through denaturing gradient gel electrophoresis. Results revealed the potential cooperative effect of microbial Fe(III) reduction and sulfate reduction on copper immobilization. After exposure to air for 144 h, more than 50% of the immobilized Cu was remobilized from the anaerobic matrices; aqueous sulfate increased significantly. Sequential extraction analysis demonstrated that the organic matter/sulfide-bound Cu increased by 52% after anaerobic incubation relative to the abiotic treatment but decreased by 32% after oxidation, indicating the generation and oxidation of Cu-sulfide coprecipitates in the inoculated red earth soil. These findings suggest that the immobilization of copper could be enhanced by mediating microbial Fe(III) reduction with sulfate reduction under anaerobic conditions. The findings have an important implication for bioremediation in Cu-contaminated and Fe-rich soils, especially in acid-mine-drainage-affected sites.

MICROCRYSTALLINE Fe-Si-Al-B THIN RIBBON

  • Sun, Guiqin;Yu, Xiaojun;Zhang, Jikai;Narita, Kenji
    • Journal of the Korean Magnetics Society
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    • v.5 no.5
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    • pp.504-506
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    • 1995
  • By means of adding B into Sendust alloy (Fe-Si-Al) with state of amorphous ribbon, mechnical properties of alloy was improved effectively, and magnetic properties didn't decrease obviously. The optimum adding quantity of B is 0.015-0.03 wt%. The adding of B was thought to give rise to reduction of ordering degree of $Fe_{3}(Si,Al)$ phase of Sedust alloy(Fe-Si-Al-B) and result in improvment of embrittlement of this alloy.

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Soft-magnetic Characteristics of Co-based Amorphous Powder Produced by Spinning Water Atomization Process (SWAP)

  • Otsuka, I.;Wada, K.;Watanabe, A.;Kadomura, T.;Yagi, M.
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09b
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    • pp.784-785
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    • 2006
  • Co-based amorphous powder was produced by a new atomization process "Spinning Water Atomization Process (SWAP)", having rapid super-cooling rate. The composition of the alloys was ($(Co_{0.95}Fe_{0.05})_{1-x}Cr_x$)$_{75}Si_{15}B_{10}$ (x=0, 0.025, 0.05, 0.075). The powders became the amorphous state even if particle size was up to about $500{\mu}m$. The coercive force of powders was about 0.35 - 0.7 Oe. Furthermore, Co-based amorphous powder cores with glass binders were made by cold-pressing and sintering methods. The initial permeability of the core in the frequency range up to 100 kHz was about 110, and the core loss at 100 kHz for Bm = 0.1 T was $350kW/m^3$.

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