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Effects of Heat Treatment Temperature and Cooling Method on Microstructure and Hardness of Cu-22Sn alloy (열처리 온도 및 냉각방법이 Cu-22Sn합금의 미세조직 및 경도변화에 미치는 영향)

  • Jeong, Museob;Shin, Ari;Han, Jun Hyun
    • Journal of the Korean Society for Heat Treatment
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    • v.31 no.3
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    • pp.104-110
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    • 2018
  • The effects of heat treatment time and cooling method on microstructure and mechanical property of Cu-22wt%Sn alloy were discussed. ${\alpha}+{\delta}$ mixed phase structure was obtained in air-cooled specimens after heat treatment at 775, 750, and $700^{\circ}C$ for 1 hour. On the other hand, in water-cooled specimens, ${\alpha}+{\beta}^{\prime}$ martensite mixed phase was obtained. In the case of water-cooled specimens, the hardness value decreased with decreasing heat treatment temperature because the volume fraction of ${\alpha}$ phase with low hardness value increased as the heat treatment temperature decreased. In water-cooled specimen after heat treatment at $600^{\circ}C$, ${\gamma}^{\prime}$ martensite was formed instead of ${\beta}^{\prime}$ martensite. The hardness value of ${\gamma}^{\prime}$ martensite was lower than those of ${\beta}^{\prime}$ and ${\delta}$ phases.

SPECTRAL DIAGNOSTICS OF NON-THERMAL PARTICLES IN THE SOLAR CHROMOSPHERE

  • FANG C.;XU Z.;DING M. D.
    • Journal of The Korean Astronomical Society
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    • v.36 no.spc1
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    • pp.55-61
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    • 2003
  • There are at least three effects of the non-thermal particle bombardment on the solar atmosphere: (1) non-thermal ionization and excitation; (2) proton-hydrogen charge exchange; (3) impact line polarization. Due to the non-thermal ionization and excitation effects of electron bombardments in flares, H$\alpha$ line is widely broadened and shows a strong central reversal. Significant enhancements at the line wings of Ly$\alpha$ and Ly$\beta$ are also predicted. In the case of proton bombardment, less strong broadening and no large central reversal are expected. However, due to proton-hydrogen charge exchange, the enhancements at the red wings of Ly$\alpha$ and especially of Ly$\beta$ lines at the early impulsive phase of flares are significant. Electron beam can also in some cases generates visible and UV continuum emission in white-light flares. However, at the onset phase, a negative 'black' flare may appear in several seconds, due to the increase of the $H^-$ opacity. The impact polarization of atomic lines can provide complementary information on the energetic particles, the energy transport and deposit in the solar chromosphere. New results of spectropolarimetric analysis for the major flare on July 23, 2002 are also given in the paper.

Volatile components of Schizandra Chinensis Bullion (오미자(Schizandra Chinensis Bullion)의 휘발성 성분)

  • Kim, Ok-Chan;Jang, Hee-Jin
    • Applied Biological Chemistry
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    • v.37 no.1
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    • pp.30-36
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    • 1994
  • The essential oil of Schizandrae Fructus was extracted by simultanous distillation-extraction and steam distillation and analyzed by GC and GC-MS. The oil content of Schizandrae Frutus was 0.64% when extracted by steam distillation and 0.88% in case of simultanous distillation extraction and sensory analysis of the oil indicated woody, camphorous, spicy and sour characteristic notes. The experimental results confirmed the presence 47 volatile components, the major components were ${\gamma}-terpinene$, p-cymene, ${\alpha}-ylangne$ and ${\beta}-elemene$. The oil was fractioned into ten fractions and 4 fraction of them have a good aroma character. The application of the oil showed the utilization possibility as flavoring materials for Korea tea.

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Generation of Klobuchar Coefficients for Ionospheric Error Simulation

  • Lee, Chang-Moon;Park, Kwan-Dong;Ha, Ji-Hyun;Lee, Sang-Uk
    • Journal of Astronomy and Space Sciences
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    • v.27 no.2
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    • pp.117-122
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    • 2010
  • An ionospheric error simulation is needed for creating precise Global Positioning System (GPS) signal using GPS simulator. In this paper we developed Klobuchar coefficients n ${\alpha}_n$ and ${\beta}_n$ (n = 1, 2, 3, 4) generation algorithms for simulator and verified accuracy of the algorithm. The algorithm extract those Klobuchar coefficients from broadcast (BRDC) messages provided by International GNSS Service during three years from 2006 through 2008 and curve-fit them with sinusoidal and linear functions or constant. The generated coefficients from our developed algorithms are referred to as MODL coefficients, while those coefficients from BRDC messages are named as BRDC coefficients. The maximum correlation coefficient between MODL and BRDC coefficients was found for ${\alpha}_2$ and the value was 0.94. On the other hand, the minimum correlation was 0.64 for the case of ${\alpha}_1$. We estimated vertical total electron content using the Klobuchar model with MODL coefficients, and compared the result with those from the BRDC model and global ionosphere maps. As a result, the maximum RMS was 3.92 and 7.90 TECU, respectively.

Microstructural Changes during Semi-solid State in Hypereutectic Al-Si Alloy (과공정 Al-Si 합금의 반고상 재가열시 미세조직 변화)

  • Kim, In-Joon;Kim, Do-Hyang
    • Journal of Korea Foundry Society
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    • v.18 no.6
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    • pp.541-549
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    • 1998
  • Microstructural characteristics of hypereutectic Al-Si alloys during reheating at semi-solid temperature have been investigated. The size and morphology of primary Si particles in wedge-type mold-cast ingot has been compared with hot-rolled sheet and Si particulate reinforced Al composite. Effects of P and Sr addition on the morphological changes of primary Si particles have been also investigated. Observation of the solidification microstructures of the wedge-type mold-cast ingot at different cooling rates showed that alloying elements such as P and Sr affect the morphology of Si particles, especially in the area solidified at a slow cooling rate. Negligible change in the size of primary crystals was observed after reheating experiment, but ${\alpha}-halo$ formed around the Si particles and fine particles of Si precipitated in the surrounding area of the Si particles. In addition, there seemed to be no coarsening with increasing of holding time and the region of ${\alpha}-halo$ being decreased. Nucleation and recrystallization was accelerated with addition of alloying elements during hot rolling resulting in a decrease of primary Si particle size. In the case of extruded specimens, morphological change of primary Si particles was not observed after reheating. No ${\alpha}-halo$ formation was observed in Si reinforced Al composite because of the oxide film formed on the Si particles which acted as a diffusion barrier between substrate and the primary Si particles.

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STRONG CONVERGENCE OF COMPOSITE IMPLICIT ITERATIVE PROCESS FOR A FINITE FAMILY OF NONEXPANSIVE MAPPINGS

  • Gu, Feng
    • East Asian mathematical journal
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    • v.24 no.1
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    • pp.35-43
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    • 2008
  • Let E be a uniformly convex Banach space and K be a nonempty closed convex subset of E. Let ${\{T_i\}}^N_{i=1}$ be N nonexpansive self-mappings of K with $F\;=\;{\cap}^N_{i=1}F(T_i)\;{\neq}\;{\theta}$ (here $F(T_i)$ denotes the set of fixed points of $T_i$). Suppose that one of the mappings in ${\{T_i\}}^N_{i=1}$ is semi-compact. Let $\{{\alpha}_n\}\;{\subset}\;[{\delta},\;1-{\delta}]$ for some ${\delta}\;{\in}\;(0,\;1)$ and $\{{\beta}_n\}\;{\subset}\;[\tau,\;1]$ for some ${\tau}\;{\in}\;(0,\;1]$. For arbitrary $x_0\;{\in}\;K$, let the sequence {$x_n$} be defined iteratively by $\{{x_n\;=\;{\alpha}_nx_{n-1}\;+\;(1-{\alpha}_n)T_ny_n,\;\;\;\;\;\;\;\;\; \atop {y_n\;=\;{\beta}nx_{n-1}\;+\;(1-{\beta}_n)T_nx_n},\;{\forall}_n{\geq}1,}$, where $T_n\;=\;T_{n(modN)}$. Then {$x_n$} convergence strongly to a common fixed point of the mappings family ${\{T_i\}}^N_{i=1}$. The result presented in this paper generalized and improve the corresponding results of Chidume and Shahzad [C. E. Chidume, N. Shahzad, Strong convergence of an implicit iteration process for a finite family of nonexpansive mappings, Nonlinear Anal. 62(2005), 1149-1156] even in the case of ${\beta}_n\;{\equiv}\;1$ or N=1 are also new.

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Sintering and Microstructure of $Ce-TZP/Al_2O_3$ Ceramic Composite ($Ce-TZP/Al_2O_3$ 세라믹 복합재료의 소결과 미세구조)

  • 박홍채;홍상희;이윤복;오기동
    • Journal of the Korean Ceramic Society
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    • v.31 no.7
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    • pp.703-714
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    • 1994
  • Sintering and microstructure of Ce-TZP/Al2O3 composite with $\alpha$-Al2O3 matrix containing dispersed 5~50 vol% ZrO2 were discussed. Sintered density was increased with elevating forming pressure in range of 6~300 MPa and about >99.2% of theoretical density was obtained at 1$600^{\circ}C$ for 2h in case of 300 MPa of 6~300 MPa uniaxially cold-pressed compacts containing 20 vol% ZrO2. All kinds of different batch composition exhibited nearly the same shrinkage behaviour with end-point shrinkage between 20 and 24%, and had the maximum shrinkage rate (0.41~0.54%/min) around 140$0^{\circ}C$. Grain growth was occurred faster in $\alpha$-Al2O3 than in {{{{ gamma }}-Al2O3 starting matrix during sintering at 1$600^{\circ}C$. Bimodal pore size distribution of interaglomerate pores with size of 0.03~0.2 ${\mu}{\textrm}{m}$ and of interaglomerate pores with size of around 60 ${\mu}{\textrm}{m}$ was obtained in Ce-TZP/$\alpha$-Al2O3 composite sintered at 130$0^{\circ}C$. But unimodal pore size distribution with around 0.1 ${\mu}{\textrm}{m}$ was observed in Ce-TZP/{{{{ gamma }}-Al2O3 composite sintered at the same temperature. Microcracks were occurred due to the tlongrightarrowm transformation of ZrO2 on cooling process.

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The Flow Analysis of Supercavitating Cascade by Nonlinear Theory (비선형이론에 의한 Supercavitation 익렬의 유동해석)

  • Pak, Ee-Tong;Hwang, Yoon
    • Solar Energy
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    • v.17 no.1
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    • pp.35-46
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    • 1997
  • In this study comparison of experiment results with the computed results of linear theory and nonlinear theory using singularity method was obtainable. Specially singularity points like sources and vortexes on hydrofoil and freestreamline were distributed to analyze two dimensional flow field of supercavitating cascade using nonlinear theory, and governing equations of flow field were derived and hydraulic characteristics of cascade were calculated by numerical analysis of the governing equations. The results compared linear theory and nonlinear theory with the experiment results of the study are as follows: The tolerances of nonlinear theory were larger than those of linear theory in case of ${\alpha}<10^{\circ}$. Moreover the computational range of attack angles could be expanded from ${\alpha}=10^{\circ}$ to ${\alpha}=25^{\circ}$, the flow field of supercavitating cascade could be analyzed in the condition which the wake thickness and the length of cavity are a variable. The shapes of cavity were changed sensitively according to various variable such as attack angles, pitches and wake thickness, and the pressure distribution of hydrofoil surface was identical almost disregarding wake thickness but changed largely according to attack angle and the length of cavity. Lift coefficient and drag coefficient were reduced according to increasing of wake thickness but the influences of wake thickness were very little in the situation of small pitch and long cavity.

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Modification of Oxidation Wool Treated with Protease(Part I)-Changes of chemical properties (산화양모의 효소처리에 의한 양모섬유의 개질(제1보)-화학적 성질의 변화-)

  • 김영리;유효선
    • Journal of the Korean Society of Clothing and Textiles
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    • v.22 no.7
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    • pp.843-850
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    • 1998
  • The purpose of this study is the investigation of chemical properties of wool treated with oxidants and protease at low temperature. The chemical degradation of the fibers were investigated by measuring $\alpha$-amimo acid contents and FT-IR analysis. In addition, urea-hydrogensulfite solubility was measured to compare to the oxidation and protease treated wool. The results were as follows. 1) By the oxidation of wool, cystine is oxidised to cysteic acid by way of the intermediate oxides, cystine-S-monooxide and cystine-S-dioxide, in the case hydrolysis catalysed by the protease catalyse. Also, $\alpha$-amimo acid contents is increased, and urea-hydrogensulfite solubility was lower than that of untreated wool. This chemical degradation of wool was occurred due to oxidate hydrolysis in the order of permonosulfate>dichloroisocyanuric acid$\geq$chlorine. 2) The chemical degradation of wool was accelerated by the protease treatment of oxidized wool. Oxidation of wool is considered to make the fiber more susceptibled to enzymatic attact by opening disulphide bond within wool. Enzymatic attact was effectively directed to the wool oxidised by permonosulfate.

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Angiotensin I-converting Enzyme Inhibitory Activities of Porcine Skeletal Muscle Proteins Following Enzyme Digestion

  • Katayama, K.;Fuchu, H.;Sakata, A.;Kawahara, S.;Yamauchi, K.;Kawamura, Y.;Muguruma, M.
    • Asian-Australasian Journal of Animal Sciences
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    • v.16 no.3
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    • pp.417-424
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    • 2003
  • Inhibitory activities against angiotensin I-converting enzyme (ACE) of enzymatic hydrolysates of porcine skeletal muscle proteins were investigated. Myosin B, myosin, actin, tropomyosin, troponin and water-soluble proteins extracted from pork loin were digested by eight kinds of proteases, including pepsin, $\alpha$-chymotrypsin, and trypsin. After digestion, hydrolysates produced from all proteins showed ACE inhibitory activities, and the peptic hydrolysate showed the strongest activity. In the case of myosin B, the molar concentration of peptic hydrolysate required to inhibit 50% of the activity increased gradually as digestion proceeded. The hydrolysates produced by sequential digestion with pepsin and $\alpha$-chymotrypsin, pepsin and trypsin or pepsin and pancreatin showed weaker activities than those by pepsin alone, suggesting that ACE inhibitory peptides from peptic digestion might lose their active sequences after digestion by the second protease. However, the hydrolysates produced by sequential digestion showed stronger activities than those by $\alpha$-chymotrypsin, trypsin or pancreatin alone. These results suggested that the hydrolysates of porcine meat were able to show ACE inhibitory activity, even if they were digested in vivo, and that pork might be a useful source of physiologically functional factors.