• Title/Summary/Keyword: alkali washing

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Effect of Washing Treatment of Aged Paper Materials for Better Conservation (열화된 종이자료의 보존성 개선을 위한 세척처리 특성)

  • Lee, Kwi-Bok;Seo, Yung-Bum;Park, So-Yeon;Jeon, Yang;Shin, Jong-Soon
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.38 no.4 s.117
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    • pp.53-60
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    • 2006
  • Paper materials for long term conservation suffer slowly mechanical and chemical deterioration, the extent of which may depend upon their conservation environment. Those deterioration includes discoloring, low moisture content, acidification, and brittleness. To slow deterioration, washing treatment, deacidification, and polymer reinforcement on paper materials are usually used. One easy and simple method of fixing low moisture content and acidification was an washing method, and we used both distilled and alkali water in washing method in this study. Alkali water is electrolyzed cathode water of high pH, and has no alkali metal ions in it. Experiment showed that washing treatment with both distilled and alkali water gave improvement in raising moisture content, pH, and mechanical strength of paper materials even after severe accelerated aging test. Advantageous effect of alkali water over distilled water on preventing deterioation was also shown clearly.

Investigation of Water-Washing Process Parameters for Removal of Alkali Metals and Chlorides from Electric Arc Furnace Dust (EAFD) (전기 제강로 분진(EAFD)으로부터 알칼리 금속 및 염화물 제거를 위한 수 세척 공정 운영인자 조사)

  • Lee, Han Saem;Park, Da so mi;Ha, Jong Gil;Shin, Hyun Sang
    • Journal of Korean Society of Environmental Engineers
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    • v.39 no.11
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    • pp.626-633
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    • 2017
  • The present study investigated the effect of a water-washing process, which is part of the acid hydrometallurgical process for recovery of high purity of zinc, on the removal of alkali metals and chlorides (Na, K, Ca, Cl) from Electric arc furnace dust (EAFD). Two EAFD samples with different properties were characterized by particle size, XRD and element analysis, and their washing efficiencies (%) on alkali metals and chlorides were compared according to pH, washing time, liquid to solid (L/S) ratio and number of washings. The results show that the alkali metals and chlorides could be effectively removed by the washing (at L/S ration of 3 for more than 30 min., pH 10~11) while minimizing loss of zinc (<0.1%), in which the washing efficiency was Na-78%, K-76%, Cl >99%, respectively. Na and K could be removed up to 97% and 89% respectively by 3 times of repeated washings. With increased sample volume (10 times) of the mixed (1:1, w/w) sample with two types of EAFD, it was confirmed that the pH(10~11) can be used as the main process control parameter for the washing of the alkali metals regardless of EAFD properties.

Changes in an Ammonia-like Odor and Chondroitin Sulfate Contents of Enzymatic Hydrolysates from Longnose Skate (Rasa rhina) Cartilage as Affected by Pretreatment Methods

  • Choi, Joo-Hyun;Woo, Jin-Wook;Lee, Yang-Bong;Kim, Seon-Bong
    • Food Science and Biotechnology
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    • v.14 no.5
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    • pp.645-650
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    • 2005
  • To reduce ammonia-like odor in chondroitin sulfate, longnose skate (Rasa rhina) cartilage was processed by washing, autoclaving, and alkali pretreatments. Content of total volatile basic nitrogen (TVB-N), index of ammonia-like odor, of raw skate cartilage without pretreatment was 254 mg/100 g, whereas those of skate cartilage pretreated with washing and autoclaving increased to 630 and 636 mg/100 g, respectively. TVB-N of skate cartilage pretreated with sodium hydroxide sharply decreased to 15 mg/l00 g at optimal condition of 0.12 M and 3.6 volume of NaOH, as determined by surface response methodology of central composite design for optimization. Alkali pretreatment resulted in 97.6% deodorizing. Washing and autoclaving pretreatments had almost no effect on the yield of chondroitin sulfate (approximately 30%), whereas decreased to 16.0% after alkali pretreatment, showing chondroitin sulfate of skate cartilage as chondroitin sulfate C.

Effect of Washing Conditions on Dimensional Change and Mechanical Properties in Polyester/Spandex Knit Fabric (세탁조건에 따른 폴리에스터/스판덱스 편성물의 형태안정성과 역학적 특성 변화)

  • Roh, Eui Kyung;Kim, Eunae
    • Fashion & Textile Research Journal
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    • v.20 no.1
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    • pp.93-100
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    • 2018
  • This study comparatively analyzed the changes in the dimensional stability and the mechanical properties of stretch knit fabrics associated with washings conditions in order to determine the most appropriate washing method. Polyester and spandex knit fabrics were washed 25 cycles with nine washing condition profiles that controled detergent, hardness. temperature and RPM. The knit fabrics with repeated washings were evaluated by dimensional stability and measured by the KES-FB system. Polyester and spandex fibers have good chemical resistance. However, the changes in the dimensional stability and the mechanical properties were observed in washed knit fabrics. After repeated washings, the knit fabrics washed in an alkali or neutral detergent had good dimensional stability compared with the knit fabric washed in functional detergent. The washed knit fabrics were extended, stiff, rough, and had a smaller volume. The changes were the result of the rearrange of polyester fibers which twisted around spandex core and chemical interactions involving the detergent and the physical and mechanical forces of washing. Especially, using an alkali detergent resulted in increased stiffness and roughness of the knit fabric. In conclusion, the washing in water with low hardness and a neutral detergent can minimize the changes in dimensional stability and mechanical properties of polyester and spandex knit fabric.

A Study on the Property and the Skin Irritability of the Reclaimed Soap (폐유을 이용한 재생비누의 특성 및 피부자극도에 대한 연구)

  • 하금;이혜자;유혜자
    • Journal of the Korean Home Economics Association
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    • v.36 no.1
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    • pp.1-11
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    • 1998
  • The purpose of this study is to find troubles in producing and using the reclaimed soaps to get the solutions of their troubles. Five kinds of reclaimed soaps were taken from religious or civic organizations and nine kinds of soaps were made by adding sodium hydroxide of different concentrations to the used vegetable oil in our laboratory. Washing efficiency, pH test, BOD, and skin irritability of the reclaimed of manufactured soaps were examined. The washing efficiency of the manufactured soaps were ±80%. The percent of free-alkali tended to increase as the amount of NaOH increased. The skinirritability was proportional to the amount of NaOH added. To make the reclaimed soap, the best percent of NaHO to used oil is 17% or 18% and this ratio(17%∼18%) should be kept. Manufactured soaps by this ratio have good apperance condition and washing efficiency. And also they have low skin irritability and free-alkali. This study has the limitations that the skin irritability test can have individual and the collected soaps couldn't represent all kinds of recaimed soap.

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Utilization of Domestic Small Timbers -Shrinkage and Swelling of Alkali-Treated Woods- (간벌재 및 소경재의 이용개발에 관한 연구 -알칼리 처리 목재의 수축팽윤성-)

  • 황원중;김남훈
    • Journal of Korea Foresty Energy
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    • v.18 no.2
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    • pp.70-77
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    • 1999
  • The behaviors of alkali swelling in four major Korean woods were examined as a function of concentration cf alkali solution. Density of alkali-treated woods increased highly with increasing alkali concentration in both softwoods and hardwoods. Wood samples swelled in dimension during alkali swelling, and thereafter they shrank highly by water washing and air drying. The air-dried wood samples after alkali treatment showed almost isotropic shrinkage in tangential and radial direction.

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Effect of Alkali-Washing at Different Concentration on the Chemical Compositions of the Steam Treated Bamboo Strands

  • MAULANA, Muhammad Iqbal;MURDA, Rio Ardiansyah;PURUSATAMA, Byantara Darsan;SARI, Rita Kartika;NAWAWI, Deded Sarip;NIKMATIN, Siti;HIDAYAT, Wahyu;LEE, Seung Hwan;FEBRIANTO, Fauzi;KIM, Nam Hun
    • Journal of the Korean Wood Science and Technology
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    • v.49 no.1
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    • pp.14-22
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    • 2021
  • The objective of this study was to investigate the effect of alkali-washing with different sodium hydroxide concentrations on the chemical compositions of steam-treated Betung bamboo strand. Strands were subjected to steam treatment at 126 ℃ for 1 h under 0.14 MPa pressure and followed by washing with 1-5% sodium hydroxide solution for 30 sec. The alteration of structural and non-structural chemical components content of bamboo strands was evaluated. Steam and washing treatments with various concentrations of sodium hydroxide solution considerably reduced the extractive content of bamboo strands, and the cell wall chemical components of the strand in the small degree. FTIR analysis showed noticeable changes in peaks related to hemicellulose and lignin. The relative crystallinity increased significantly after steam and washing treatment with sodium hydroxide up to 3% concentration. SEM Images showed smooth and clean strands surface after washing with 3% sodium hydroxide.

Remediation of Insecticides (Parathion, Diazinon) Contaminated Soil by Washing Process (토양 세척을 통한 살충제 (파라티온, 다이아지논)로 오염된 토양의 정화)

  • 현재혁;백정선;조미영
    • Proceedings of the Korean Society of Soil and Groundwater Environment Conference
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    • 1999.10a
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    • pp.3-6
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    • 1999
  • Several chemical washing procedures were applied to Parathion and Diazinon contaminated soil. Batch and column tests were performed to determine the insecticides extraction efficiency as a function of pH. Washing efficiency of methanol is more higher than that of water and HCl when washed parathion and diazinon are. Those are completely miscible with most organic solvents. For parathion, release trend is increased as pH is increased because it is hydrolyzed easily at the condition of alkali. But diazinon shows reverse because diazinon is decomposed rapidly at the condition of acidic So, diazinon is more released than parathion is because this experiment is peformed in acidic and weak acidic conditions. Generally, parathion and diazinon are classified as having low mobility, so they can be easily controlled if the proper washing process are applied.

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Dyeability and Functional Characteristics of Arecae semen Extract (빈랑자 추출물의 염색성 및 기능성에 관한 연구)

  • 김지선;조용석;최순화
    • Journal of the Korean Home Economics Association
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    • v.41 no.7
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    • pp.13-24
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    • 2003
  • Recently there has been interested in the use of natural dyes in textile applications. Generally natural dyes can exhibit better biodegradability and have a higher compatibility with the environment. In this study, cotton, wool and silk fabrics were dyed with alkali extract of Arecae semen using various mordants, and their dyeabilities were discussed. Additionally the fastness to washing, perspiration, light, rubbing, and drycleaning and UV-B protection rate were also investigated. Cotton, silk and wool fabrics dyed with alkali extract of Arecae semen were colored in reddish yellow tint. The optimum dyeing condition of the colorants extracted from the Alecae semen was three repeated dyeing at $95^{\circ}C$ for 1.5 hrs. The dyed fabrics by using mordanting methods improved the fastness to washing, perspiration and drycleaning, but the fastness to light and rubbing were not increased. The UV-B protection rate of the wool fabrics were increased by dyeing with extract of Arecae semen.

A Study on the Change of Physical Properties of Lining Fabric by Washing (세탁에 의한 안감의 물성변화에 관한 연구)

  • Song, Kyoung-Hun;Jung, Young-Hee;Kim, Hyun-Mi
    • Korean Journal of Human Ecology
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    • v.7 no.1
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    • pp.175-182
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    • 1998
  • This study was to investigated physical properties of lining fabric (Nylon, Acetate, Rayon and Polyester) such as shrinkage, tensile strength, moisture regain and crease resistance. The results were as follows. 1. The number of repeated washing times and the concentration of the detergent almost didn't affect on the change of tensile strength. 2. As washing increase more, the shrinkage of all sample was more increased. In the case of Rayon, it was showed that shrinkage was high by $1{\sim}3$ times washing. In the case of Nylon, it was showed minus shrinkage according to frequency of washing. 3. The moisture regain was very decreased by 1 times washing. But the moisture regain was increased with increase in frequency of washing and resulted in it was showed a similar value with controls. 4. As the frequency of washing and the concentration of detergent increase more, the crease resistance was decreased considerably because the elasticity of fiber decreased by mechanical force such as tension, bending and pressure and alkali.

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