• 제목/요약/키워드: ageing stability

검색결과 36건 처리시간 0.023초

셀룰로오스 유도체 용액을 이용한 열화 한지의 강도보강 처리에 관한 연구 (Studies on the Reinforcement Treatment of Aged Hanji Using Cellulose Derivative Solutions)

  • 강광호;김형진
    • 펄프종이기술
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    • 제43권2호
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    • pp.40-48
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    • 2011
  • To build up the conservativeness of aged paper heritages, the strength reinforcement treatment using various cellulose derivative solutions was considered. Hand-made Hanji prepared by traditional papermaking technique was firstly simulated in order to modify the overall of paper properties like aged paper heritages by accelerated ageing treatment at $150^{\circ}C$ for 24 hours, and then the ageing stability of Hanji was verified through the secondary accelerated ageing at $150^{\circ}C$ for 12 hours. The physical properties of aged Hanji were improved by applying with cellulose derivative solutions. The ageing stability for physical, optical (L, brightness, opacity, yellowness) and chemical (oxidation index, degree of polymerization) properties of aged Hanji treated with all kinds of cellulose derivative solutions was also good compared to those of untreated samples, especially using MC solution. Therefore, it was that a kind of MC solution would be well-suited for the strength reinforcement treatment of aged paper heritages.

Impacts of post-mortem ageing prior to freezing on technological and oxidative properties of coarse ground lamb sausage in a model system

  • Choe, Juhui;Kim, Hyun-Wook;Farouk, Mustafa M.;Kim, Yuan H. Brad
    • Asian-Australasian Journal of Animal Sciences
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    • 제30권7호
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    • pp.1021-1028
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    • 2017
  • Objective: The objective of this study was to evaluate the effects of ageing time of lamb loins prior to freezing on technological characteristics and oxidation stability of coarse ground lamb loin sausage using in a model system. Methods: Lamb loins (M. longissimus lumborum, n = 25) were aged at $-1.5^{\circ}C$ for 0, 1, 2, 3, and 8 wk and then frozen for the remaining days (a total of 30 wk). The aged/frozen/thawed lamb loins were ground, and model sausages were formulated with 75% aged/frozen/thawed lamb loin, 25% water, 1.5% sodium chloride (NaCl) and 0.3% sodium tripolyphosphate. The pH and thaw/purge loss of aged/frozen/thawed lamb loins were evaluated, and protein functionality (protein solubility and emulsifying capacity), water-holding capacity and textural properties of model sausages were determined. Cooked model sausages were vacuum-packaged in a plastic bag and displayed under continuous fluorescent natural white light ($3^{\circ}C{\pm}1^{\circ}C$). Colour and lipid oxidation of the cooked model sausages were evaluated on 0 and 21 d of display storage. Results: Ageing prior to freezing had no impact on pH and purge/thaw loss of lamb loins and the colour of cooked sausages (p>0.05) made from the loins. Lamb loins aged for at least 3 wk prior to freezing numerically improved total and myofibrillar protein solubilities (p>0.05) and emulsion activity index (p = 0.009) of meat batter, but decreased cooking loss (p = 0.003) and lipid oxidation (p<0.05) of model sausages. Conclusion: This study suggests that post-mortem ageing of raw meat prior to freezing could improve water-holding capacity and lipid oxidative stability of sausage made from the meat.

Insight Into the Crystallinity of Chinese Ancient Silk by Synchrotron Radiation-Based and Conventional X-ray Diffraction Methods

  • Gong, Decai;Zhang, Xiaoning;Gong, Yuxuan
    • 보존과학회지
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    • 제36권1호
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    • pp.1-14
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    • 2020
  • This study investigates the crystallinity distribution of ancient silk. Owing to the inherent multi-hierarchical structure of silk protein and the complicated structural changes that occur due to various burial environments, it is challenging but worthwhile to study ancient silk ageing behavior, which is based on the fact that ageing begins with a single fiber and then spreads to a whole fabric. Crystallinity was one of the most effective indicators found to reveal the ageing status of silk. Therefore, a synchrotron radiation-based X-ray diffraction(SR-XRD) method was employed to study the crystallinity distribution of single fibers of ancient silk unearthed from seven archaeological sites in China from historical periods including the warring states, Han dynasty, Song dynasty, and Ming dynasty. In comparison, the conventional X-ray diffraction method, which uses large amounts of samples, was also performed to determine the integral crystallinity of ancient silk. Thermal stability experiments by thermogravimetry(TG) as well as morphology observations by scanning electron microscopy(SEM) and optical microscopy(OM) all confirmed the deterioration of ancient silk. Moreover, the ageing mechanism of ancient silk was proposed with the assistance of an artificial ageing study. The results confirmed the effectiveness of SR-XRD as an ageing indicator, revealing the crystallinity distribution. This research could provide motivation to determine the deterioration status of ancient silk, and would also aid in explaining the fragility of ancient silk due to ageing.

Effect of surface finishing treatments on the color stability of CAD/CAM materials

  • Ozen, Funda;Demirkol, Nermin;Oz, Ozge Parlar
    • The Journal of Advanced Prosthodontics
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    • 제12권3호
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    • pp.150-156
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    • 2020
  • PURPOSE. The aim of this study was to evaluate the effect of different surface finishing processes on the color stabilities of lithium disilicate glass-ceramics, zirconia-reinforced lithium silicate ceramics, and resin nanoceramics after artificial ageing. MATERIALS AND METHODS. 216 samples were prepared from 3 different CAD/CAM materials (LAVA Ultimate, IPS e.max CAD, VITA Suprinity) with A1 HT color at a size of 14 × 12 mm and a thickness of 0.5 ± 0.05 mm. Color measurements of the samples were performed with a spectrophotometer using color parameters and CIE Lab color system on a gray backing between baseline color and after 5000 cycles of artificial ageing in 4 stages (i.e. the first measurement before the treatment, the second measurement after polishing, the third measurement after cement application, and the fourth measurement after artificial ageing). The results were evaluated using the Variance analysis and Fisher's LSD test. RESULTS. Resin nanoceramics (LU) exhibited higher color change values than zirconia-reinforced lithium silicate (VS) and lithium disilicate (EC) ceramics after artificial ageing. Manual polishing and glazing resulted in similar color change for LU and VS (P>.05). In the EC group, glazing provided statistically different results as compared to the manual polishing and control groups (P<.05). Among the ceramic groups, color change values of the subgroup, which was treated by glazing, of the zirconia-reinforced lithium silicate (VS) and lithium disilicate (EC) samples were below the clinically acceptable level (ΔE < 3.5). CONCLUSION. The lowest color change for all stages was observed in Vita Suprinity.

중·고령층 고용변화 추이와 고용안정성이 탈빈곤에 미치는 영향 (Labor Transition of Middle-aged and Elderly and the Effects of Perceived Job Stability on Poverty Exit)

  • 강성호;조준용
    • 한국콘텐츠학회논문지
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    • 제16권2호
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    • pp.231-242
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    • 2016
  • 본 연구는 고령화연구패널조사(KLoSA)를 활용하여 중 고령층의 연령대에 따른 고용변화 특성을 종단적으로 분석하고, 고용안정성의 탈빈곤 효과를 추정하였다. 연구 결과 현재의 중 고령층은 조기퇴직 등으로 인해 50대 중반 이후 급격한 고용불안을 경험하며, 이후 재취업이 어려워 향후 노후소득보장 측면에서 위험이 큰 집단으로 나타났다. 특히 시간이 지날수록 중 고령층의 고용불안이 심화되고 있으며, 고령일수록 고용상 지위가 악화되는 것으로 나타났다. 로짓분석을 활용하여 중 고령층이 인지하는 고용안정성이 탈빈곤에 미치는 영향에 대해 분석한 결과, 65세 이상의 고령자보다 조기퇴직이 시작되는 55세 전후에서 경험하는 고용안정성이 가져오는 탈빈곤 효과가 큰 것으로 나타났다. 이는 퇴직 전에 충분한 노후준비를 갖추는 것이 무엇보다 중요함을 의미한다. 이러한 측면에서, 단계적인 정년 연장, 중 고령층에 대한 일자리 대책, 부처간 사업의 통합 및 일관성 확보, 연령 및 특성에 맞춘 맞춤형 고용-복지 연계제도의 도입에 대한 적극적인 정책적 고려가 필요하다.

송전선로에 사용되는 갭형 피뢰기 소자의 뇌임펄스 전류특성 (Characteristics of Lightning Impulse Current of Zno Block for Transmission Line Arrester with External Gap)

  • 조한구;유대훈
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2009년도 춘계학술대회 논문집
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    • pp.61-62
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    • 2009
  • This paper describes the characteristics of lightning impulse current of ZnO block for transmission line arrester with external gap. The ageing parameters of lightning arresters ate impulse current, moisture ingress, temperature ageing and so on. Especially it is important to estimate the change of electrical characteristics by impulse current. Total energy applied to the ZnO arrester each time is $4/10{\mu}s$, 30kA and $2/20{\mu}s$, 10kA impulse current. Before and After the test, the residual voltage variation of varistors passed was below 5%. According to the test, it is thought that the ZnO arrester shows good stability with impulse current test.

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송전선로에 사용되는 갭형 피뢰기 소자의 뇌임펄스 전류특성 (Characteristics of Lightning Impulse Current of ZnO Block for Transmission Line Arrester with External Gap)

  • 조한구;유대훈
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2007년도 하계학술대회 논문집 Vol.8
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    • pp.458-459
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    • 2007
  • This paper describes the characteristics of lightning impulse current of ZnO block for transmission line arrester with external gap. The ageing parameters of lightning arresters are impulse current, moisture ingress, temperature ageing and so on. Especially it is important to estimate the change of electrical characteristics by impulse current. Total energy applied to the ZnO arrester each time is $4/10{\mu}s$, 30kA and $2/20{\mu}s$, 10kA impulse current. Before and After the test, the residual voltage variation of varistors passed was below 5%. According to the test, it is thought that the ZnO arrester shows good stability with impulse current test.

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The Structural and Electrochemical Properties of Thermally Aged Li[Co0.1Ni0.15Li0.2Mn0.55]O2 Cathodes

  • Park, Yong-Joon;Lee, Ju-Wook;Lee, Young-Gi;Kim, Kwang-Man;Kang, Man-Gu;Lee, Young-Il
    • Bulletin of the Korean Chemical Society
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    • 제28권12호
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    • pp.2226-2230
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    • 2007
  • As a cathode material of lithium rechargeable batteries, charged Li[Co0.1Ni0.15Li0.2Mn0.55]O2 electrodes, which were aged thermally at 25 oC and 90 oC respectively, were characterized by means of charge/discharger, impedance spectroscopy, and X-ray diffraction. The discharge capacity diminution of the electrodes aged at 25 oC and 90 oC for 1 week was 4% and 23%, respectively. The cell aged at 25 oC was recovered on cycling. However, the capacity loss after ageing at 90 oC was not recovered in a subsequent cycling test, which demonstrates that the reaction occurring during ageing at 90 oC is irreversible. A significant impedance increase of aged electrode at 90 oC is associated with irreversible capacity loss. The structural changes including phase transformation were not detected by XRD analysis, because it could be due to out of detection limit. After ageing, impedance was slightly decreased during subsequent cycling test. It could be explained the cyclic performance of aged sample is stable. The thermal stability was not deteriorated by ageing even at the high temperature of 90 oC.

은퇴 전후 세대 재정안정성 -노년기 삶의 수준에 대한 기대와 지원- (The Financial Stability of Before-and-after Retirement -Expectation and Support for the Quality of the Elderly Life-)

  • 김은영
    • 한국사회복지학
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    • 제66권1호
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    • pp.61-85
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    • 2014
  • 최근 들어 노인 빈곤층문제가 심각한 사회적 이슈로 대두됨에 따라, 중장년층 은퇴 전후 세대들의 소득과 소비를 중심으로 재정안정성 문제를 살펴보았다. '고령화연구패널조사'자료를 활용하여, 은퇴자그룹과 비은퇴자그룹을 나누고, 연령별 차이를 비교 분석하였다. 연구의 주요결과는 다음과 같다. 첫째, 은퇴자그룹의 개인총소득은 비은퇴자그룹의 개인총소득에 비해 소득이 3배 이상 낮았다. 둘째, '공적연금소득' 수급비율은 은퇴자그룹은 전체의 30%에 불과하고, 공적연금의 비중은 개인총소득의 40% 이하로 나타났다. '개인연금소득'은 두 그룹 모두 수급비율이 1%내외로 매우 낮은 것으로 조사되었고, 은퇴자그룹에서는 '사적이전소득'이 전체소득에서 차지하는 비중이 크다는 것을 확인하였다. 셋째, 소득이 줄어든 만큼 소비는 은퇴를 하더라도 크게 줄지 않기 때문에, 연령이 증가함에 따라 재정안정성이 낮아지는 것으로 나타났다. 넷째, 국가로부터의 노후생활 지원에 대한 기대감은 양 그룹 모두 낮은 것으로 조사되었다. 다섯째, 은퇴자그룹의 공적연금소득에 미치는 영향요인을 비은퇴자그룹 개인 총소득에 미치는 주요 요인과 비교한 결과, 성별, 연령, 학력, 건강상태가 주요 요인으로 나타났다. 본 연구는 은퇴 전후 세대의 노후소득보장을 위한 정부차원에서의 공적연금 확대와 개인연금 활성화 지원의 필요성을 제안한 점에서 기여도가 있다.

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Oxidation Stability and Antioxidant Capacity of Lubricants Measured by a Pressure DSC

  • Cerny, Jaroslav
    • 한국윤활학회:학술대회논문집
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    • 한국윤활학회 2002년도 proceedings of the second asia international conference on tribology
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    • pp.359-360
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    • 2002
  • A methodology was developed for evaluation of oxidation stability of base stocks and engine oils. Analytical procedures for both classes of lubricants were based on the ASTM standards D 6186 and/or E 2009. The procedures were applied to a set of engine oils of the SAE 5W-30 specification, and to a set of several hydrocracked and solvent neutral base oils, both with and without addition of antioxidant. A potential of a pressure DSC for diagnostic purposed was also demonstrated by monitoring the engine oil ageing during its operation in heavy-duty engine.

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