• Journal of Powder Materials
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• v.26 no.4
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• pp.305-310
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• 2019

In the present work, spheroidization of angular vanadium powders using a radio frequency (RF) thermal plasma process is investigated. Initially, angular vanadium powders are spheroidized successfully at an average particle size of $100{\mu}m$ using the RF-plasma process. It is difficult to avoid oxide layer formation on the surface of vanadium powder during the RF-plasma process. Titanium/vanadium/stainless steel functionally graded materials are manufactured with vanadium as the interlayer. Vanadium intermediate layers are deposited using both angular and spheroidized vanadium powders. Then, 17-4PH stainless steel is successfully deposited on the vanadium interlayer made from the angular powder. However, on the surface of the vanadium interlayer made from the spheroidized powder, delamination of 17-4PH occurs during deposition. The main cause of this phenomenon is presumed to be the high thickness of the vanadium interlayer and the relatively high level of surface oxidation of the interlayer.

• Mass Spectrometry Letters
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• v.11 no.4
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• pp.77-81
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• 2020

Characterization of the various chemical aspects of composite polymers is important for quality control of manufactured polymers. In this study, we compared three suitable matrices (α cyano-4-hydroxycinnamic acid [CHCA], 2,5 dihydroxy benzoic acid [2,5-DHB], and dithranol), to characterize various synthetic polymers by matrix-assisted laser desorption/ionization time-of-flight mass spectrometry. Although the spectra obtained with the CHCA and 2,5-DHB matrices were generally good, in certain samples ghost peaks disappeared only when dithranol was used as the matrix. Furthermore, we examined the use of sodium trifluoroacetate (NaTFA) as an additive to reduce interference by metals and copolymers in the spectra. In conclusion, appropriate selection of a matrix, according to the characteristics of the polymer, and the use of additives to improve sensitivity are important considerations for polymer analysis and development.

• Journal of Powder Materials
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• v.29 no.3
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• pp.233-239
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• 2022

Aluminum alloys are extensively employed in several industries, such as automobile, aerospace, and architecture, owing to their high specific strength and electrical and thermal conductivities. However, to meet the rising industrial demands, aluminum alloys must be designed with both excellent mechanical and thermal properties. Computer-aided alloy design is emerging as a technique for developing novel alloys to overcome these trade-off properties. Thus, the development of a new experimental method for designing alloys with high-throughput confirmation is gaining focus. A new approach that rapidly manufactures aluminum alloys with different compositions is required in the alloy design process. This study proposes a combined approach to rapidly investigate the relationship between the microstructure and properties of aluminum alloys using a direct energy deposition system with a dual-nozzle metal 3D printing process. Two types of aluminum alloy powders (Al-4.99Si-1.05Cu-0.47Mg and Al-7Mg) are employed for the 3D printing-based combined method. Nine types of Al-Si-Cu-Mg alloys are manufactured using the combined method, and the relationship between their microstructures and properties is examined.

• Journal of the Korean Society of Safety
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• v.37 no.6
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• pp.1-8
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• 2022

This study analyzed the characteristics of insulation resistance and operating time based on an accelerated degradation test of a low-voltage circuit breaker. The experimental sample used a molded case circuit breaker (MCCB) and an earth leakage circuit breaker (ELCB). After measuring the insulation resistance of the circuit breakers, the leakage current was affected by an external rather than an internal structure. Furthermore, the insulation resistance of the circuit breakers with accelerated degradation was measured using a Megger insulation tester. In the accelerated degradation test, aging times of five, ten, 15, and 20 years were applied according to a temperature derived using the Arrhenius equation. Circuit breakers with an equivalent life of ten, 15, and 20 years had increased insulation resistance compared to those with less degradation time. In particular, the circuit breaker with an equivalent life of ten years had the highest insulation resistance. Component analysis of the circuit breaker manufactured through an accelerated degradation test confirmed that the timing of the increase in insulation resistance and the time of additive loss were the same. Finally, after analyzing the operating time of the circuit breakers with degradation, it was confirmed that the MCCB did not change, but the ELCB breaker failed.

• Transactions of the Korean Society of Pressure Vessels and Piping
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• v.17 no.2
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• pp.75-82
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• 2021

The 3D printing technology is one of the fourth industrial revolution technology that drives innovation in the manufacturing process, and should be applied to nuclear industry for various purposes according to the manufacturing trend change. In nuclear industry, it can be applied to manufacture obsolete items and new designed parts in advanced reactors or small modular reactors (SMRs), replacing the traditional manufacturing technologies. A gate valve body was manufactured, which was obsolete in nuclear power plant, using DED(Directed Energy Deposition) metal 3D printing technology after restoring design characteristics including 3D design drawing by reverse engineering. The 3D printed valve body was assembled with commercial parts such as seat-ring, disk, stem, and actuator for performance test. For the valve assembly, including 3D printed valve body, several tests were performed, including pressure test, end-loading test, and seismic test according to KEPIC MGG and KEPIC MFC. In the pressure test, hydraulic pressure of 391kgf/cm² was applied to 3D printed valve body, and no leak was detected. Also the 3D printed valve assembly was performed well in end-loading and seismic tests.

• Journal of Powder Materials
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• v.30 no.3
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• pp.210-216
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• 2023

In this study, machine learning models are proposed to predict the Vickers hardness of AlSi10Mg alloys fabricated by laser powder bed fusion (LPBF). A total of 113 utilizable datasets were collected from the literature. The hyperparameters of the machine-learning models were adjusted to select an accurate predictive model. The random forest regression (RFR) model showed the best performance compared to support vector regression, artificial neural networks, and k-nearest neighbors. The variable importance and prediction mechanisms of the RFR were discussed by Shapley additive explanation (SHAP). Aging time had the greatest influence on the Vickers hardness, followed by solution time, solution temperature, layer thickness, scan speed, power, aging temperature, average particle size, and hatching distance. Detailed prediction mechanisms for RFR are analyzed using SHAP dependence plots.

• Journal of the Korean Society of Industry Convergence
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• v.27 no.2_2
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• pp.371-375
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• 2024

Epoxy resins are widely used in various fields due to their high adhesion, mechanical strength, and solvent resistance. However, as the volume decreases during the hardening process and the cooling process after hardening, stress is generated and when an external force is applied, the brittle material exhibits destruction behavior. To complement this, research has been conducted using inorganic nanofillers such as halloysite nanotube(HNT). HNT has a nanotube structure with the chemical formula of Al₂Si₂O₅(OH)₄·nH₂O and is a natural sediment of aluminosilicate. It has been used as additive to improve the mechanical properties of epoxy composites with exchange of amine group as a terminal functional group. In order to simplify complicated procedures of common wet method, a dry coating machine was designed and used for amine group exchange in previous research. In this study, they were applied as filler in epoxy composites, and mechanical properties such as tensile strength and flexural strength of composites were examined.

• Transactions of Materials Processing
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• v.33 no.4
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• pp.241-247
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• 2024

The triply periodic minimum surface (TPMS) shape with a complex geometry can easily manufactured from additive manufacturing processes. The TPMS shape has a high surface-to-volume ratio. In addition, the TPMS shape increases the possibility of the self-circulation when the fluid flows inside the TPMS structure. Due to these reason, the performance of the fluid flow filter can be greatly improved when the TPMS structure is applied to the filter. The aim of this paper is to investigate the influence of the design of the unit cell for TPMS on self-circulation characteristics of air using computational fluid dynamics (CFD). From the results of the CFD, the effects of the shape and the dimension of the unit cell for TPMS on the self-circulation pattern and the pressure difference are examined. Finally, a proper design of the TPMS is discussed from the viewpoint of self-circulation of air.

• Journal of the Korean Society for Heat Treatment
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• v.37 no.5
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• pp.237-246
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• 2024

In this study, hydrogen embrittlement was investigated for 316L stainless steel (SS316L) and CoCrFeNi medium-entropy alloy (MEA) fabricated by laser-powder bed fusion. The in-situ hydrogen charging tensile tests revealed that the reduction in ductility due to hydrogen was more significant in the CoCrFeNi MEA, compared to the SS316L. In the case of SS316L, hydrogen-assisted cracks (HACs) were observed mainly on the surface, whereas in CoCrFeNi, cracks were found not only at the edges but also in the central region. HACs analysis confirmed that transgranular (TG) cracks were predominant in SS316L, whereas only intergranular cracks were formed in the CoCrFeNi MEA. The difference in hydrogen embrittlement resistance between SS316L and CoCrFeNi was discussed in terms of the differences in deformation microstructure and hydrogen diffusivity, as investigated through electron channeling contrast imaging and nanoindentation.

• Archives of Metallurgy and Materials
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• v.66 no.3
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• pp.795-798
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• 2021

Molybdenum (Mo) is used to form a barrier layer for metal wiring in displays or semiconductor devices. Recently, researches have been continuously attempted to fabricate Mo sputtering targets through additive manufacturing. In this study, spherical Mo powders with an average particle size of about 37 um were manufactured by electrode induction melting gas atomization. Subsequently, Mo layer with a thickness of 0.25 mm was formed by direct energy deposition in which the scan speed was set as a variable. According to the change of the scan speed, pores or cracks were found in the Mo deposition layer. Mo layer deposited with scan speed of 600 mm/min has the hardness value of 324 Hv with a porosity of approximately 2%. We demonstrated that Mo layers with higher relative density and hardness can be formed with less effort through direct energy deposition compared to the conventional powder metallurgy.