• 한국염색가공학회지
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• 제11권3호
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• pp.15-22
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• 1999

This study investigated the mordanting effect of natural mordants such as camellia ash, bean chaff ash and pyrolignite of iron(Iron(II) Acetate) on silk fabrics dyed with green tea extracts. Experimental variables include the conditions of extraction and dyeing, and types of natural mordants. Inorganic ion contents In natural mordants were analysed by Induced Coupled Plasma Atomic Emission Spectrometer. In the ash Al, Fe, Si and Mn were in % unit, Cr and Ni were detected in ppm unit, and in the aqueous extracts of the ash all the metal ions were in ppm unit. On the other hand, fairly high content of Al(2.13% ) in camellia ash extract and Fe(7.91% ) in the aqueous extracts of pyrolignite iron were detected. The absorbance intensity of green tea extracts in UV-Visible spectrum increased with the temperature and time of extraction. The maximum absorption wavelength of the extracts appeared at 272.5nm and 210.5nm. The US values of silk fabrics dyed with green tea extracts were increased with temperature and time of dyeing. Surface color of silk fabric dyed with green tea extracts was 9.1YR, but it was changed from 7.9YR to 7.5YR by camellia ash extract and 7.4YR to 6.4YR by bean chaff ash extract with increase in mordant concentration. Pre-mordanted and post-mordanted fabrics with pyrolignite of iron were changed from 1.4YR to 1.1R and 7.2P to 4.2P, respectively.

• Composites Research
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• 제21권1호
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• pp.40-45
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• 2008

자동차용 유압브레이크 고무호스 어셈블리 제품은 자동차에 장착되어 실제로 사용 중에 가압, 굽힘, 비틀림, 열하중 등의 복합적인 스트레스를 받는다. 고무호스의 재질은 EPDM(ethylene-propylene diene monomer)고무와 PVA(polyvinyl acetate)섬유 보강층 그리고 중간고무로 NR(natural rubber)고무가 사용되고 있다. 고무호스 어셈블리 제품의 내구성과 파괴 메커니즘을 조사하기 위해 굽힘과 비틀림의 반복하중 사이클 수가 10만, 20만, 30만, 40만, 최종파열 사이클 수까지 되도록 시험하였다. 유압브레이크 고무호스의 초기크랙 발생을 알아보기 위해 제품 시험편을 다이아몬드 휠커터를 이용하여 수직 절단하여 폴리싱한 후 광학현미경과 주사형 전자현미경(SEM)으로 단면을 관찰하였다. 40만 사이클의 피로하중을 받은 시험편을 보면 외면고무와 PVA섬유 사이의 계면을 따라 길이 1mm의 층간분리가 일어났으며, 이러한 손상은 외면고무의 표피층으로 균열을 진전시켜 고무호스를 최종적으로 찢어지게 하는 것이다.

• 폴리머
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• 제37권1호
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• pp.52-60
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• 2013

셀룰로오스 아세테이트(CA) 섬유를 $Na_2CO_3$ 용액으로 가수분해하여 탈아세테이트 반응시키면 레이온 섬유로 전환된다. 이때 처리조건을 조절함으로써 표면만 가수분해시켜, 표면은 레이온 성분이고 내부는 CA 성분으로 된 sheath-core형 표면가수분해 CA(SH-CA) 섬유를 얻었다. 시료들의 가수분해는 FTIR 스펙트럼 및 WAXD 패턴으로 분석하였으며, CA 성분을 아세톤으로 용출시킨 시료들의 SEM 사진으로부터 sheath-core 구조를 확인하였다. 이 sheath-core 형태의 SH-CA 섬유로 된 벨벳 직물을 사용하여, 액정디스플레이(LCD)용 폴리이미드 배향막을 러빙시키고 편광 FTIR 스펙트럼으로 분석하여 이 SH-CA 섬유 벨벳직물이 LCD용 러빙포로 사용될 수 있음을 확인하였다.

• 한국염색가공학회지
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• 제17권5호
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• pp.26-36
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• 2005

This study was carried to evaluate mechanical characteristics of Poly(ethylene terephthalate) fabrics (by Kawabata evaluation system(KES)) which was systematically treated with $O_2$ low temperature plasma and chitosan acetate solution. Furthermore, surface structure was investigated by SEM, AFM, air permeability and wettability. Tensile energy(WT), shear rigidity(G) and surface roughness(MIU) properties calculated by KES-FB have increased with increasing plasma treatment time, while bending rigidity(G) and energy of compression(WC) value were decreased compared with those of the untreated. SEM photographs showed the identification of chitosan coating but did not confirm the plasma etching structure. Air permeability was decreased according to plasma treatment time with increasing concentrations of chitosan. The water absorption rate made rapid progress by chitosan treatment.

• 한국의류산업학회지
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• 제10권2호
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• pp.254-259
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• 2008

Poly(ethylene-co-vinylacetate)(EVA) microspheres were prepared by a thermally induced phase separation. The microsphere formation occurred by the nucleation and growth mechanism in the metastable region. The diluents used were toluene. The microsphere formation and growth was followed by the cloud point of the optical microscope measurement. The microsphere size, which was obtained by SEM observation and particle size analyzer, became decreased when the titanium dioxide($TiO_2$) concentration was higher. The deodorizing function of the prepared fabrics was studied by the determination of the decomposing capability for $NH_3$. The deodorant activity of these deodorizing fabrics was measured by chromogenic gas detector tubes. The deodorant activity of $NH_3$ increased with increasing $TiO_2$ concentration of EVA microsphere.

• 한국생활과학회지
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• 제21권5호
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• pp.989-1004
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• 2012

The purpose of this study was to investigate the characteristics of the pigment and the dyeability of juniperus chinensis needles, berry, bark and heartwood extracts using distilled water, methanol, normal butanol and ethyl acetate as a solvent. Ultraviolet-visible absorption spectrum bands of the extracts were measured at around 280nm to 320nm in all the solvent extracts. The maximum absorption wavelength was able to determine tannin. All the solvent extracts except for distilled water extracts were able to confirm the presence of chlorophyll. Infrared absorption spectra (FT-IR) of all parts of the extracts showed broad absorption bands of OH due to phenolic-OH, benzene CH peak of phenol chemical structure, ether-based stretching vibration peak and the peak of flavonoid compounds that appeared in all the solvent extracts. The yield of juniper needles and heartwood in distilled water and methanol extraction were effective. Extraction of berry yields in distilled water was also effective. The yield of ethanol extraction from the bark showed better efficiency. As a result of using distilled water for the dye solution, the color of the fabrics dyed with all extracts of the needles and Y series berries generally showed light Y progression with a strong red tinge. By using a mixture of 20% ethanol and 80% distilled water for the dye solution, the color of the fabrics dyed with needles and berry extracts showed Y series dominantly. The color of the fabrics dyed with Bark and heartwood extracts were dominantly R series.

• 한국염색가공학회지
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• 제7권4호
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• pp.87-96
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• 1995

Colorant concentrates are prepared by use of concentration method of colorants extracted from Sappan wood using met hanol. Dyeabilities and fastness properties of silk fabrics dyed with concentrate of Sappan wood are investigated.The results obtained are as follows; 1. The storage stability of colorant concentrate is poor as concentration is excess. 2. Because the colors of dyeings are different with mordants, aluminium acetate, copper acetate, chromium alum and tin chloride are used in order to obtain reddish color. 3. The optimum dyeing temperature and dyeing time are 6$0^{\circ}C$ and 60 min, respectively. 4. Dry cleaning fastness is very good, and light fastness and washing fastness are low. 5. The dyeing method is simple owing to usehess of colorant concentrate prepared without extraction of colorant every time.

• 한국의류학회지
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• 제37권4호
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• pp.506-513
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• 2013

Rubia cordifolia L (Indian madder) contains red color purpurin (65-67%) and yellow color munjistin (10-12%) as well as nordamncanthal (9-10%). Purpurin is a traditional red dye. The purpose of this research is to increase the dyeability of silk and light fastness of dyed silk fabric. We dyed silk fabrics after pretreatment to remove the yellow component of madder using various solvents such as ethyl acetate, ethanol, methanol, chloroform, and acetone. The total K/S value was the highest in the case of chloroform and reflectance was the lowest at the red color region from 470nm to 530nm. Chloroform dissolved the yellow color of Rubia cordifolia; in addition, we found that the total K/S value increased and the ${\Delta}E$ value decreased by chloroform pretreatment for silk dyeing.

• 한국염색가공학회지
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• 제33권3호
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• pp.97-104
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• 2021

In this study, the dyeability of m-aramid fabric with various cationic dyes using two bath two step dyeing method were investigated. The exhaustion properties of Doracryl series recommend for aramid(Doracryl^® Red GL 100%(DR), Doracryl^® Blue GL 300%(DB), Doracryl^® Yellow XGRL 200%(DY)) and commercial cationic Synocryl series(Synocryl^® Red GRL ED(SR), Synocryl^® Blue GSL ED(SB), Synocryl^® Yellow 3RL ED(SY)) for acrylic were measured by using Dye-O-meter. In the presence of carrier, the exhaustions of Doracryl series were higher to those of Synocryl series and the opposite phenomenon was observed in the absence of carrier. And the severe migrations of cationic dyes to acetate, nylon and wool fabrics were observed without carrier.

• 한국의류산업학회지
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• 제13권6호
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• pp.972-982
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• 2011

The purpose of this study is to improve the method of color developing with alkali solution as a promotor of color developing for feasible use. Cotton fabric was dyed with persimmon extract ranged with 0~3% alkali component with 5 types of strong to mild alkali solution. Heat treatment for color developing was applied to fabric dyed with persimmon extract and alkali mixing solution. Tests were carried out to analyze the change of surface color, ${\Delta},Ea^*b^*$, and water repellent of the dyed cotton fabric. The alkali mixing sample showed higher ${\Delta},Ea^*b^*$ value than control one without alkali mixing on the base of dyed fabric due to high color developing by alkali in the initial step of dyeing process. As alkali concentration increased, deeper dark color appeared on the fabric. The fabric color was changed to more dark in the application of sodium hydroxide, sodium carbonate, potassium carbonate in the initial step of dyeing process but color was not changed by increased heating time. However, the fabric showed a slight dark color with sodium acetate and more color change than that of the fabric dyed with persimmon extract without alkali. Therefore, sodium acetate seemed to a suitable promotor for color developing in persimmon extract dyeing. Property of water repellent was showed after color developing by heating with low concentration of alkali treatment.