• Proceedings of the Korean Society For Composite Materials Conference
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• 1999.11a
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• pp.160-163
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• 1999

The mechanical properties and failure behaviour of carbon/phenolic composites were inverstigated by tension and compression. Carbon/phenolic composites were fabricated by infiltration of matrix into 8 harness satin woven fabric of PAN-based carbon fibers. The tensile and compressive tests were performed at 25℃ under air atmosphere and, at 400℃ and 700℃ under N₂ atmosphere. The tensile strengths of carbon/phenolic composites in with-laminar/0° warp direction were about 10 times higher than those in with-laminar/45° warp direction, which was analyzed due to a change of fracture mode from fiber pull-out by shear to tensile fracture of fibers. The fracture of carbon/phenolic composites in with-laminar/45° direction was analyzed due to delamination by buckling. Tensile and compressive strength of carbon/phenolic composites decreased to about 50% at 400℃, and to about 10% at 700℃ compared to that at room temperature. The main reason for the decrease of tensile or compressive strength with increasing temperature was analyzed due to a reduction of bond strength between fibers and matrix resulting from thermal degradation of phenolic resin.

• Transactions of the Korean Society of Mechanical Engineers
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• v.16 no.5
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• pp.943-951
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• 1992

The objectives of this study are to analyse the thermal response behavior occurring in the charring ablative material more realistically by considering ablation and char phenomena occurring in several material layers, and to increase the reliability of thermal analysis by being able to get stable solutions through using the finite analytic method. A program has been developed to predict the temperature distribution, ablation thickness, char thickness, ablation velocity and char velocity by solving non-linear one-dimensional heat conduction equation. Results of calculation were compared with results of published papers. From this compariosn this program was proved to be a very good tool for thermal design and analysis of charring ablative materials used in the rocket propulsion system.

• Applied Chemistry for Engineering
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• v.18 no.3
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• pp.227-233
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• 2007

Carbon/carbon (C/C) composites as unique materials possess exceptional thermal resistance with light weight, high stiffness, and strength even at high temperature. However, one serious obstacle for application of the C/C composites is their poor oxidation resistance in high temperature oxidizing environments. SiC coating has been employed to protect the composites from oxidation. This study explored combustion characteristics of 4-directional (4D) carbon/carbon composites using liquid fuel rocket engine to investigate ablative motion of the materials. C/C composites were made of coal tar pitch as a matrix precursor, and heat-treated at $2300^{\circ}C$. Throughout repeated densification process, the density of the material reached $1.903g/cm^3$. After machining 4D C/C composites, the nozzle surface was coated by a SiC layer by pack-cementation method to improve oxidation resistance. Erosion characteristics of SiC-coated C/C composites were measured as function of the ratio of oxygen to fuel. The morphological change of the composites after combustion test was investigated using SEM and erosion mechanism also was discussed.

• Current Industrial and Technological Trends in Aerospace
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• v.9 no.1
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• pp.139-149
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• 2011

The combustion chamber and nozzle of a liquid rocket engine need thermal protection against the high temperature combustion gas. The nozzle extension of a high-altitude engine also has to be compatible with high temperature environment and several kinds of cooling methods including gas film cooling, ablative cooling and radiative cooling are used. Especially for an upper-stage nozzle extension having a large expansion ratio, the weight impact on the launcher performance is crucial and it necessitated the development of light-weight refractory material. The present survey on the nozzle extension materials employed in the liquid rocket engines of USA, Russia and European Union has revealed a trend that the heavier metals like stainless steels and titanium alloys are being substituted with light weight carbon fiber or ceramic matrix composite materials.

• Journal of the Korean Society of Propulsion Engineers
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• v.4 no.3
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• pp.38-44
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• 2000

In general liquid rocket nozzles are protected from hot combustion gas by regenerative cooling techniques. But due to the complexity of the cooling system, it causes increase of system cost and frequently source of the system malfunction. Recently, instead of regenerative cooing, ablative material are used to protect combustion chamber wall and nozzle. To determine the nozzle material erosion rate and erosion shape, more than 500 hot fire test were performed by using 100 lb thrust experimental liquid rocket. Test variable were propellant feed sequence, injector, position of igniter and liquid oxygen supply temperature.

• Aerospace Engineering and Technology
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• v.4 no.2
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• pp.135-141
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• 2005

The procedure of conceptual and detailed design of sub-scale combustor using bipropellant swirl or impinging injector with external or internal mixing for a liquid rocket engine are described in this paper. The sub-scale combustor uses liquid oxygen(LOx) and kerosene as propellants and has a injector head, an ablative material combustor wall and a water cooled nozzle. The injector head has LOx manifold, fuel manifold, fire face plate, one center swirl or impinging injector and 18 main swirl or impinging injectors.

• Proceedings of the Korean Society of Propulsion Engineers Conference
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• 2005.11a
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• pp.335-340
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• 2005

A study on the variation of combustion characteristics by injector geometries was conducted. Coaxial swirl injectors were used. Existence of swirl chamber and variation of a nozzle length become key parameters. Injectors were identified as open, closed and mixed type by existence of swirl chamber. Variation of nozzle length was made extruding the both nozzle along the axis while other design parameters remain the same. A uni-element combustor with ablative material liner and a water cooled nozzle made by oxygen free copper with outer stainless steel casing were used.

• Macromolecular Research
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• v.12 no.1
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• pp.134-140
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• 2004

Semi-crystalline poly(ethylene terephthalate) (PET) film surfaces were modified with argon and oxygen plasmas by radio-frequency (RF) glow discharge at 240 mTorr/40 W; the changes in topography and surface structure were investigated by atomic force microscopy (AFM) in conjunction with specular reflectance of infrared microspectroscopy (IMS). Under our operating conditions, analysis of the AFM images revealed that longer plasma treatment results in significant ablation on the film surface with increasing roughness, regardless of the kind of plasma used. The basic topographies, however, were different depending upon the kind of gas used. The specular reflectance analysis showed that the ablative mechanisms of the argon and oxygen plasma treatments are entirely different with one another. For the Ar-plasma-treated PET surface, no observable difference in the chemical structure was observed before and after plasma treatment. On the other hand, the oxygen-plasma-treated PET surface displays a significant decrease in the number of aliphatic C-H groups. We conclude that a constant removal of material from the PET surface occurs when using the Ar-plasma, whereas preferential etching of aliphatic C-H groups, with respect to, e.g. , carbonyl and ether groups, occurs upon oxygen plasma.

• Journal of the Korean Society for Aeronautical & Space Sciences
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• v.32 no.10
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• pp.102-111
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• 2004

The procedure of design and manufacture of sub-scale combustor using bipropellant swirl injector with external mixing for a liquid rocket engine are described. The results of cold flow test, ignition test and combustion test of the sub-scale combustor are also given in this paper. The sub-scale combustor uses liquid oxygen(LOx) and kerosene as propellants and has a injector head, an ablative material combustor wall and a water cooled nozzle. The injector head has LOx manifold, fuel manifold, fire face plate, one center swirl injector and 18 main swirl injectors. The cold flow, ignition and combustion tests were successfully performed without damage of combustor. Results of hot firing tests show that combustion efficiency meets the target of design and operations of start and stop cyclogram are stable and high frequency combustion instability does not occur.

• Journal of the Korean Society for Aeronautical & Space Sciences
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• v.32 no.4
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• pp.80-87
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• 2004

To understand the each performance parameter correlation of flight type liquid-propellant rocket engine for KSR-III(Korea Sounding Rocket-III), the analysis of engine stand-alone combustion test results was carried out. Considering the variation of ablative material combustion chamber caused by erosion, linear regression analysis that ignores oxidizer/fuel ratio effect and two-variable 2nd-order polynomial regression analysis that considers oxidizer/fuel ratio change were performed. It can be described that linear regression analysis is simple and very practical method, and can predict the performance within 1% error inside analyzed region. And two-variable 2nd-order polynomial regression analysis can predict with very high accuracy inside region and shows that KSR-III engine's optimum oxidizer/fuel ratio for thrust(or specific impulse) is 2.22 and that for combustion chamber pressure(or characteristic velocity) is 2.17.