• Title/Summary/Keyword: Zone-melting

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The effects of the microstructure of the feed rod of $SrTiO_{3}$ on the melting stability ($SrTiO_{3}$ 원료봉의 미세구조가 용융대 안정에 미치는 영향)

  • Cho, Hyun;Shim, Kwang-Bo;Auh, Keun-Ho
    • Journal of the Korean Crystal Growth and Crystal Technology
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    • v.6 no.2
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    • pp.247-253
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    • 1996
  • Microscopic analysis has been performed in order to investigate effects of the microstructure of the starting feed rods on the morphology of the S-L interface and the stability of the molten zone during single crystal growth of $SrTiO_{3}$ using a floating zone method. Undoped and $Fe_{2}O_{3}$ doped $SrTiO_{3}$ doped $SrTiO_{3}$ specimens, sintered at the different temperatures have been used. In the case of the feed rods sintered at the lower temperature($1400^{\circ}C$), the poor densification made the stability of the molten zone difficult to maintain. The feed rods sintered at the higher temperature ($1600^{\circ}C$) exhibited the higher density but their molten zone was difficult to maintain due to the presence of the abnormally grown grains. It is concluded that the uniform grain size distribution of the feed rod is the critical factor to maintain the stable molten zone and therefore to give optimum growth condition during FZ single crystal growth.

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Petrochmical study on the Volcanic Rocks Related to Depth to the Benioff Zone and Crustal Thickness in the Kyongsang Basin, Korea: A Review (경상분지 화산암류의 지화학적 연구. 섭입대(베니오프대)의 깊이와 지각의 두께)

  • Jong Gyu Sung
    • Economic and Environmental Geology
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    • v.32 no.4
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    • pp.323-337
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    • 1999
  • Late Cretaceous to early Tertiary volcanic rocks in the Kyongsang basin exhibit high-K calc-alkaline characteristics, and originated from the magmatism related genetically to subduction of Kula-Pacific plate. They represent HFSE depletion and LlLE enrichment characteristics as shown by magmas related to subduction. Early studies on the depth of magma generation has been estimated as 180-230 km based on K-h relation should be reevaluated, because the depth of peridotite partial melting with 0.4 wt. % water is 80-120 km at subduction zone, and subducting slab in premature arc can melted even lower than 70 km. Moreover the increase of potassium contents depends on either contamination of crustal material and fluids of subducting slab or low degree of partial melting. If the inclination of subduction zone is 30 degrees and the depth to the Benioff zone is 180-230 km, the calculated distance between the volcanic zone and trench axis would be 310-400 km. It is unlikely because the distance between the Kyongsang basin and trench during late Cretaceous to early Tertiary is closer than this value and not comparable with generally-accepted models in subduction zone magmatism. $K_{55}$ of the volcanics in the Kyongsang basin is 0.3-2.3 wt.% and the average indicate that the depth ranges between 80-170 km on the diagram of Marsh, Carmichael (1974). Fractionation from garnet lherzolite, assumed the depth of 180-230km, is not consistent with the REE patterns of the volcanoes in the Kyongsang basin. Futhermore, the range of depth suggested by many workers, who studied magmatism related to subduction, imply shallower than this depth. Crustal thickness calculated by the content of CaO and $Na_2O$ is about 30 km and about 35 km, respectively. Paleo-crustal thickness during late Cretaceous to early Tertiary times in the Kyongsang basin inferred about 30 km calculated by La/Sm versus LaJYb data, which is also supported by many previous studies.

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PETROGEOCHEMISTRY OF THE GRANITIC ROCKS DISTRIBUTED IN IMGYE AND SAMHWA AREA, KANGWEON-DO (강원도 임계 및 삼화지역에 분포하는 화강암류에 대한 암석지구화학)

  • MIN, KYOUNG WON;KIM, SUNG BUM
    • Journal of Industrial Technology
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    • v.10
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    • pp.33-48
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    • 1990
  • The Imgye and the Samhwa granitoids distributed in the northeastern part of the Okchon Zone are known to be emplaced during the Mesozoic time. These granitoids intruded the Precambrian metasedimentary bedrocks and Cambro-ordovician sedimentary rocks. Petrographically the Samhwa granitoid is a biotite granite of mainly coars-grained texture with some fine-grained exceptions and the Imgye granitoid contains typically large phenocrysts of pinkish K-feldspars. Geochemical discriminators in terms of major elements suggest that the Samhwa and the Imgye granitoids are I-type and magnetite series. These granitoids are also classified as calc-alkalic rocks of subalkalic series. The Imgye and the Samhwa granitoids could have been evolved mainly by fractional crystallization and minimum partial melting respectively.

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Liquid Phase Diffusion Bonding Procedure of Rene80/B/Rene80 System -Liquid Phase Diffusion Bonding Using B Powder Coating Method (Rene80/B/Rene80계의 액상확산 접합과정 -B분말 도포법을 이용한 액상확산접합)

  • 정재필;강춘식
    • Journal of Welding and Joining
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    • v.13 no.2
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    • pp.132-138
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    • 1995
  • Rene80 superalloy was liquid phase diffusion bonded by using boron(B) as an insert material, where B has high diffusivity and higher melting point as an insert material. Bonding procedure and bonding mechanism of Rene80/B/Rene80 joint were investigated. As results, liquid metal was produced by solid state reaction between base metal and insert material on bonding zone. The liquid metal was produced preferentially at the grain boundary. Except for production of liquid metal, other bonding procedure was nearly same as TLP(Transient Liquid Phase) bonding. Bonding time, however, was reduced compared to prior result of TLP bonding. By bonding S.4ks at l453K, Ren80/B/Rene80 joint was isothermally solidified and homogenized where thickness of insert material was 7.5.mu.m.

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Pulsed laser surface modification for heat treatment and nano-texturing on biometal surface

  • Jeon, Hojeong
    • Proceedings of the Korean Institute of Surface Engineering Conference
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    • 2016.11a
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    • pp.118.1-118.1
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    • 2016
  • The laser surface modification has been reported for its functional applications for improving tribological performance, wear resistance, hardness, and corrosion property. In most of these applications, continuous wave lasers and pulsed lasers were used for surface melting, cladding, alloying. Since flexibility in processing, refinement of microstructure and controlling the surface properties, technology utilizing lasers has been used in a number of fields. Especially, femtosecond laser has great benefits compared with other lasers because its pulsed width is much shorter than characteristic time of thermal diffusion, which leads to diminish heat affected zone. Moreover, laser surface engineering has been highlighted as an effective tool for micro/nano structuring of materials in the bio application field. In this study, we applied femtosecond and nanosecond pulsed laser to treat biometals, such as Mg, Mg alloy, and NiTi alloy, by heating to improve corrosion properties and functionalize their surface controlling cell response as implantable biomedical devices.

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A suggestion of the SOI MOSFET device with buried island structure (매몰된 island 구조를 갖는 SOI MOSFET 소자의 제안)

  • Lee, Ho-Jun;Kim, Choong-Ki
    • Proceedings of the KIEE Conference
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    • 1992.07b
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    • pp.806-808
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    • 1992
  • This paper describes a buried-island SOI MOSFET structure which can reduce the edge channel effect by improving the interface properties at the side wall of active island and by reducing the strength of electric field applied at the upper corner of the side wall from the gate. Also, the buried-island SOl structure can obtain the uniform thickness of SOl film. The buried-island structure can be achieved by Zone- Melting-Recrystallization of polysilicon and polishing. Both simulated and experimental results show that the buried-island SOl NMOSFET has less edge channel effect than the conventional SOl NMOSFET using LOCOS or mesa isolation technique.

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Microscopic Study on the Laser Surface-Melted Alloy 600

  • Lim, Yun-Soo;Cho, Hai-Dong;Kuk, Il-Hiun;Kim, Joung-Soo
    • Proceedings of the Korean Nuclear Society Conference
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    • 1996.05c
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    • pp.347-352
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    • 1996
  • Studies on tile microstructural and compositional changes in sensitized Ni base Alloy 600 by laser surface melting have been carried out using TEM equipped with EDXA. The microstructure of the laser melted zone was mainly consisted of fine cells, and along the cell and grain boundaries, Cr enrichment due to its segregation was observed. Cr carbides having formed along the grain bundaries during the sensitization treatment have been completely dissloved. The cell walls were decorated with dislocations and the very tiny precipitates, found to be Ti(CN) type, were distributed randomly along the cell walls with tangled dislocations around them.

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Electrical Properties of Single Crystal CdTe by Impurity (불순물에 의한 CdTe단결정의 전기적 특성)

  • 박창엽
    • 전기의세계
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    • v.20 no.2
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    • pp.9-14
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    • 1971
  • N type single crystal CdTe is grown by doping Gallium as 0.01 percent, by using zone melting method. And also p type CdTe is grown by doping Ag, Sb, and Te as 0.01%. Resistivity and Concentration of the n.p type single crystal are measured. And then Li ions are implanted on the n type CdTe by high voltage accellerator with different amount of impurity. Indium is evaporated on the p type in high vacuum condition. These sample are heated so as to make P-N Junction in Argon gas flow. Electrical properties for solar cell are investigated. Photovoltage and current are found to be varyed according to following factor: 1) amount of impurity 2) diffusion thickness 3) temperature and time for making P-N junction. Efficiency of the P-N Junction evaporated Indium is 6.5 when it is heated at 380.deg. C for 15 minutie.

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CFRP Laser Joining Computer Simulation in a Parallel Kinematic Machine (병렬가공기계용 CFRP의 레이저 용접특성 시뮬레이션)

  • Lee, Seung-Taek;Park, Seung-Gyu;Choi, Hae-Woon
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.16 no.1
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    • pp.77-82
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    • 2017
  • A computer simulation method is introduced to understand the joining phenomena of PC and CFRP by estimating the temperature of the weld zone. Following the prior or preliminary research, the power range was set between 3 watts and 7 watts, and the scanning speed was set at 500 mm/min and 1,000 mm/min, respectively. Based on the computer simulation, the temperature near the joining boundary was not sufficient at the scanning speed of 1,000 mm/min, regardless of the selected powers. However, the temperature increases above the melting temperature of the selected polymers at the scanning speed of 500 mm/min. The simulation results were compared with actual weld samples to validate its actual use.

Microstructures and Hardness of Al-Si Coated 11%Cr Ferritic Stainless Steel, 409L GTA Welds (Al-Si 용융도금된 11%Cr 페라이트 스테인리스강, STS409L GTA 용접부의 미세조직과 경도)

  • Park, Tae-Jun;Kong, Jong-Pan;Na, Hye-Sung;Kang, Chung-Yun;Uhm, Sang-Ho;Kim, Jeong-Kil;Woo, In-Su;Lee, Jong-Sub
    • Journal of Welding and Joining
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    • v.28 no.3
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    • pp.92-98
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    • 2010
  • Ferritic stainless steels, which have relatively small thermal expansion coefficient and excellent corrosion resistance, are increasingly being used in vehicle manufacturing, in order to increase the lifetime of exhaust manifold parts. But, there are limits on use because of the problem related to cosmetic resistance, corrosions of condensation and high temperature salt etc. So, Aluminum-coated stainless steel instead of ferritic stainless steel are utilized in these parts due to the improved properties. In this investigation, Al-8wt% Si alloy coated 409L ferritic stainless steel was used as the base metal during Gas Tungsten Arc(GTA) welding. The effects of coated layer on the microstructure and hardness were investigated. Full penetration was obtained, when the welding current was higher than 90A and the welding speed was lower than 0.52m/min. Grain size was the largest in fusion zone and decreased from near HAZ to base metal. As welding speed increased, grain size of fusion zone decreased, and there was no big change in HAZ. Hardness had a peak value in the fusion zone and decreased from the bond line to the base metal. The highest hardness in the fusion zone resulted from the fine re-precipitation of the coarse TiN and Ti(C, N) existed in the base metal during melting and solidification process and the presence of fine $Al_2O_3$ and $SiO_2$ formed by the migration of the elements, Al and Si, from the melted coating layer into the fusion zone.