• Title/Summary/Keyword: X8

Search Result 8,976, Processing Time 0.034 seconds

Electrochemical Oxidation of Silver (I) Salt (Ag(I) 염의 전해산화)

  • Duk Mook Kim
    • Journal of the Korean Chemical Society
    • /
    • v.29 no.2
    • /
    • pp.158-163
    • /
    • 1985
  • The anodic oxidations of the Silver(I) / Silver(II) / Silver(III) system have been studied in aq. 2M $AgNO_3$ solution with Platinum and Carbon electrodes. It has been found that $Ag_7O_8NO_3$ can be produced at relatively higher current density. Deposited black Oxy-salt were analyzed with several methods such as oxidizing power, X-ray powder diffraction patterns, thermal analysis, and reduction curves. It decomposed to AgO upon being suspended in boiling water. AgO compound obtained from $Ag_7O_8NO_3$ were purer and denser than Alfa-product AgO.

  • PDF

Crystal Structure Analysis of 3-(4-ethylphenyl)-3H-chromeno[4,3-c]isoxazole-3a(4H)-carbonitrile

  • Malathy, P.;Ganapathy, Jagadeesan;Srinivasan, J.;Manickam, Bakthadoss
    • Journal of Integrative Natural Science
    • /
    • v.8 no.4
    • /
    • pp.250-257
    • /
    • 2015
  • The crystal structure of the potential active 3-(4-ethylphenyl)-3H-chromeno[4,3-c]isoxazole-3a(4H)-carbonitrile ($C_{19}H_{16}N_2O_2$) has been determined from single crystal X-ray diffraction data. In the title compound crystallizes in the monoclinic space group $P2_1/c$ with unit cell dimension a=6.6869 (8) ${\AA}$, b=15.8326 (19) ${\AA}$ and c= 15.237 (2) ${\AA}$ [${\alpha}=90^{\circ}$, ${\beta}=100.663^{\circ}$ and ${\gamma}=90^{\circ}$]. In the structure chromene, isoxazole and carboxylate are almost coplanar each other. All geometrical parameters revelled that chromene ring of pyran ring adopt sofa conformation. The crystal packing is stabilized by intermolecular C-H...N and C-H...O hydrogen bond interaction.

A Study on the Characteristics of Sn-Ag-X Solder Joint (Sn-Ag-X계 무연솔더 접합부의 미세조직 및 전단강도에 관한 연구)

  • 김문일;문준권;정재필
    • Journal of Welding and Joining
    • /
    • v.20 no.2
    • /
    • pp.77-81
    • /
    • 2002
  • Many kinds of Pb-free solder have been investigated because of the environmental concerns. Sn-Ag-Cu system is well blown as most competitive Pb-free solder. However, since Sn-Ag-Cu system has relatively high melting point compared to Sn-Pb eutectic, it may a limitation, the some application. In this study, Bi and In contained solder of $Sn_3Ag_8Bi_5In$ which has relatively lower melting point, $188~204^{\circ}C$, was investigated. $Sn_3Ag_8Bi_5In$ solder ball of $500\mu\textrm{m}$ diameter was set on the Ni/Cu/Cr-UBM and reflow soldered in the range of $220~240^{\circ}C$ for 5~15s. The maximum shear strength of the solder ball was around 170mN by reflowing at $240^{\circ}C$ for 10s. Intermetallic compound formed on the UBM of Si-wafer was analysed by SEM(scanning electron microscope) and XRD(X-ray diffractometer).

A Study on the Gasification of Combustible Waste (가연성 폐기물의 가스화에 관한 연구)

  • 정준화
    • Journal of Environmental Health Sciences
    • /
    • v.16 no.2
    • /
    • pp.89-95
    • /
    • 1990
  • This study was investigated to the energy recovery by the pyrolysis of waste tyre. the pyrolysis of the waste tyre was made by using the pyrolysis chamber for the gasification and the combustion chamber for the combustion of the pyrolysis gas. In batch system, the amount of waste tyre was put 150kg in the pyrolysis chamber and the proper air flow rate for the stable production of the pyrolysis gas was 0.95Nm$^{3}$ /min. the production time of the pyrolysis gas was stable above 210minutes, and the stable production rate was above 3.8Nm$^{3}$ /min. The production temperature of pyrolysis gas was 170$^{\circ}$C and combustion temperature of pyrolysis gas was 1,000$^{\circ}$C. The combustible component of washing gas in pyrolysis gas of waste tyre was CO, CH$_{4}$, $C_{2}H_{6}$ and $C_{3}H_{8}$, and total amount was 22.7%. Heat value of condensed material was 9,804Kcal/kg. The average concentration of air pollutants between cyclone and scrubber was CO 420.4ppm, SO$_{x}$ 349.8ppm. NO$_{x}$ 68.Sppm, HCl 24.4ppm and Dust 240.0g / Nm$^{3}$, respectively.

  • PDF

Electro Optic Characteristics of PLZT Ceramics Fabricated by Two Stage Sintering Method (2단소성방법으로 제조한 PLZT 세라믹의 전기광학 특성)

  • 박창엽;강원구;위규진;정익채
    • Journal of the Korean Ceramic Society
    • /
    • v.24 no.6
    • /
    • pp.527-536
    • /
    • 1987
  • PLZT ceramics of composition La/Zr/Ti=X/65/35(X=5-10 at.%) were fabricated by two state sintering technique.Transparent PLZT ceramics were obtained in the composition above 8 at. % La. Variations of electrooptic properties in the compositions between 8 at. % and 9 at. % La were able to be expected from the significant differences of P-E hysteresis curve and the changes of dielectric phase transition. The range of birefringence of 8/65/35 specimen was 4.08${\times}$10-3. Domain switching of 9/65/35 specimen was agreed with the applied electric pulse because input pulse signal corresponds to optical pulse response.

  • PDF

MINIMAL QUADRATIC RESIDUE CYCLIC CODES OF LENGTH $2^{n}$

  • BATRA SUDHIR;ARORA S. K.
    • Journal of applied mathematics & informatics
    • /
    • v.18 no.1_2
    • /
    • pp.25-43
    • /
    • 2005
  • Let F be a finite field of prime power order q(odd) and the multiplicative order of q modulo $2^{n}\;(n>1)\;be\; {\phi}(2^{n})/2$. If n > 3, then q is odd number(prime or prime power) of the form $8m{\pm}3$. If q = 8m - 3, then the ring $R_{2^n} = F[x]/ < x^{2^n}-1 >$ has 2n primitive idempotents. The explicit expressions for these primitive idempotents are obtained and the minimal QR cyclic codes of length $2^{n}$ generated by these idempotents are completely described. If q = 8m + 3 then the expressions for the 2n - 1 primitive idempotents of $R_{2^n}$ are obtained. The generating polynomials and the upper bounds of the minimum distance of minimal QR cyclic codes generated by these 2n-1 idempotents are also obtained. The case n = 2,3 is dealt separately.

Fluxon resonance steps in the $Bi_2Sr_2CaCu_2O_{8+x}$ single crystals

  • Bae, Myung-Ho;Lee, Hu-Jong
    • Progress in Superconductivity
    • /
    • v.8 no.2
    • /
    • pp.138-142
    • /
    • 2007
  • We observed discrete fluxon-flow resonance steps in high magnetic fields in a stack of Josephson junctions with lateral size of $1.5{\times}17{\mu}m^2$. The measurement sample was prepared by sandwiching a stack of $Bi_2Sr_2CaCu_2O_{8+x}$ intrinsic Josephson junctions between two Au electrodes by using the double-side-cleaving technique. This technique allowed us to isolate the intrinsic Josephson junction structures from the inductive interference of the basal stack. The resonance steps observed are in good agreement with the collective Josephson fluxon dynamics that are in resonance with the plasma oscillation modes inside the stacked Josephson junctions.

  • PDF

Mechanical Properties of W-X (X=Cu, Ag or BAg-8) Composites

  • Hanado, H.;Hiraoka, Y.;Inoue, T.;Akiyoshi, N.
    • Proceedings of the Korean Powder Metallurgy Institute Conference
    • /
    • 2006.09b
    • /
    • pp.1054-1055
    • /
    • 2006
  • Bend tests were performed at temperatures between 77 and 473K for W-19vol%Cu, W-22vol%Ag and W-19vol%(BAg-8) composites. Yield and maximum strengths and ductility of the composite were discussed in terms of microstructure and fractography. Results are summarized as follows. (1) Almost no difference was recognized in yield strength between the composites. In contrast, a large difference was recognized in maximum strength and ductility between the composites. (2) Inferior mechanical properties of W-Ag composite to W-Cu composite are attributed to heterogeneous distribution of Ag-phases, whilst inferior mechanical properties of W-(BAg-8) composite to W-Cu composite are attributed to large pores at grain boundaries.

  • PDF

Pairing symmetry analyzed by a peak shape of density of states in an Bi2Sr2CaCu2O8+x superconductor

  • Kim, Hyun-Tak;Kang, Kwang-Yong
    • Proceedings of the Korea Institute of Applied Superconductivity and Cryogenics Conference
    • /
    • 2003.10a
    • /
    • pp.30-34
    • /
    • 2003
  • For an inhomogeneous superconductor, we reveal a relation of an observed superconducting gap, $\Delta$$_{obs}$ and the intrinsic true gap, $\Delta$$_{i}$, $\Delta$$_{obs}$(equation omitted) where band filling, 0<$\rho$<$\leq$1. $\Delta$$_{obs}$ is the effect of measurement when 0<$\rho$<1. The true gap is observed only when $\rho$=1. Parring symmetry analyzed by a coherence-peak shape of density of states, observed in B $i_2$S $r_2$CaC $u_2$ $O_{8}$$\chi$ superconductors, is s- wave.X> $O_{8}$$\chi$ superconductors, is s- wave. wave.

  • PDF