• Title/Summary/Keyword: X-ray absorption

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Analysis of Continuum X-ray Specturum and Determination of Electron Temperature from Iodine Photodissociation Laser produced plasma (집속된 광분해 옥소레이저에 의한 플라즈마로부터 방출되는 연속 X-선 스펙트럼 분석과 전자온도 결정)

  • 김동환;김남성;이상수
    • Proceedings of the Optical Society of Korea Conference
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    • 1988.06a
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    • pp.135-144
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    • 1988
  • 1-GW Iodine photodissociation Laser (λ=1.315${\mu}{\textrm}{m}$)is focused to generate the continuum x-ray radiation at titanium(z=22)target. A piced of aluminum(360 )-mylar(8${\mu}{\textrm}{m}$) film is used to isolate the soft X-ray radiation emitted. Convex-xurved mica crystal spectrometer is used to obtain the soft x-ray spectra from the laser titanium target plasma and the slope of continum X-ray spectra are found to show two different different electron effective temperaturres, 0.11keV and 7.1KeV. We compare the two temperature result with the foil absorption method.

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The potential of X-ray irradiation as a new pasteurization technology for food (식품 살균을 위한 X선 조사 기술의 활용 및 전망)

  • Lim, Jong-Seong;Ha, Jae-Won
    • Food Science and Industry
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    • v.53 no.3
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    • pp.264-276
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    • 2020
  • Ionizing radiation is one of the efficient non-thermal pasteurization methods. The US Food and Drug Administration (FDA) allows the use of ionizing radiation to a dose up to 10 kGy for controlling foodborne pathogens and extending the self-life of foods. Recently X-rays, generated on absorption of high energy electrons in an appropriate metal target, have been used commercially for sterilization purposes. X-rays have the advantages of higher penetration power than E-beams and absence of harmful radioactive sources, such as Cobalt-60 or Cesium-137 associated with gamma-rays. That is why it has continued to receive attention as an attractive alternative to gamma-ray or E-beam irradiation. In this article, the potential of X-ray irradiation for controlling foodborne pathogens in various food products and necessary pre-requisite knowledge for the introduction of X-ray irradiation to the Korean food industry will be provided.

Spectroscopic Study of the X-ray Dip at Pre-eclipse Phase of Hercules X-1

  • Choi, C.S.;Nagase, F.;Makino, F.;Dotani, T.;Min, K.W.
    • Bulletin of the Korean Space Science Society
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    • 1992.10a
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    • pp.21-21
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    • 1992
  • The X-ray binary pulsar Her X-1 was observed with Ginga on 1988 August 28 during the orbital phase of 0.76 to 0.85 at the main-on phase of the 35 day cycle. During the observations the X-ray intensity varied by a factor of five or more on a time scale as short as 30 sec, due mostly to the soft X-ray absorption in the pre-eclipse phase. From the studies of pulse profiles and energy spectra, we revealed that there exists in the dipphase an unpulsed component which is "3% of the intensity at the non-absorbed high-level. We suggest that scattering of the source continuum by the optically thin hot corona is responsible for the unpoised component. In the spectral analysis, we find that the high-state non-absorbed spectra can be fitted by a power-law without absorption, and the spectra observed in the different abgorption states by two components of a power-law with the same photon index. An iron-K emission line is required in to the cases of fitting. The estimated equivalent width of the iron line varies from 0.18 to 0.51 key according to the change in the absorption column density along the line of sight. We suggest that the fluorescent iron line arises in a cool and relatively small region, like the Alfvensur face, and may be partially intercepted by the optically thick gas cloud passing across the line of sight.1 Korea Astronomy Observatorya The Institute of Space and Astronautical Science in Japan3 Korea Advanced Institute of Science and Technology

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Zinc Sulfide-selenium X-ray Detector for Digital Radiography

  • Park, Ji-Koon;Kang, Sang-Sik;Kim, Jae-Hyung;Mun, Chi-Woong;Nam, Sang-Hee
    • Transactions on Electrical and Electronic Materials
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    • v.3 no.4
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    • pp.16-20
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    • 2002
  • The high bias voltage associated with the thick layer (typically 500-1000 ㎛) of selenium required to have an acceptable x-ray absorption in radiography and fluoroscopy applications may have some practical inconvenience. A hybrid x-ray detector with zinc sulfide-amorphous selenium structure has been developed to improve the x-ray sensitivity of a a-Se based flat-panel digital imaging detector. Photoluminescence(PL) characteristic of a ZnS:Ag phosphor layer showed a light emission peak centered at about 450 nm, which matches the sensitivity spectrum of selenium. The dark current of the hybrid detector showed similar characteristics with that of a a-Se detector. The x-ray sensitivity of hybrid and a-Se x-ray detector was 345 pC/㎠/mR and 295 pC/㎠/mR at an applied voltage of 10 V/㎛, respectively. The purpose of this study was to evaluate the pertinence of a solution using a thin selenium layer, as a photosensitive converter, with a thick coating of silver doped zinc sulfide phosphor.

A study on the optical property and in-situ preparation of water-based acrylic emulsion containing $Cu_xS$ nanoparticle (금속 nanoparticle이 함유된 수분산성 아크릴 코팅제의 제조 및 흡광 특성)

  • Lee, Soo;Kim, Jin-Woo
    • Journal of the Korean Applied Science and Technology
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    • v.27 no.4
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    • pp.445-451
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    • 2010
  • To prepare very stable acrylic type emulsion having a visible ray absorption property, in-situ preparation technique of $Cu_xS$ nanoparticle was adopted. Firstly, the acylic emulsions of methyl methacrylate(MMA), butyl acrylate(BA), and acrylonitrile(AN) were synthesized by pre-emulsion polymerization at $60^{\circ}C$ in the presence of anionic surfactant. Secondly, $Cu_xS$ nanocomposited emulsions were directly prepared in the prepolymerized acrylic emulsion with $CuSO_4$ at $50^{\circ}C$. The presnce of $Cu_xS$ nanoparticle in emulsion was confirmed by SEM and EDS. The final $Cu_xS$ nanocomposited emulsion showed an olive-green colour and good emulsion stability up to 1 month. In addition the PET films coated with our $Cu_xS$ nanocomposited emulsion absorbed effectively the visible ray.

Electronic structure studies of Co-substituted FINEMET alloys by x-ray absorption spectroscopy

  • Chae, K.H.;Gautam, S.;Song, J.H.;Kane, S.N.;Varga, L.K.
    • Proceedings of the Korean Vacuum Society Conference
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    • 2010.02a
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    • pp.377-377
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    • 2010
  • FINEMET type nanocrystalline materials synthesized by controlled crystallization of amorphous ribbons[1] exhibit excellent soft magnetic properties making them attractive for technological applications. Present work reports the electronic structure studies of Co-substituted FINEMET to get information on the effect of successive Co substitution on local environment around Fe and Co atom by using near edge x-ray absorption fine structure (NEXAFS) and x-ray magnetic circular dichroism (XMCD) measurements. NEXAFS spectroscopy and XMCD measurements have been carried out at Fe $L_{3,2}$ and Co $L_{3,2}$-edges to investigate the chemical states and electronic structure of FINEMET [$(Fe_{100-x}Co_x)_{78}Si_9Nb_3Cu_1Ba$](0$L_{3,2}$-edge reveal that Fe is in 2+ state and in tetrahedral symmetry with other elements. The magnetic properties exhibiting soft magnetic behavior[2] are discussed on the basis of the electronic structure studied through XMCD.

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Local Structure Study of Ni in Ni-Zn Alloy Coating on Steel by X-ray Absorption Spectroscopy (X선 흡수 분광법을 이용한 Ni-Zn 도금 강판에서의 Ni의 국부 구조에 관한 연구)

  • Lee, Do-Hyung
    • Analytical Science and Technology
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    • v.11 no.3
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    • pp.202-205
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    • 1998
  • X-ray absorption fine structure spectroscopic studies at the Ni K-edge have been performed for the Ni-Zn alloy coating layer on steel. The Ni-Zn interatomic distances and Debye-Waller factors were determined by fitting the experimental data with the theoretical spectra in the temperature range of 80 to 300K. The average Ni-Zn interatomic distance was found to be $2.557{\AA}$ and the variation of the Ni-Zn interatomic distance with temperature in this range was insignificant. From the comparison of the Ni-Zn interatomic distance with the nearest neighbor distance of pure Zn lattice it has been suggested that there is an apparent contraction around Ni atom.

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FT-IR and X-Ray Diffraction Characterization of Melanoidins Formed from Glucose and Fructose with Amino Acid Enantiomers in the Maillard Reaction

  • Kim, Ji-Sang;Lee, Young-Soon
    • Food Science and Biotechnology
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    • v.18 no.2
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    • pp.546-551
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    • 2009
  • The objective of this study was to investigate Fourier transform infrared (FT-IR) spectrometry and the X-ray diffraction (XRD) characterization of melanoidins formed from glucose and fructose with amino acid enantiomers in the Maillard reaction. Before dialysis, FT-IR spectroscopy of all the samples showed that the characteristic absorption intensities appeared as a broad and intense band of the stretching vibration of the -OH group at 3,400/cm for a high pH. The absorption bands of the melanoidins sharply decreased in intensity after dialysis as compared to those before dialysis. In particular, the absorption bands at 992 and 575/cm disappeared. The XRD confirmed that the crystal structure of the melanoidins disappeared after dialysis and a new crystal structure was formed at 9 and $28^{\circ}$ ($2{\theta}$. In particular, broad diffraction peaks were formed in the $10-21^{\circ}$ ($2{\theta}$) range for a high pH, while other sharp diffraction peaks disappeared.

Structure design of Csl-Se Detector using Monte Carlo Simulation (몬테카를로 시뮬레이션을 통한 Csl-Se 검출기의 구조 설계)

  • Park, Ji-Koon;Kang, Sang-Sik;Choi, Jang-Young;Lee, Hung-Won;Nam, Sang-Hee
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2002.11a
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    • pp.420-423
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    • 2002
  • In recent years, there has been keen interest in developing f1at panel detectors for all modalities of radiology, including gerneral radiology, fluoroscopy(angiography and cardiology), electronic portal imaging, and mammography. In this paper, we report the new hybrid x-ray detector consisted of CsI(Tl) photoemission layer and a-Se photoconductor layer to resolve conventional x-ray detector such as the direct detector using a-Se and the indirect detector using CsI(Tl)/a-Si. To design the structure of CsI(Tl)/a-Se detector, the penetrated energy spectrum and absorption fraction was estimated using MCNP 4C code. Experimental results showed that the absorption fraction of $500{\mu}m-Se$ film and $150{\mu}m-CsI\left(Tl \right)/a-Se\left( 30{\mu}m \right)$ film is 70% at 70 kVp. The absorption energy is 90% at $350{\mu}m-CsI(Tl)$.

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Dyeing of PTT Fiber(1) - Effect of Heat Setting on Dyeing and Physical Properties of PTT Fiber - (PTT 섬유의 염색성 (1) - 열처리한 PTT 섬유의 염색성 및 물성 -)

  • 이두환;정동석;이문철
    • Textile Coloration and Finishing
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    • v.14 no.5
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    • pp.268-276
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    • 2002
  • Poly(trimethylene terephthalate)(PTT) and Poly(ethylene terephthalate)(PET) fibers were annealed at various temperatures ranging from $100^\circ{C}$ to $230^\circ{C}$ for 10 min under tension and tension free. Dyeing rates and absorption isotherms of both fibers were obtained with C.I. Disperse Red 60 at 100, 120 and $130^\circ{C}$ in water system. Also X-ray diffraction pattern, moisture regain and water absorption were investigated. The dyeing rate of PTT fiber is faster than PET fiber, and dyeing of PTT fiber begin at lower temperature compared to PET fiber. The absorption isotherms from both fibers with disperse dye we nearly linear up to the saturation dye uptake, which increase with dyeing temperature. Equilibrium dye uptake of PTT fiber annealed under tension above $180^\circ{C}$ was remarkably decreased because of a changes in the fine structure of fiber. The intensities of X-ray diffraction peaks of both annealed fibers were increased with increasing in annealed temperature. The reflections observed at $2\theta$=$15.8^\circ$, $24^\circ$ and $25.2^\circ$ were assigned reflection of crystal at the planes of (010), $(1\bar02,\;\bar112),\;and\;(\bar13,\; \bar113)$ respectively, and the peak became sharp with heat setting temperature.