• Title/Summary/Keyword: X-probe

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Complex Permittivity Measurement using a Coaxial Slotted Line of Reference Liquids at Mobile Communication Frequencies (동축 슬롯 선로를 이용한 기준 용액들의 이동 통신 주파수帶에서의 복소 유전율 측정)

  • 김정호;김윤명
    • The Journal of Korean Institute of Electromagnetic Engineering and Science
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    • v.14 no.9
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    • pp.955-960
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    • 2003
  • In this paper, complex permittivities of reference liquids were measured by a sample holder of terminated slotted coaxial line with a movable probe at mobile communications frequencies. The validity of the liquid measurement system was checked by experimental tests with the reference liquids proposed in IEEE Std 1528-200X.

Experimental Investigation on the Turbulence Augmentation of a Gun-type Gas Burner by Slits and Swirl Vanes

  • Kim, Jang-kweon
    • Journal of Mechanical Science and Technology
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    • v.18 no.10
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    • pp.1819-1828
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    • 2004
  • The purpose of this paper is to investigate the effects of slits and swirl vanes on the turbulence augmentation in the flow fields of a gun-type gas burner using an X-type hot-wire probe. The gun-type gas burner adopted in this study is composed of eight slits and swirl vanes located on the surface of an inclined baffle plate. Experiment was carried out at a flow rate of 450 ι/min in burner model installed in the test section of subsonic wind tunnel. Swirl vanes playa role diffusing main flow more remarkably toward the radial direction than axial one, but slits show a reverse feature. Consequently, both slits and swirl vanes remarkably increase turbulence intensity in the whole range of a gun-type gas burner with a cone-type baffle plate.

Characterization of Heterogeneous NaCl-Na$_2$SO$_4$ Particles Using Low-Z Electron Probe X-ray Microanalysis (Low-Z Electron Probe X-ray Microanalysis를 이용한 불균일 NaCl-Na$_2$SO$_4$ 입자의 분석)

  • 구희준;안용훈;김혜경;노철언
    • Proceedings of the Korea Air Pollution Research Association Conference
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    • 2003.11a
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    • pp.394-395
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    • 2003
  • 대기 중의 황산염 입자는 인체 건강에 좋지 않은 영향을 미칠 뿐 아니라, 지구에 유입되는 빛을 산란시키고 구름을 생성하는 핵으로 작용함으로서 직ㆍ간접적으로 햇빛을 차단하여 전지구적 기후 변화에 상당한 역할을 하는 것으로 알려져 있다. 황산염 입자는 대기 중 SO$_2$의 산화에 의해 주로 생성되는데, 지금까지의 대기 모델을 활용한 연구에 의하면 대기 중의 SO$_2$의 양에 비해 황산염의 양은 과소 평가되고 있다. 이는 대기 중 황산염의 생성에 대한 대기 화학 반응기전이 제대로 파악되지 않아서 global scale의 예측이 불확실하기 때문이다. (중략)

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Single particle characterization of atmospheric aerosol particles collected in Seoul, using low-Z electron probe X-ray microanalysis (Low-Z Electron Probe X-ray Microanalysis를 이용한 서울시 대기 중 입자상 물질 분석)

  • 구희준;노철언;김혜경
    • Proceedings of the Korea Air Pollution Research Association Conference
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    • 2002.11a
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    • pp.352-353
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    • 2002
  • 최근 산업이 발달함에 따라 수도권을 비롯한 도시에서의 인구집중과 증가로 인한 운행 차량 수의 증가, 산업규모의 확대 둥으로 인해 대기분진 중 호흡성 또는 미세분진 농도의 증가가 관찰되고 있으며 이로 인한 주민건강 위해의 가능성이 제기되고 있다. 2.5$\mu\textrm{m}$ 이하의 미세 입자는 폐포내 침착율이 높으며, 유해성 가스 및 중금속을 쉽게 흡착하여 인체에 전달하는 매체가 되기도 하고, 빛을 흡수, 산란시키기 때문에 시정을 악화.시킨다. 따라서 도시대기의 입자상 물질의 물리적, 화학적 특성에 대해서 많은 연구가 진행되어 왔다. (중략)

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X-ray Micro-Imaging Technique and Its Application to Micro-Bubbles in an Opaque Tube (X-ray Micro-Imaging 기법 소개 및 불투명 튜브 내부의 마이크로 버블 가시화 연구)

  • Lee Sang-Joon;Kim Seok;Paik Bu-Geun
    • 한국가시화정보학회:학술대회논문집
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    • 2002.11a
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    • pp.31-34
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    • 2002
  • Imaging techniques using x-ray beam at high energies (>6KeV) such as contact radiography, projection microscopy, and tomography have been used to nondestructively discern internal structure of objects in material science, biology, and medicine. This paper introduces the x-ray micro-imaging method using 1B2 micro-probe line of PAL (Pohang Accelerator Laboratory). Cross-sectional information on low electron density materials can be obtained by probing a sample with coherent synchrotron x-ray beam in an in-line holography setup. Living organism such as plants, insects are practically transparent to high energy x-rays and create phase shift images of x-ray wave front. X-ray micro-images of micro-bubbles of $20\~120\;{\mu}m$ diameter in an opaque tube were recorded. Clear phase contrast images were obtained at Interfaces between bubbles and surrounding liquid due to different decrements of refractive index.

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Preparation, Structure, and Photoemission Studies on the High Temperature Superconductor $YBa_2Cu_{3-x}Ni_xO_{7-{\delta}}$

  • Choy, Jin-Ho;Choe, Won-Young
    • Bulletin of the Korean Chemical Society
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    • v.11 no.5
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    • pp.379-383
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    • 1990
  • $YBa_2Cu_{3-x}Ni_xO_{7-{\delta}}$, with x = 0.05, 0.2, 0.4, 0.7 and 1.0 had been prepared by the thermal decomposition of corresponding nitrates. Among them, the sample with x = 0.05 shows above-liquid-$N_2$ temperature superconductivity with $T_c$ of 88.7K. According to the X-ray diffraction analysis, its crystal symmetry was estimated as orthorhombic with the lattice parameters of a = 3.866${\AA}$, b = 3.893${\AA}$, c = 11.715${\AA}$. The chemical composition of the sample was determined by electron probe microanalysis and the chemical composition around its grain boundaries was carefully studied by the X-ray line scanning technique. From the observed binding energy of Ni-$2p_{3/2}$ orbital electron (B.E. = 853 eV) measured by X-ray photoelectron spectroscopy, the valency state of nickel stabilized in $YBa_2Cu_{2.95}Ni_{0.05}O_{7-{\delta}}$ oxide lattice could be determined to be Ni(II).

A High-speed Atomic Force Microscope for Precision Measurement of Microstructured Surfaces

  • Cui, Yuguo;Arai, Yoshikazu;Asai, Takemi;Ju, BinFeng;Gao, Wei
    • International Journal of Precision Engineering and Manufacturing
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    • v.9 no.3
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    • pp.27-32
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    • 2008
  • This paper describes a contact atomic force microscope (AFM) that can be used for high-speed precision measurements of microstructured surfaces. The AFM is composed of an air-bearing X stage, an air-bearing spindle with the axis of rotation in the Z direction, and an AFM probe unit. The traversing distance and maximum speed of the X stage are 300 mm and 400 mm/s, respectively. The spindle has the ability to hold a sample in a vacuum chuck with a maximum diameter of 130 mm and has a maximum rotation speed of 300 rpm. The bandwidth of the AFM probe unit in an open loop control circuit is more than 40 kHz. To achieve precision measurements of microstructured surfaces with slopes, a scanning strategy combining constant height measurements with a slope compensation technique is proposed. In this scanning strategy, the Z direction PZT actuator of the AFM probe unit is employed to compensate for the slope of the sample surface while the microstructures are scanned by the AFM probe at a constant height. The precision of such a scanning strategy is demonstrated by obtaining profile measurements of a microstructure surface at a series of scanning speeds ranging from 0.1 to 20.0 mm/s.

Spatial Distributions of Alloying Elements Obtained from Atom Probe Tomography of the Amorphous Ribbon Fe75C11Si2B8Cr4

  • Shin, Jinkyung;Yi, Seonghoon;Pradeep, Konda Gokuldoss;Choi, Pyuck-Pa;Raabe, Dierk
    • Korean Journal of Materials Research
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    • v.23 no.3
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    • pp.190-193
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    • 2013
  • Spatial distributions of alloying elements of an Fe-based amorphous ribbon with a nominal composition of $Fe_{75}C_{11}Si_2B_8Cr_4$ were analyzed through the atom probe tomography method. The amorphous ribbon was prepared through the melt spinning method. The macroscopic amorphous natures were confirmed using an X-ray diffractometer (XRD) and a differential scanning calorimeter (DSC). Atom Probe (Cameca LEAP 3000X HR) analyses were carried out in pulsed voltage mode at a specimen base temperature of about 60 K, a pulse to base voltage ratio of 15 %, and a pulse frequency of 200 kHz. The target detection rate was set to 5 ions per 1000 pulses. Based on a statistical analyses of the data obtained from the volume of $59{\times}59{\times}33nm^3$, homogeneous distributions of alloying elements in nano-scales were concluded. Even with high carbon and strong carbide forming element contents, nano-scale segregation zones of alloying elements were not detected within the Fe-based amorphous ribbon. However, the existence of small sub-nanometer scale clusters due to short range ordering cannot be completely excluded.

Pseudoisodicentric X chromosome in a female with primary amenorrhea (원발성 무월경 여성에서 관찰된 Pseudoisodicentric X 염색체)

  • Park, Sang-Hee;Shim, Sung-Han;Chin, Mi-Uk;Kang, Su-Jin;Bae, Sung-Mi;Sohn, Soo-Min;Cha, Dong-Hyun;Yoon, Tae-Ki;Cho, Jung-Hyun
    • Journal of Genetic Medicine
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    • v.5 no.1
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    • pp.61-64
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    • 2008
  • A 24-year-old female with primary amenorrhea was referred for a chromosome study. The karyotype of the patient was 46,X,der(X) under initial GTG-banding analysis. Fluorescence in situ hybridization (FISH) analysis with an LSI Kallmann (KAL) region probe [probes for Xp22.3(KAL) and CEP(X) for control] was carried out. The abnormal chromosome was KAL- and CEP(X)${\times}2$. In addition, interphase FISH analysis revealed the patient to be mosaic for two different cell lines: 90% of cells had three signals and 10% of the cells had only one signal for CEP(X). Based on these results, the karyotype of the patient was 45,X/46,X,psu idic(X)(p22.1), which is partial trisomy for Xqter${\rightarrow}$Xp22.1 and partial monosomy for Xpter${\rightarrow}$Xp22.1. This karyotype was considered a variant of Turner syndrome. In summary, Idic(X) and low-level mosaicism was successfully characterized by FISH analysis with a CEP(X) probe.

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