• Title/Summary/Keyword: X-RAY SCATTERING

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Evolution of Growth Orientation and Surface Roughness During Sputter Growth of AIN/Si(111) (스퍼터링 방법에 의한 AIN/Si(111)의 성장 방향과 표면 거칠기의 성장 시간에 대한 연구)

  • 이민수;이현휘;서선희;노동영
    • Journal of the Korean Vacuum Society
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    • v.7 no.3
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    • pp.237-241
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    • 1998
  • The growth orientation and the surface roughness of AIN/Si(111) films grown by radio frequency (RF) reactive magnetron sputtering were investigated using in-situ x-ray scattering technique and atomic force microscopy (AFM). AIN films were initially grown with the <001> preferred growth orientation under most growth conditions. As the film gets thicker, however, the growth orientation changes significantly, especially at high substrate temperature and high RF powers. We attribute the observed behavior to the competition between the surface energy that prefers the <001> growth orientation and the strain energy that randomizes the growth orientation. In addition, we investigated the evolution of the surface morphology during the growth using the x-ray reflectivity measurement.

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Eclipse Spectrum of Her X-1 Observed by ASCA in the Low Intensity State

  • Choi, C.S.;Seon, K.I.
    • Bulletin of the Korean Space Science Society
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    • 1995.10a
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    • pp.30-30
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    • 1995
  • We present the results of analysis on the X-ray observations of the binary X-ray pulsar Her X-I. made with ASCA/SIS on August 13-14. 1993. An eclipse transition from ingress to egress was fully covered by the observations. The main findings are as follows; (1) a model of power-law plus black-body is required to interpret the entire eclipse spectrum. and the black-body component appears at < 0.7 keV. (2) the power-law continuum which has photon index ${\alpha}\;=\;{0.84^{\;+0.14}}_{\;-0.19}$ is very similar to that of detected by Ginga/LAC (${\alpha}\;=\;0.80\;{\pm}\;0.04$), (3) the calculated eclipse flux of $2^{-10}\;keV.{\;}~{\;}1.8{\pm}10^{-11}{\;}ergs{\;}cm^{-2}s^{-1}$, is consistent with the Ginga observation carried out in the high intensity state ~2.0{\pm}10^{-11}{\;}ergs{\;}cm^{-2}s^{-1}$, (4) there is no significant absorption feature. and an upper limit of the aborption column $NH{\;}\leq{\;}3{\pm}10^{20}\;cm^{-2}$ is determined at the 90% confidence limit. Based on these results, we suggest that extended matter surrounding the binary system should be existed persistently with stable conditions, and scattering of the source continuum by the matter is responsible for the eclipse emission.ission.

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An Evaluation Method of X-ray Imaging System Resolution for Non-Engineers (비공학도를 위한 X-ray 영상촬영 시스템 해상력 평가 방법)

  • Woo, Jung-Eun;Lee, Yong-Geum;Bae, Seok-Hwan;Kim, Yong-Gwon
    • Journal of radiological science and technology
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    • v.35 no.4
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    • pp.309-314
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    • 2012
  • Nowadays, digital Radiography (DR) systems are widely used in clinical sites and substitute the analog-film x-ray imaging systems. The resolution of DR images depends on several factors such as characteristic contrast and motion of the object, the focal spot size and the quality of x-ray beam, x-ray scattering, the performance of the DR detector (x-ray conversion efficiency, the intrinsic resolution). The DR detector is composed of an x-ray capturing element, a coupling element and a collecting element, which systematically affect the system resolution. Generally speaking, the resolution of a medical imaging system is the discrimination ability of anatomical structures. Modulation transfer function (MTF) is widely used for the quantification of the resolution performance for an imaging system. MTF is defined as the frequency response of the imaging system to the input of a point spread function and can be obtained by doing Fourier transform of a line spread function, which is extracted from a test image. In clinic, radiologic technologists, who are in charge of system maintenance and quality control, have to evaluate or make routine check on their imaging system. However, it is not an easy task for the radiologic technologists to measure MTF accurately due to lack of their engineering and mathematical backgrounds. The objective of this study is to develop and provide for radiologic technologists a medical system imaging evaluation tool, so that they can measure and quantify system performance easily.

A Study on the Resolution Analysis of Digital X-ray Images with increasing Thickness of PMMA (조직 등가물질 두께 증가에 따른 디지털 엑스선 영상의 해상도 분석에 관한 연구)

  • Kim, Junwoo
    • Journal of the Korean Society of Radiology
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    • v.15 no.2
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    • pp.173-179
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    • 2021
  • Scattered x-ray generated by digital radiography systems also have the advantage of increasing signals, but ultimately detectability is reduced by decreasing resolution and increasing noise of x-ray images transmitted objects. An indirect method of measuring scattered x-ray in a modulation-transfer function (MTF) for evaluating resolution in a spatial-frequency domain can be considered as a drop in the MTF value corresponding to zero-frequency. In this study, polymethyl methacrylate (PMMA) was used as a patient tissue equivalent, and MTFs were obtained for various thicknesses to quantify the effect of scattered x-ray on resolution. X-ray image signals were observed to decrease by 35 ~ 83% with PMMA thickness increasing, which is determined by the absorption or scattering of x-rays in PMMA, resulting in reduced MTF and increased scatter fraction. The method to compensate for MTF degradation by PMMA resulted in the MTF inflation without considering the optical spreading generated by the indirect-conversion type detector. Data fitting or zero-padding are needed to compensate for MTF more reasonably on edge-spread function or line-spread function.

Homopolymer Distribution in Polystyrene - Poly(methyl methacrylate) Diblock Copolymer (폴리스티렌-폴리(메틸 메타크릴레이트) 이종 블록 공중합체 내의 단일중합체 분포)

  • Hong, Sung-Ho;Lee, Eun-Ji;Song, Kwon-Bin;Lee, Kwang-Hee
    • Polymer(Korea)
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    • v.35 no.6
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    • pp.531-536
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    • 2011
  • Homopolymer distribution in block copolymer/homopolymer blends was investigated as a function of homopolymer concentration and homopolymer molecular weight. The deuterated poly(methyl methacrylate) or polystyrene was blended with a deuterated polystyrene-poly(methyl methacrylate) diblock copolymer up to a concentration of 20 wt%. Samples were characterized by small-angle X-ray scattering (SAXS), neutron reflectivity and transmission electron microscopy. The block copolymer with a thin-film geometry formed alternating lamellar microdomains oriented parallel to the substrate surface. By adding the homopolymer, the microdomain structure was significantly disturbed. As a consequence, a poorly ordered morphology appeared when the homopolymer concentration exceeded 15 wt%. Increasing the homopolymer concentration and/or the homopolymer molecular weight caused the microdomains to swell less uniformly, resulting in segregation of the homopolymer toward the middle of the microdomains.

Application of sound scattering models to swimbladdered fish, red seabream (Chrysophys major)

  • Kang Donhyug;Hwang Doojin;Na Jungyul;Kim Suam
    • Proceedings of the Acoustical Society of Korea Conference
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    • spring
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    • pp.233-236
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    • 2000
  • The acoustical response of fish depends on size and physical structure na, most important, on the presence or absence of a swimbladder. Acoustic scattering models for swimbladdered fish represent a fish by an ideal pressure-release surface having the size and shape as the swimbladder. Target strength experiments of red seabream (Chrysophrys major) have been conducted using 38 (split-beam), 120 (split-beam) and 200kHz (dual-beam) frequencies. At each start of each experiment, the live fish are placed in the cage at the surface, then the cage is lowed to about $4{\cal}m$ depth where it remains during the measurements. To test the acoustic models, predictions of target strength based on swimbladder morphometries of 10 red seabream offish total length from $103{\cal}mm{\;}to{\;}349{\cal}mm$ ($3 <$TL/\lambda$ < 45)are compared with conventional target strength measurements on the same, shock-frozen immediately after caged experiments. X-ray was projected along dorsal aspect to know the morphological construction of swimbladder. and fish body. At high frequencies, Helmholtz-kirchhoff(HK) approximation would greatly enhance swimbladdered fish modeling. Sound scattering model [HK-ray approximation model] for comparison to experimental target strength data was used to model backscatter measurements from individual fish. The scattering data can be used in the inverse method along with multiple frequency sonar systems to investigate the adequacy of classification and identification of fish

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X-Ray Scattering Studies on Molecular Structures of Star and Dendritic Polymers

  • Jin, Sang-Woo;Jin, Kyeong-Sik;Yoon, Jin-Hwan;Heo, Kyu-Young;Kim, Je-Han;Kim, Kwang-Woo;Ree, Moon-Hor;Higashihara, Tomoya;Watanabe, Takumi;Hirao, Akira
    • Macromolecular Research
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    • v.16 no.8
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    • pp.686-694
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    • 2008
  • We studied the molecular shapes and structural characteristics of a 33-armed, star polystyrene (PS-33A) and two $3^{rd}$-generation, dendrimer-like, star-branched poly(methyl methacrylate)s with different architectures (pMMA-G3a and PMMA-3Gb) and 32 end-branches under good solvent and theta ($\Theta$) solvent conditions by using synchrotron small angle X-ray scattering (SAXS). The SAXS analyses were used to determine the structural details of the star PS and dendrimer-like, star-branched PMMA polymers. PS-33A had a fuzzy-spherical shape, whereas PMMA-G3a and PMMA-G3b had fuzzy-ellipsoidal shapes of similar size, despite their different chemical architectures. The star PS polymer's arms were more extended than those of linear polystyrene. Furthermore, the branches of the dendrimer-like, star-branched polymers were more extended than those of the star PS polymer, despite having almost the same number of branches as PS-33A. The differences between the internal chain structures of these materials was attributed to their different chemical architectures.

A study on Protector Performance Evaluation According to X-ray Scattering Distribution of Portable Radiation System (이동형 방사선 발생장치 차폐물 설치에 관한 연구)

  • Kim, Hyong-Gyun;Sung, Dong-Keon;Cho, Kyong-Mi;Kim, Sang-Beom;Kim, Jae-Young;Choi, Jun-Ho
    • Korean Journal of Digital Imaging in Medicine
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    • v.11 no.2
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    • pp.85-92
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    • 2009
  • This study, "The study about performance evaluations of mobile cover for X-ray's diffusion and distribution in mobile radiation" is based on the rules of mobile defense apparatus for radiation producer in 2006. To use the mobile cover for X-ray for diagnosis has been compulsory in common wards except operation rooms, emergency rooms and intensive care units. we have confirmed the effect in arbitrary shielding material after Qualitiy Control was carried out for accuracy in an experiment of mobile photographing equipment. The performance evaluation was conducted with the fabrics of selenium, 0.2 mmPb, 0.1 mmPb and aluminiums. Considering the result, we choosed 0.1 mmPb and attached cover to mobile photographing equipment. We have finished making the cover after drew up the draft to attach cover to mobile photographing equipment through the modeling and the structural analysis. the process of the study is that we assembled the manufactured structures and carried out the practical experiment to take the photograph after attaching the fabric of 0.1 mmPb to mobile photographing equipment. It is need of additional thesises hereafter that we compare the result between the part to improve for safety besides convenience in photographic experiment about clinical radiation and the effect of covering the diffusion in condition attached the cover.

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In situ Structural Investigation of Iron Phthalocyanine Monolayer Adsorbed on Electrode Surface by X-ray Absorption Fine Structure

  • Kim, Seong Hyeon;Toshiaki Ohta;Gang, Gwang Hun
    • Bulletin of the Korean Chemical Society
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    • v.21 no.6
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    • pp.588-594
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    • 2000
  • Structural changes of an iron phthalocyanine (FePC) monolayer induced by adsorption and externally applied potential on high area carbon surface have been investigated in situ by iron K-edge X-ray absorption fine structure (XAFS) in 0.5 M $H_2S0_4.$ Fine structures shown in the X-ray absorption near edge structure (XANES) for microcrystalline FePC decreased upon adsorption and further diminished under electrochemical conditions. Fe(II)PC(-2) showed a 1s ${\rightarrow}$ 4p transition as poorly resolved shoulder to the main absorption edge rather than a distinct peak and a weak 1s ${\rightarrow}$ 3d transition. The absorption edge position measured at half maximum was shifted from 7121.8 eV for Fe(lI)PC(-2) to 7124.8 eV for $[Fe(III)PC(-2)]^+$ as well as the 1s ${\rightarrow}$ 3d pre-edge peak being slightly enhanced. However, essentially no absorption edge shift was observed by the 1-electron reduction of Fe(Il)PC(-2), indicating that the species formed is $[Fe(II)PC(-3)]^-$. Structural parameters were obtained by analyzing extended X-ray absorption fine structure (EXAFS) oscillations with theoretical phases and amplitudes calculated from FEFF 6.01 using multiple-scattering theory. When applied to the powder FePC, the average iron-to-phthalocyanine nitrogen distance, d(Fe-$N_p$) and the coordination number were found to be 1.933 $\AA$ and 3.2, respectively, and these values are the same, within experimental error, as those reported ( $1.927\AA$ and 4). Virtually no structural changes were found upon adsorption except for the increased Debye-Wailer factor of $0.005\AA^2$ from $0.003\AA^2.$ Oxidation of Fe(II)PC(-2) to $[Fe(III)PC(-2)]^+$ yielded an increased d(Fe-Np) (1 $.98\AA)$ and Debye-Wailer factor $(0.005\AA^2).$ The formation of $[Fe(II)PC(-3)]^-$, however, produced a shorter d(Fe-$N_p$) of $1.91\AA$ the same as that of crystalline FePC within experimental error, and about the same DebyeWaller $factor(0.006\AA^2)$.

Radiation Shielding Analysis for the X-ray Facility (X-선 발생장치 시설의 방사선 차폐 해석)

  • Kwon, Seog-Guen;Choi, Ho-Sin;Moon, Philip-S.;Yook, Jong-Chul
    • Journal of Radiation Protection and Research
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    • v.12 no.1
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    • pp.34-39
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    • 1987
  • Radiation shielding analysis for a 6MeV X-ray facility was carried out. The primary and leakage radiation for the facility can be evaluated based on the methodology in NCRP No. 49 and 51. The present study deals with radiation scattering analysis for the outside and inside door of the facility based on the albedo concept. The calculated dose rates were compared with the results of MORSE-CG code calculation and the measured data, resulting in a good agreement, even though there existed some deviation for the inside door. These results can be utilized to the radiation shielding design of the medical and industrial X and gamma ray facilities, and to the safety evaluation of these facilities.

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