• Proceedings of the KSME Conference
• /
• 2003.11a
• /
• pp.1939-1943
• /
• 2003

The precise structural analysis of $SnO_{2}$ thin film, which was prepared by PECVD and thickness 2400 ${\AA}$, was tried to do the structural refinement using X -ray diffraction data. The observed diffraction patterns of $SnO_{2}$ thin film had the strongly preferred orientation effect. WIMV method was used to correct the preferred orientation effect. The final weighted R-factor, $R_{WD}$ was 7.92 %. The lattice parameters, a = b == 4.7366(1) ${\AA}$ and c = 3.1937(1) ${\AA}$, were almost in accordance with ones of $SnO_{2}$ powder.

• Proceedings of the Korean Powder Metallurgy Institute Conference
• /
• 2006.09a
• /
• pp.442-443
• /
• 2006

Vacuum carbonization of nanometer tungsten powder was investigated in a simple designed apparatus. An X-Y recorder was used to plot differential thermal analysis (DTA) curves to determine starting temperature of carbonization of four samples with different specific surface area. The product was detected by X-ray Diffraction (XRD) and small angle X-ray scattering (SAXS). The results show that finer tungsten powder has lower starting temperature of carbonization. Tungsten powder, which BET surface area is $32.97m^2/g$, is completely carbonized to tungsten carbide at $1050^{\circ}C$, although the starting temperature is $865^{\circ}C$. Particle grows sharply before carbonization.

• Proceedings of the Korean Magnestics Society Conference
• /
• 2007.05a
• /
• pp.131.1-131.1
• /
• 2007

• Polymer Science and Technology
• /
• v.24 no.6
• /
• pp.590-595
• /
• 2013

• Proceedings of the Materials Research Society of Korea Conference
• /
• 1998.08a
• /
• pp.137.2-137
• /
• 1998

• Proceedings of the Materials Research Society of Korea Conference
• /
• 1998.08a
• /
• pp.137.3-137
• /
• 1998

• Korean Journal of Crystallography
• /
• v.8 no.1
• /
• pp.20-25
• /
• 1997

Two experimental methods have been developed for high resolution measurement of x-ray scattering. The methods used were (1) an x-ray double crystal diffraction (DCD) spectrometer set-up and (2) an x-ray triple crystal diffraction (TCD) spectrometer set-up. With the DCD arrangement of Si(511)-sample(hkl), rocking curves have been plotted for Si (333), Si(004) and GaAs(004). Also, with the TCD arrangement of Si(111)-Si(111)-Si(511)-sample(hkl) including monolithic monocro-collimator and $K_{\alpha1}$ selector, rocking curves have been plotted for Si(333), Si(004) and GaAs(004). The results of FWHM by DCD and TCD set-up have been compared each other and discussed. The reflection topographs (004) and (115) in an $In_{0.037}Ga_{0.0963}As/GaAs$ sample have been obtained by DCD set-up.

• Bulletin of the Korean Chemical Society
• /
• v.29 no.2
• /
• pp.445-449
• /
• 2008

Micrometer-sized copper (mCu) powders are weakly surface-enhanced Raman scattering (SERS) active by the excitation at 632.8 nm, but nearly ineffective as a SERS substrate at 514.5 nm excitation. The SERS activity of mCu powders at both excitation wavelengths can be increased dramatically by a simple method of the galvanic exchange reaction with AgNO3 in aqueous medium. In this work, the SERS activity of the Ag-exchanged Cu powders (mCu@Ag) has been evaluated by taking a series of Raman spectra using benzenethiol (BT) as the probe molecule. It is clearly confirmed by field emission scanning electron microscopy and X-ray diffractometry that the SERS activity of mCu@Ag powders is, in fact, highly dependent on the extent of galvanic reaction.

• Journal of Astronomy and Space Sciences
• /
• v.33 no.2
• /
• pp.93-99
• /
• 2016

A redback system is a binary system composed of a pulsar and a main sequence star. The inverse Compton (IC) scattering between the stellar soft photons and the relativistic pulsar wind will generate orbital-modulating GeV photons. We look for these IC emissions from redback systems. A multi-wavelength observation of an unassociated gamma-ray source, 3FGL J2039.6-5618, by Salvetti et al. (2015) detected an orbital modulation with a period of 0.2 days in both X-ray and optical cases. They suggested 3FGL J2039.6-5618 to be a new redback candidate. We analyzed the gamma-ray emission of 3FGL J2039.6-5618 using the data from the Fermi large area telescope (Fermi-LAT) and obtained the spectrum in different orbital phases. We propose that the spectrum has orbital dependency and estimate the characteristic energy of the IC emission from the stellar-pulsar wind interaction.

• Progress in Superconductivity
• /
• v.11 no.2
• /
• pp.141-146
• /
• 2010

Phase stability diagram and boundary of a- and c-axis orientation of $SmBa_2Cu_3O_{7-y}$ (SmBCO) thin films grown by pulsed laser deposition (PLD) were reported with studies based on x-ray diffraction [1]. Four different samples are systematically analyzed: normal c-axis oriented orthorhombic $SmBa_2Cu_3O_{7-y}$, a-axis oriented $SmBa_2Cu_3O_{7-y}$, c-axis oriented orthorhombic $SmBa_2Cu_3O_{7-y}$ with $Sm_2BaCuO_5$ phase, and a mixture with c-axis oriented orthorhombic $SmBa_2Cu_3O_{7-y}$ and anomalously long-c tetragonal $SmBa_2Cu_3O_x$. Raman scattering spectroscopy equipped with polarization analysis elucidates the crystal orientation and the origin of the growth of the materials. It indicates that the technique can be used for quality control of conductor manufacturing processes as well as for enhancement of the materials properties.