• Title/Summary/Keyword: Wet bonding

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Bondline Strength Evaluation of Honeycomb Sandwich Panel For Cure Process and Moisture Absorption (경화공정 및 수분흡수에 따른 복합재료 하니콤 샌드위치 판넬의 접합강도특성 연구)

  • Choe, Heung-Seop;Jeon, Heung-Jae;Nam, Jae-Do
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.25 no.1
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    • pp.115-126
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    • 2001
  • In this paper, through a series of comparative experiments, effects of two different cure processing methods, cocure and precure, on the mechanical properties of honeycomb core materials for aircraft applications are considered. Mass of moisture accumulated into the closed cells of the sandwich panel specimen from the measured mass of moisture diffused to the full saturation state into the elements(skin, adhesive layer, Nomex honeycomb), consisting the honeycomb sandwich specimen has been calculated. Water reservoir of 70$\^{C}$ was used to have specimens absorb moisture to see the influence of moisture absorbed into sandwich panel on its mechanical properties. For the repair condition holding for 2 hours at 177$\^{C}$(350℉) temperature, a pressure due to the vapor expansion in each cell of the sandwich panel, which may result in the local separation of the interface between laminated skin and the surface of the honeycomb, has been estimated by vapor pressure-temperature relation from the thermodynamic steam table and compared to the pressure from the ideal gas state equation. The bonding strengths of the laminated skins on the flat surface of the Nomex honeycomb have been compared by the flatwise tension test and climbing drum peel test performed at room temperature for dry, wet and wet-repair specimens, respectively.

Effect of Vinyl Acetate-Ethylene(VAE) Emulsion on Coated Paper Properties (비닐아세테이트 에틸렌 공중합체 바인더가 도공지의 품질에 미치는 영향)

  • Lee, Yong-Kyu;Won, Jong Myoung;Lee, Woo-Jae;Choi, Yong-Hae
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.45 no.5
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    • pp.37-43
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    • 2013
  • This study was focused on applying a new paper coating binder, vinyl acetate-ethylene(VAE) emulsion, with SB-latex and acrylic emulsion for paper coating application. VAE emulsion has a low monomer cost and is non-toxic chemical than conventional adhesive for paper coating such as styrene-butadiene latex( SB-latex) and acrylic emulsion. We conducted double coating in order to test VAE emulsion, which was applied on top surface only. The results showed that optical properties of the coated paper with VAE were similar with the SB-latex binders. In case of bonding strength, dry-pick of the coated paper with VAE showed almost same with other binders while wet-pick of the coated paper with VAE had a little bit lower strength than that with SB-latex.

Preparation and Characterization of Chitosan/Cellulose Acetate Blend Film (키토산/셀룰로오스 아세테이트 복합필름의 제조와 특성)

  • Jung, Young-Jin;An, Byung-Jae;Choi, Hae-Wook;Kim, Hong-Sung;Lee, Young-Hee
    • Textile Coloration and Finishing
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    • v.19 no.4
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    • pp.10-17
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    • 2007
  • Chitosan(CS) and cellulose acetate(CA) composite films were prepared using formic acid as a cosolvent by casting, solvent evaporating and neutralization method. This study examines if the blending method, which uses formic acid as a cosolvent is efficient in improving the mechanical properties of CS film, especially wet strength and elongation. Formic acid is an effective cosolvent for the blend of CS and CA. Under wet condition, tensile strength and elongation of the composite films were obviously higher than those of the films made from pure CS. FTIR, DSC, and X-ray diffraction showed that the composite films exhibit a high level of compatibility and that strong interaction between the CS and CA was caused by intermolecular hydrogen bonding. The affinity series of composite film to transition metal ions are Cu(II) > Cd(II) > Cr(III). The adsorption of Cu((II) ion was shown to be highly pH sensitive.

Studies on Mechanical Properties of Thermoplastic Vulcanizate Containing Acid Group (Acid Group이 도입된 TPV (Thermoplastic Vulcanizate)계 열가소성 탄성체의 기계적 물성에 관한 연구)

  • Kim, Dong Ho;Kim, Gu Ni
    • Journal of Adhesion and Interface
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    • v.16 no.2
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    • pp.63-68
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    • 2015
  • We synthesized thermoplastic polyurethane elastomer containing carboxylic acid group and TPV (thermoplastic vulcanizate). We measured the mechanical, grip, debris, contact angle and adhesion properties according to introducing acid group in elastomer structure. Mechanical and wet slip properties were improved because of the hydrogen bonding by introduction of acid group. Also adhesion strength was increased as increasing of surface polarity by carboxylic acid group. The debris property of TPV made from TPU containing carboxylic acid group was improved.

THE EFFECTS OF SURFACE CONTAMINATION ON THE SHEAR BOND STRENGTH OF COMPOMER

  • Heo, Jeong-Moo;Lee, Su-Jong;Im, Mi-Kyung
    • Proceedings of the KACD Conference
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    • 2001.11a
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    • pp.577-577
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    • 2001
  • The lastest concepts in bonding are "total etch", in which both enamel and dentin are etched with an acid to remove the smear layers, and "wet dentin" in which the dentin is not blown dry but left moist before application of the bonding primer. Ideally, the application of a bonding agent to tooth structure should be insensitive to minor contamination from oral fluids. Clinically contaminations such as saliva, gingival fluid, blood and handpiece lubricant are often encountered by dentists during preparation of a restoration. The aim of this study was to evaluate the effect of contamination by hem-ostatic agents on shear bond strength of compomer restorations. One hundred and ten extracted human maxillary and mandibular molar teeth were collected. The teeth were cleaned from soft tissue remnant and debris and stored in physiologic solution until they were used. Small flat area on dentin of the buccal surface were wet ground serially with 400, 800 and 1200 abrasive paper on automatic polishing machine. The teeth were randomly divided into 11 groups. Each group was conditioned as follows: Group 1 : Dentin surface was not etched and not contaminated by hemostatic agents. Group2 : Dentin surface was not etched but was contaminated by Astringedent (Ultradent product Inc., Utah, U.S.A.). Group3 : Dentin surface was not etched but was contaminated by Bosmin (Jeil Phann, Korea.). Group4 : Dentin surface was not etched but was contaminated by Epri-dent (Epr Industries, NJ, U.S.A.). Group5: Dentin surface was etched and not contaminated by hemostatic agents. Group 6 : Dentin surface was etched and contaminated by Astringedent. Group7 : Dentin surface was etched and contaminated by Bosmin. Group8 : Dentin surface was etched and contaminated by Epri-dent. Group9 : Dentin surface was contaminated by Astringedent. The contaminated surface was rinsed by water and dried by compressed air. Group10 : Dentin surface was contaminated by Bosmin. The contaminated surface was rinsed by water aud dried by compresfed air. Group 11 : Dentin surface was contaminated by Epri-dent. The contaminated surface was rinsed by water and dried by compresfed air. After surface conditioning, F2000 was applicated on the conditoned dentin surface. The teeth were thermocycled in distilled water at $5^{\circ}C\;and\;55^{\circ}C$ for 1000 cycles. The samples were placed on the binder with the bonded compomer-dentin interface parallel to the lmife-edge shearing rod of the Universal testing machine(Zwick 020, Germany) running at a cross head speed of 1.0mmimin. There were no significant differences in shear bond strength between groups 1 and group 3 and 4, but group 2 showed significant decrease in shear bond strength compared with group 1. There were no significant differences in shear bond strength between group 5 and group 7 and 8, but group 6 showed significant decrease in shear bond strength compared with group 5. There were no significant differences in shear bond strength between group 5 and group 9, 10 and 11.

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A Study on the Characteristics of Bonding Strength by Types of Repair Materials by Mechanical Pressurizing Equipment(MPE) (기계식 가압장비(MPE)에 의한 보수재 종류별 부착강도 특성에 관한 연구)

  • Yu, Hyeong-Sik;Chung, Jee-Seung
    • The Journal of the Convergence on Culture Technology
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    • v.6 no.2
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    • pp.553-560
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    • 2020
  • In the existing research paper, we developed Mechanical Pressurizing Equipment(MPE) that can apply a certain amount of pressure and found out about improving the bonding strength of repair materials constructed in the repair section, and if pressurized, the bonding strength could be increased. In this study, the pressure of Mechanical Pressurizing Equipment(MPE) was changed to 0, 10, 30, 50, and 80 kPa, and the test was conducted to select effective pressure by measuring the flexural, compressive, and bonding strength of the specimens and deformation of the pressure plate at the age of 3 and 28th days. As a result of the test, 30 kPa was the most efficient pressure for the MPE. After producing the specimen with three types of repair materials with different main components, the bonding strength was measured according to dry and wet conditions, construction site (ceiling, wall and floor), and whether or not pressurized, on the 3rd, 7th, 14th, and 28th, indicating that the repair materials mixed with cellulose fiber was most effective for the MPE.

Improvement of Paper Strength using Pretreated Precipitated Calcium Carbonate (PCC) (종이의 강도향상을 위한 경질탄산칼슘(PCC) 전처리에 대한 연구)

  • Kim, Chul-Hwan;Lee, Ji-Young;Gwak, Hye-Joeng;Chung, Ho-Kyung;Back, Kyung-Kil;Lee, Hui-Jin;Kim, Sung-Ho;Kang, Ha-Ryoun
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.42 no.1
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    • pp.41-47
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    • 2010
  • Increasing ash content of the paper is one of the most effective methods for saving raw materials and steam consumption and improving optical properties and better print quality. However, the increase of filler loading or filler content using a conventional wet end system is limited due to severe loss in strength properties, affecting runnability and product quality. This is because the filler has no ability to make bonding with cellulosic fibers. Therefore, if the technology to give filler the bonding ability is developed, the ash content of the paper can be increased more than ever. This study was carried out to modify PCC by coating its surface with starch contributing to better bonding with fibers. To prepare the modified PCC, cationic starch was selected as a polymer and then pretreatment was done by mixing PCC and cationic starch. Consequently, the pretreated PCC contributed to higher tensile strength, stiffness and opacity than the conventional filler, such as GCC and untreated PCC. However, CIE whiteness and ISO brightness decreased slightly compared to conventional fillers.

Direct Bonding of Si || SiO2/Si3N4 || Si Wafer Pairs With a Furnace (전기로를 이용한 Si || SiO2/Si3N4 || Si 이종기판쌍의 직접접합)

  • Lee, Sang-Hyeon;Lee, Sang-Don;Seo, Tae-Yun;Song, O-Seong
    • Korean Journal of Materials Research
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    • v.12 no.2
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    • pp.117-120
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    • 2002
  • We investigated the possibility of direct bonding of the Si ∥SiO$_2$/Si$_3$N$_4$∥Si wafers for Oxide-Nitride-Oxide(ONO) gate oxide applications. 10cm-diameter 2000$\AA$-thick thermal oxide/Si(100) and 500$\AA$-Si$_3$N$_4$LPCVD/Si (100) wafers were prepared, and wet cleaned to activate the surface as hydrophilic and hydrophobic states, respectively. Cleaned wafers were premated wish facing the mirror planes by a specially designed aligner in class-100 clean room immediately. Premated wafer pairs were annealed by an electric furnace at the temperatures of 400, 600, 800, 1000, and 120$0^{\circ}C$ for 2hours, respectively. Direct bonded wafer pairs were characterized the bond area with a infrared(IR) analyzer, and measured the bonding interface energy by a razor blade crack opening method. We confirmed that the bond interface energy became 2,344mJ/$\m^2$ when annealing temperature reached 100$0^{\circ}C$, which were comparable with the interface energy of homeogenous wafer pairs of Si/Si.

Effects of Base Paper Properties and the Composition of Adhesives on the Physical Properties of Multilayered Paper (원지특성 및 접착제 조성이 합지 물성에 미치는 영향)

  • Kim, Tae-Young;Jung, Yang-Jin;Jang, Yoon-Jin;Yoon, June-Hee;Heo, Yong-Dae
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.40 no.4
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    • pp.34-42
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    • 2008
  • Generally, paper multilayering was performed before wet pressing process. However, sheets whose characteristics are different could be put together at the dry state by adhesives for the specialty paper products. In this paper, potential adhesives such as PVAc, oxidised starch, latex, and PVA were chosen and multilayering of several sheets was performed in laboratory scale. The effects of base paper properties and the composition of adhesives on the physical properties of multilayering paper were investigated. Physical properties such as bonding strength and stiffness were measured. For the practical reasons, mill trial was also executed. According to the result of laboratory tests and mill trial test, the physical properties of multilayered paper were greatly affected by the composition of adhesives and it was found that PVAc showed the best performance in all its aspects among four adhesives. Oxidised starch had an advantage of high stiffness and PVA gave high bonding strength to the multilayered paper. And it was also found that the properties of base paper showed the great influences not only on multilayering process, but also on the physical properties of the multilayered paper.

Development of a Spray-Injection Patching System and a Field Performance Evaluation of 100% RAP Asphalt Mixtures using a Rapid-Setting Polymer-Modified Asphalt Emulsion (아스팔트 긴급보수용 스프레이 패칭 장비 개발 및 현장 적용성 평가)

  • Han, Soo Hyun;Lee, Sang Yum;Rhee, Suk Keun;Kwon, Bong Ju
    • International Journal of Highway Engineering
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    • v.20 no.1
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    • pp.77-85
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    • 2018
  • PURPOSES : The purpose of this study was to develop an urgent road-repair system and perform a field applicability test, as well as discover the optimum mix design for machine applications compared to the optimum mix design for lab applications. METHODS : According to reviews of the patent and developed equipment, self-propelled and mix-in-place equipment types are suitable for urgent pavement repair, e.g., potholes and cracks. The machine-application mix design was revised based on the optimum lab-test mix design, and the field application of a spray-injection system was performed on the job site. The mixture from the machine application and lab application was subjected to a wet-track abrasion test and a wheel-tracking test to calibrate the machine application. RESULTS and CONCLUSIONS : This study showed that the binder content could differ for the lab application and the machine application in the same setting. Based on the wet-track abrasion test result, the binder contents of the machine application exceeded the binder contents of the lab application by 1-1.5% on the same setting value. Moreover, the maximum dynamic stability value for the machine application showed 1% lower binder contents than the maximum lab-application value. Collectively, the results of the two different tests showed that the different sizes and operating methods of the machine and lab applications could affect the mix designs. Further studies will be performed to verify the bonding strength and monitor the field application.