• Title/Summary/Keyword: Water soluble components

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Anti-oxidative Capacity Analysis of Water-Soluble Substances According to Varieties and Maturity Stages in Mulberry Leaves and Fruits (뽕나무 품종별.시기별 뽕잎과 오디의 항산화능 분석)

  • Kim Hyun-Bok
    • Journal of Sericultural and Entomological Science
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    • v.47 no.2
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    • pp.62-67
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    • 2005
  • Much attention has been focused on the activity of the natural antioxidants present in fruits and vegetables, because potentially these components may reduce the level of oxidative stress. Especially, mulberry leaves containing many natural components are considerable resource far natural antioxidants. The antioxidant capacity of mulberry leaves was investigated with minilum L-100 device and ARAW-KIT (anti-radical ability of water-soluble substance), in comparison to the ascorbic acid. The appropriate conditions for pre-treatments of mulberry leaves were 80% MeOH, 30 sec. vortex mixing. The antioxidant capacity of 16 varieties was 3303.4 nmol (ascorbic acid equivalents) at opening stage of five leaves in spring. The highest stage of antioxidant capacity (3708.0 nmol) and yield rate was just before the coloration stare with anthocyanin in fruits, whereas the lowest stage was middle of June (2231.6 nmol) and about two months growing stage after summer pruning (2064.6 nmol). But after summer pruning, the antioxidant capacity of mulberry.

Chemical Composition of Respirable PM2.5 and Inhalable PM10 in Iksan City during Fall, 2004 (익산지역 가을철 대기 중 호흡성 및 흡입성 먼지입자의 화학조성)

  • Kang, Gong-Unn
    • Journal of Environmental Health Sciences
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    • v.36 no.1
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    • pp.61-71
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    • 2010
  • Intensive measurements of airborne respirable $PM_{2.5}$ and inhalable $PM_{2.5}$ were conducted in the downtown area of Iksan city. The $PM_{2.5}$ and $PM_{2.5}$ samples were collected twice a day in the Iksan city of Korea from October 17 to November 1, 2004. The purpose of the study was to determine the inorganic water-soluble components and trace elements of $PM_{2.5}$ and $PM_{2.5}$ in the atmospheric environment and estimate the contribution rate of major chemical components from a mass balance of all measured particulate species. The chemical analysis for PM samples was conducted for water-soluble inorganic ions using ion chromatography and trace elements using PIXE analysis. The mean concentrations of respirable $PM_{2.5}$ and inhalable $PM_{2.5}$ were $51.4{\pm}29.7$ and $79.5{\pm}39.6\;{\mu}g/m^3$, respectively, and the ratio was 0.62. The ion species of $NO_3$, $SO_4^2$, and $NH_4^+$ were abundant in both $PM_{2.5}$ and $PM_{2.5}$. These components predominated in respirable $PM_{2.5}$ fraction, while $Na^+$, $Mg^{2+}$, $Ca^{2+}$ mostly existed in coarse particle mode. Elemental components of S, Cl, K, and Si were abundant in both $PM_{2.5}$ and $PM_{2.5}$. These elements, except for Si, were considered to be emitted from anthropogenic sources, while Si, Al, Fe, Ca existed mainly in coarse particle mode and were considered to be emitted from crustal materials. The averaged mass balance analysis showed that ammonium nitrate, ammonium sulfate, crustal component, and other trace elements were composed of 18.4%, 13.2%, 4.8%, 3.5% for PM2.5 and 17.0%, 11.6%, 13.7%, 4.4% for $PM_{2.5}$, respectively.

Changes of Sensory Characteristics in Red Pepper by Different Extraction Conditions (추출 조건에 따른 고추 수용액의 관능적 특성 변화)

  • Lee, Hyun-Duck;Lee, Cherl-Ho
    • Korean Journal of Food Science and Technology
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    • v.30 no.3
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    • pp.535-541
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    • 1998
  • The soluble solid of red pepper extracted by water was evaluated with descriptive analysis by 10 trained sensory subjects. In the result of the sensory evaluation, the character notes on the flavor of soluble solid were expressed as pungency, sweet, fresh sour, bitter, alcoholic, meaty, chalkiness and astringent. The score of redness was the highest at $4^{\circ}C$ and decreased after 2 hr at $90^{\circ}C$ and the score of sensory pungency was more than 50 and was especially higher at $40^{\circ}C\;and\;90^{\circ}C$. Principal component analysis of the mean ratings showed that kochoojang (fermented red pepper paste) and chigae (meat and vegetable stew) differed from kimchi (unfermented kimchi) and that they had unique sensory attributes. The first two principal components could be explained by 51% of all the components and the taste of soluble solid at $40^{\circ}C$ was highly correlated with sensory attributes such as meaty, fresh sour and sweet and that at $4^{\circ}C$ was chiefly correlated with color components and the taste of soluble solid at $60^{\circ}C$ was showed close relation to astringent, alcoholic and pungency.

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Review of the Determination Methods for Metal Compounds with Different Occupational Exposure Limits Depending on Solubility (용해도에 따라 노출기준이 다른 금속화합물의 정량방법 고찰)

  • Park, Seung-Hyun;Ro, Jiwon;Jang, Miyeon
    • Journal of Korean Society of Occupational and Environmental Hygiene
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    • v.30 no.2
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    • pp.87-98
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    • 2020
  • Objective: The purpose of this study was to propose a sequential procedure for the simultaneous analysis of soluble and insoluble metal compounds. Methods: Methods for sampling and analyzing metal compounds such as ISO standards, NIOSH methods, HSE methods, and OSHA methods were reviewed. Results: Some metals have different OELs depending on the solubility of the compound. Therefore, we should take into account these characteristics and perform an exposure assessment. Soluble metal compounds are first extracted from the filter, and then the filter is digested by acids to analyze residual insoluble components. The extraction of soluble compounds can be completed by agitation for about 60 minutes with a leach solution (water) in a water bath at 37℃. For the analysis of insoluble compounds, the sample filter and the filtration filter remaining after the extraction of the soluble compounds are analyzed. This allows simultaneous determination of soluble and insoluble metal compounds. For hexavalent chromium compounds, soluble hexavalent chromium can first be extracted from the filter by using sulfate buffer. The insoluble hexavalent chromium remaining in the filter can then be extracted using carbonate buffer. Conclusion: Workers are often exposed to many hazardous substances with different exposure limits at industrial sites. The OELs for compounds of the same metal can be set differently depending on solubility. This study can help evaluate a worker's exposure to metal compounds by suggesting methods for the simultaneous determination of soluble and insoluble metal compounds.

A Study on the Characteristics of Particulate Matter in the Coastal Regions (해안지역에서 입자상물질의 특성에 관한 연구)

  • 최민규;조기철;강충민;여현구;김희강
    • Journal of Environmental Health Sciences
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    • v.24 no.3
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    • pp.114-123
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    • 1998
  • Particulate matters(less than 10 $\mu$m, PM10) at Kanghwa and Yangyang, which are located in the western and the eastern coastal regions in Korea, were measured in using low volume air sampler from December 1995 to November 1996, and their characteristics were investigated from the view point of background level.(and in order to characterize the particulate matters.) The particulate matters were analyzed for major water soluble ionic components(SO$_{4}^{2-}$, NO$_{3}^{-}$, Cl$^{-}$, Na$^{+}$, NH$_{4}^{+}$, K$^{+}$, Mg$^{2+}$ and Ca$^{2+}$) by ion chromatography. Mass concentrations of particulate matters were $48.77 \pm 22.45 \mug/m^{3}$ at Kanghwa and $54.04 \pm 32.98 \mug/m^{3}$ at Yangyang and SO$_{4}^{2-}$, NO$_{3}^{-}$ and NH$_{4}^{+}$ contributed largely to water soluble ionic components. nss(non sea salt)-SO$_{4}^{2-}$, contributed more than 95 percentage to SO$_{4}^{2-}$ and nss-K$^{+}$ and nss-Ca$^{2+}$ also contributed high percentages to K$^{+}$ and Ca$^{2+}$. It was supposed that most SO$_{4}^{2-}$, was originated from anthropogenic sources, and K$^{+}$ and Ca$^{+}$ were mainty originated from soil. The results of factor analysis suggested possibility of interpreting the correlation between air pollutants and regional characteristics.

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Anti-metastatic and Immunomodulating Activity of Water-Soluble Components from Five Mushroom Extracts

  • Yoo, Hwa-Seung;Han, Sung-Soo;Kim, Jung-sun;Cho, Chong-Kwan;Lee, Yeon-Weol;Park, Sang-Yong;Lee, Soo-Jin
    • The Journal of Korean Medicine
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    • v.30 no.3
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    • pp.61-69
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    • 2009
  • Objectives : This experiment was conducted to evaluate the inhibitory effects against lung metastasis and promotion of splenocytes by water-soluble components from five mushrooms extracts (WEFM): Garnoderma frondosa, Corious versicolor, Codyceps militaris, Hericium erinaceus and Lentinula edodes. Methods : Colon 26-L5 carcinoma cells were injected through the tail vein to induce lung metastatic cancer. Changes in weight of lung were observed and cytokine level was analyzed to evaluate immunological changes. Results : Oral administration of WEFM resulted in a significant inhibition of lung metastasis after intravenous injection of colon 26-L5 cells in a dose-dependent manner. There was also a significant increase in T cell and B cell mitogenic stimuli and production of IFN-g by splenocytes stimulated with Con A compared to untreated controls. Conclusion : WEFM may have anti-tumor activities via Th1-type dominant immune responses.

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Antibacterial Activity of Water Soluble Components of Elfvingia applanata Alone and in Combinations with Quinolones

  • Kim, Young-So;Eo, Seong-Kug;Oh, Ki-Wan;Lee, Chong-Kil;Lee, Young-Nam;Han, Seong-Sun
    • Mycobiology
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    • v.29 no.1
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    • pp.11-14
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    • 2001
  • A preparation of water soluble components(EA) was made from carpophores of Elfvingia applanata(Pers.) Karst and its in vitro antibacterial activity on a number of bacterial species was examined by macrobroth dilution assay. Among 16 species of bacteria tested, the most potent antibacterial activity was observed against Staphylococcus epiderrnidis and Proteus vulgaris, of which MICs were 1.25 mg/ml. To investigate the antibacterial effects in combinations of EA with quinolone antibiotics, such as ciprofloxacin, enoxacin, lomefloxacin, norfloxacin, and ofloxacin, the fractional inhibitory concentrations(FICs) and the fractional inhibitory concentration indices(FICIs) for four bacterial strains were determined by macrobroth dilution checkerboard assay. Combinations of EA and quinolones exhibited either additive or indifferent effects of antibacterial activity in most instances. However, both synergistic and antagonistic effects were not observed in any cases.

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A Study on the Characteristics of Ambient Suspended Particulate Matter at Coastal Area, Kangwha (해안지역 대기부유미립자상 물질의 특성에 관한 연구)

  • 강공언;우상윤;강병욱;김희강
    • Journal of Environmental Health Sciences
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    • v.20 no.4
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    • pp.1-9
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    • 1994
  • In order to investigate the regional level of air pollutants at Kangwha island situated on the western coast in Korea, the suspended particulate matter samples were collected by using the low volume air sampler on ten interval from March 1992 to February 1993 and the mass concentration of suspended particulate matter (SPM) and the chemical composition of water-soluble major ionic components in SPM samples were measured. During the sampling period, the average concentration of SPM under diameter 10 $\mu$m was found to be 48 $\mu$g/m$^3$ (+ 12). The seasonal concentration of SPM was showed in order of spring>fall>winter>summer. It was considered that higher concentration on spring than other season was affected by the long-range transport of Yellow sand particulate from China continent and lower concentration on summer by the washout and rainout effect of large rainfall. The content of water-soluble component in SPM samples was founded to be about 31% (14.69 $\mu$g/m$^3$) and 65% was unknown or unanalyzed. The content of cationic component showed in order of NH$_4^+$ (44.6%)>Na$^+$ (21.2%)>K$^+$ (14.7%)>Ca$^{2+}$ (13.6%)>Mg$^{2+}$ (5.9 %) and the content of anionic component SO$_4^{2-}$ (62.5%)>NO$_3^-$ (22.3%)>Cl$^-$ (15.2%), respectively. This fact indicates that ammonium and sulfate ion of water-soluble component in SPM sample were dominant in this region. From the chemical composition of water-soluble component, the most of Na$^+$, Mg$^{2+}$ and Cl$^-$ were originated from seawater source but K$^+$, Ca$^{2+}$ and SO$_4^{2-}$ were originated from other non-marine source. The contribution of seasalt to the composition of precipitation was 23%.

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Formation and Chemical Characteristics of Dewfall in Western Busan Area (부산 서부지역의 이슬 생성과 화학적 특성)

  • Jeon Byung-Il;Hwang Yong-Sik;Park Moon-Po
    • Journal of Environmental Science International
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    • v.13 no.12
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    • pp.1079-1088
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    • 2004
  • In order to understand chemical characteristics and dewfall formation in western Busan area, we analysed monthly distribution of dewfall, and investigated the correlation between dewfall formation amount and meteoro­logical factors. This study used the modified teflon plate $(1m{\times}1m)$ at Silla university in Busan from August 2002 to April 2003. In order to estimate qualitatively water soluble components, IC, ICP and UV methods for water soluble ions are also used respectively. Dewfall amount of sampling periods (47 day) collected 3.8 mm. Meteorological conditions for the formation of dewfall above $50\;g/m^{2}$ showed that temperature diurnal $range(^{\circ}C)\;was\;5.6^{\circ}C$ above, cloud amounts (1/10) at dawn of the sampling day was 7/10 below, mean wind speed at dawn (0~6hr) of the sampling day was 4.4 m/sec below, and mixing ratio at 6hr of the sampling day was 3.2 g/kg above. Distribution of water soluble ions in dewfall founded the highest concentration (206.1\;{\mu}eq/{\ell}\;for\;SO_{4}^{2-},\;42.4\;{\mu}eq/{\ell}\;for\;NH_{4}^{+},\;249.2\;{\mu}eq/{\ell}\;for\;Ca^{2+},\;and\;42.0\;{\mu}eq/{\ell}\;for\;Mg^{2+})$ during the March, the lowest concentration $(73.0\;{\mu}eq/{\ell}\;for\;SO_{4}^{2-},\;4.6\;{\mu}eq/{\ell}\;for\;NH_{4}^+\;and\;72.7\;{\mu}eq/{\ell}\;for\;Ca^{2+})$ during the August. Monthly equivalent ratio of $[SO_{4}^{2-}]/[NO_{3}^-]$ showed the highest value (4.99) during the October, the lowest value (1.84) during the August, and the mean value was 3.45.

Characteristics of $PM_{2.5}$ in Kanghwa (강화에서의 $PM_{2.5}$ 특성)

  • 최민규;여현구;임종억;조기철;김희강
    • Journal of Korean Society for Atmospheric Environment
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    • v.16 no.6
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    • pp.573-583
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    • 2000
  • In order to investigate the characteristics of PM(sub)2.5 in the background area, the following pollutant were measured from February 1996 to June 1999 in Kanghwa: PM(sub)2.5 mass, sulfate, nitrate, chloride, ammonium, sodium, calcium, magnesium and potassium. The mean concentration of PM(sub)2.5 mass was 25.8$\pm$1.2$\mu\textrm{g}$/㎥(range 5.18~85.74). This value was higher than the annual PM(sub)2.5 US NAAQS(15$\mu\textrm{g}$/㎥) and the total number of samples higher than the 24-h PM(sub)2.5 US NAAQS(65$\mu\textrm{g}$/㎥) was seven. PM(sub)2.5 masses also showed temporal variations both yearly and seasonally. Total water soluble ions constituted about 45% of PM(sub)2.5 miss, and sulfate, nitrate and ammonium were main components in water soluble ions. Compared with the literature data from other areas, the measured PM(sub)2.5 concentrations were relatively high.

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