• Analytical Science and Technology
• /
• v.27 no.6
• /
• pp.292-299
• /
• 2014

Iopromide is an X-ray contrast agent that has been detected frequently with high concentration level in surface waters. Structural characterization of degradation products and measurement of degradation efficiency of iopromide by an electron beam irradiation were performed. For the fortified sample with iopromide, electron beam irradiation (UELV-10-10S, klysotrn, 10 MeV, 1 mA and 10 kW) was performed. The chemical structures of I_D_665 and I_D_663, which are degradation products of iopromide, were proposed by interpretation of mass spectra and chromatograms by LC/ESI-MS/MS. The mass fragmentation pathways of mass spectra in tandem mass spectrometry were also proposed. Iopromide was degraded 30.5~98.4% at dose of 0.3~5 kGy, and 97.8~30% in the concentration range $0.5{\sim}100{\mu}g/kg$ at electron beam dose of 0.3 kGy, respectively. Thus, increased degradation efficiency of iopromide by electron beam irradiation was observed with a higher dose of electron beam and lower concentration.

• Proceedings of the KSR Conference
• /
• 2010.06a
• /
• pp.1416-1422
• /
• 2010

Monorail has been classified as straddled type and suspended type. However, Inchon Wolmi Eunha rail, a center guide type first ever introduced in the world, uses a new concept Y-Beam as guide rail. Since Y-Beam takes horizontal loads of monorail through guide wheels, it is an essential structure for the safe operation along with concrete surface and steel beam which take vertical loads through main tires. This study presents the characteristic and reliability of Y-Beam and Y-Beam fixture, clamp, which are not only taking horizontal loads but also guarantying both guiding and stability of monorail and holding power supply line.

• Proceedings of the Korean Society of Precision Engineering Conference
• /
• 2005.06a
• /
• pp.1518-1521
• /
• 2005

The application of focused ion beam (FIB) technology in micro/nano machining has become increasingly popular. Its usage in micro/nano machining has advantages over contemporary photolithography or other micro/nano machining technologies such as small feature resolution, the ability to process without masks and being accommodating for a variety of materials and geometries This paper focus to apply the sputtering technology accumulated by experiments to 3d structure fabrication with high resolution. Therefore some verifications and discussions of the characteristics of FIB sputtering results according to focal length were described in this paper. And we suggested the definition of rectangular pattern profile and made the verifications of sputtering results based on definition of it.

• Transactions of the Korean Society of Automotive Engineers
• /
• v.10 no.4
• /
• pp.158-165
• /
• 2002

This Paper deals with the headlamp lens surface temperature distribution of p/c headlamp using the three categories of H4 halogen bulbs. Glass is gradually replaced by P/C for the lens material off vehicle headlamp due to the weight reduction and stream lined body of a vehicle. With this trend, the newly established standards for a headlamp with a P/C lens in Europe requires that the heat generated by a bulb should not distort the lens surface. Also the requirements fur the bulb of a headlamp are being enforced in U.S.A & Europe. However, such requirements are not established yet in Korea. By using three kinds (60/55w, 100/90w, 130/90w) of H4 halogen bulbs in this experiment, the surface temperature distribution and Max. temperature on the lens were measured. The results of this study implies the necessity of requirement fur the bulb off headlamp.

• Journal of Welding and Joining
• /
• v.9 no.2
• /
• pp.29-36
• /
• 1991

6mm 두께의 AISI 316 스테인레스강의 레이저 용접 특성에 대해서 고찰하였다. 3kW C $O_{2}$레이저를 사용하였으며, 레이저 빔은 TE $M_{00}$모우드였고 연속파이었다. 용입 깊이, 비드 폭, 고온 크랙, 가공등의 특성을 고찰하는데 있어서, 레이저 출력은 1kW에서 2.5kW까지, 용접 속도는 5.1m/min까지 적용하였다. 3차원 열전달 방정식에 의한 용입 깊이와 비드 폭에 대한 예측치와 실험 결과를 비교하였는데, 서로 잘 일치하였다.다.

• Korean Journal of Optics and Photonics
• /
• v.9 no.3
• /
• pp.186-190
• /
• 1998

We fabricated a diode-side pumped high power Nd:YAG laser with a gold coated flow tube(diameter of 10mm) and three sets of 140W diode bar. The diameter of Nd:YAG rod was 6mm and its length was 130mm. We obtained 130W cw power from a linear resonator with an 11% output coupler, which corresponds to the slope efficiency of 43% and the optical efficiency of 31%. The measured beam quality factor(M$^2$) reached about 85 which is fairly large due to the large size of the rod. Thermal lensing of the rod was measured to be 5.3-7.4D/$kW_{pump}$ when the laser was operating.

• Korean Journal of Crystallography
• /
• v.3 no.2
• /
• pp.85-97
• /
• 1992

EBFZM( Electron Beam Floating Zone Melting) 법을 이용하여 몰리브덴에서의 금속계 불순물과 침입형 불순물의 정련기구 및 단결정 성장기구를 연구하 였다. Fe, Cr, Co등의 금속계 불순물은 몰리브덴과의 평형증기압의 차이에 따른 불순물의 선택적 증발에 의하여 우수한 정련효과를 나타내며, 몰리브덴보다 응점이 높은 Ta, W는 잘 제거되지 않았다. 한편 대역 정제에 의한 정련효과는 미약함을 확인하였다. EBF ZM은 C,0,N등의 침입형 불순물의 정련에도 효과적 이었다. 본 연구의 모든 조건에서 몰리브덴은 단결정으로 성장하였으며 2차 재결정 epitaxy에 의한 단결 정 성장기구가 제시되었다. 몰리브덴 단결정 내의 전 위밀도는 strain-anneal법에 의한 단결정의 경우보다 높았으며,본 실험의 열처리 조건에서는 변화하지 않았다. The purification and single crystal growth mechanisms of molybdenum were analysed in EBFZM ( electron beam floating zone melting). Metallic impurities of Fe, Cr, Co were purified efficiently but Ta and W were not removed well in this study. It was due to a preferential evaporation of the elements caused by the difference in equillibrium vapor pressure between the elements and molybdenum. The pu- rification effect by zone refining was not significant. The EBFZM also refined the interstitial impurities of C, 0 and N, effectively. The single crystals of molybdenum were grown regardless of the experimental conditions and the secondary recrystallization epitaxy was surge sled as a growth mechanism. The dislocation density in single crystal was higher than that by strain-anneal method, and was not reduced by heat treatments.

• Proceedings of the Korean Society of Precision Engineering Conference
• /
• 2005.06a
• /
• pp.1186-1189
• /
• 2005

Focused Ion Beam machining is an attractive approach to produce nano-scale 3D structures. However, like other beam-based manufacturing processes, the redeposition of the sputtered material during the machining deteriorates the geometric accuracy of ion beam machining. In this research a new approach to reduce the geometric error in FIB machining is introduced. The observed redeposition phenomena have been compared with existing theoretical model. Although the redeposition effect has good repeatability the prediction of exact amount of geometric error in ion beam machining is difficult. Therefore, proposed method utilizes process control approach. Developed algorithm measures the redeposition amount after every production cycle and modifies next process plan. The method has been implemented to a real FIB machine and the experimental results demonstrated considerable improvement of five micrometer-sized pocket machining.

• Journal of the Korean Vacuum Society
• /
• v.12 no.1
• /
• pp.64-69
• /
• 2003

Using a high fewer electron beam gun (max. power 20 kW), Gadolinium (Gd, atomic number 64) metal was melted and the temperature distribution of melted surface was measured. With proper optical filters and the adjustment of aperture of lens, the radiation of melted surface was received by a ccd camera and its signal transferred to a computer. The real time monitoring of melted surface with a variation of electron beam Power was Possible and stable operation of electron beam was achieved. It was found that the max. temperature measured by a ccd camera with an assumption of blackbody radiation of melted Gd surface and adaption of Planet's law was above 100~$200^{\circ}C$ compared to that measured by a pyrometer in the same e-beam power.

• Korean Journal of Optics and Photonics
• /
• v.19 no.2
• /
• pp.144-149
• /
• 2008

Thermal distortion of the laser mirrors which are the Coude mirrors of the laser beam director and the wavefront error caused by the thermal distortion are studied. Coude mirrors consist of three relay mirrors and one fast steering mirror. The mirrors have reflectivity of 99.5% with respect to the laser wavelength of $3.8\;{\mu}m$, and absorption of 500 W per second. Thermal distortion and its related wavefront errors are studied with laser beam irradiation for 5 seconds. For the relay mirror, the wavefront error is 334 nm_PV, 98 nm rms and for fast steering mirror, $11.5\;{\mu}m$_PV, $3{\mu}m$ rms.