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Estimaion of the sintering and forging characteristics of the W/Cu nanocomposite powders produced by the spray conversion process (Spray conversion 법으로 제조된 W/Cu 나노복합분말의 소결특성 및 단조특성 평가)

  • 김태형;노준웅;김은표
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2002.11a
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    • pp.36-36
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    • 2002
  • 최근 한국기계연구원에서 개발된 Mechanochemical process (MCP)는 Spray conversion 법에 의하여 나노크기의 W/Cu 복합 분말을 제조하는 방법으로서, 현재 (주)나노테크에서 산업화를 위한 시험/개발이 진행 중이다. 이 방법에 의하여 W /1 0 ~ 40wt. %Cu 조성의 초미렵 W/Cu 복합 분말의 양산화가 가능하게 됨으로써, 나노복합분말을 사용한 초미립 W/Cu 합금의 소결 제조 연구 역시 나 노태크에서 분말사업화와 동시에 수행되고 있다. 현재 Spray conversion 법으로 제조되고 있는 W/Cu 나노복합분말 및 그 소결체는 Cu의 조성범 위에 따라 민수용 및 군수용 제품으로의 적용이 시도되고 있으며, 각기 특성향상을 목표로 각 적용 분야에서 요구되는 제반 성능에 대한 검토가 이루어지고 있다. 특히 군수용의 목적으로 사용될 경우, 정적 및 동적부하상태에서 재료의 균일한 변형이 가장 중요한 특성이다. 현 개발품의 경우, 일반 W 빛 Cu 원료에 비하여 상대적으로 높은 순도의 원료를 사용하였기 때문에 분말 및 소재상태 에서의 순도가 높아서, 연성을 저하시키는 것으로 알려진 기지상내 합금원소 또는 interface 게재물 이 존재할 가능성이 매우 낮다. 또한 초미립 W 입자들과 Cu 상의 혼합도가 극대화된 상태이기 때문에 상대적으로 저옹에서도 완전치밀화된 미세조직을 얻을 수 있는데, 이는 분말상태의 균일한 미세구조를 유지할 수 있으며, 동시에 W 업자간의 과도한 neck 형성을 방지함으로써 기계적 변형시 재료의 연성 향상이 기대된다. 이러한 W/Cu 나노복합분말 소결체의 특성은 균일한 밀도분포와 동시에 과도한 동적 부하상태에서 균일한 변형이 보장되어야만 하는 특정 군수용 목적에 잘 부합하는 것으로 판단된다. 본 고에서는 상기한 W/Cu 나노복함분말을 사용하여 균일한 미세구조를 가지는 완전치밀화된 소결재를 제조하는 과정과 제조된 소결재를 향후 군수용 제품에 척용시키기 위하여 진행된 단조특성에 대한 연구결과틀을 재료의 미세구조척 관점에서 논의하였다.

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Relationship Between Lodging-Related Characteristics and Field Lodging in Rice (벼 도복 관련형질과 포장도복과의 관계)

  • 임준택;권병선;정병관
    • KOREAN JOURNAL OF CROP SCIENCE
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    • v.36 no.4
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    • pp.319-323
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    • 1991
  • To determine how closely related to field lodging for several characters affecting the field lodging for several characters affecting field lodging, and to obtain the basic information for selection of lodging resistance genotype, an experiment was conducted with 10 varieties from May to Oct., 1990 at the experimental field in Sunchon Xational University. Culm length, dry weight per unit culm length (W/1), bending moment per unit culm diameter (W1/d), lodging index (L), bending load ratio (W1/P), and index of critical lodging load(W$_{s}$$^{2}$/1$^4$) were the most closely related characters to field lodging. Culm length showed highly significant positive correlation coefficient with field lodging(r=0.7607), but it may be undesirable to judge lodging resistance of genotype by culm length itself without consideration of culm stiffness. Considering the difficulty and time-consuming to measure the character, clum length, W/1, W1/d, and W$_{s}$$^{2}$/1$^4$ were easy to measure and hence would be the most useful variables to judge the lodging resistance of genotype. Culm diameter, cross sectional area of culm, thickness of culm wall, and the second inertia moment of cross section of culm were not correlated with field lodging at all. Breaking strength of culm showed significantly negative correlation coefficient (r=-0.3986) with field lodging.ing.

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Retrogradation Characteristics of Jeungpyun by Different Milling Method of Rice Flour (쌀가루의 제분방법에 따른 증편의 노화도 특성)

  • Kim, Young-In;Kum, Jun-Seok;Lee, Sang-Hyo;Lee, Hyun-Yu
    • Korean Journal of Food Science and Technology
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    • v.27 no.6
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    • pp.834-838
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    • 1995
  • The relative retrogradation of Jeungpyun investigated with different milling methods of rice flour. The relative retrogradation of Jeungpyun was reduced in order that of W-C, W-P, D-M, D-J in DSC(Differential Scanning Calorimetry) method while W-C, D-M, D-J, W-P in Diastase method. In wet milling method, the relative retrogradation of Jeungpyun by pin mill (W-P) was lower than Jeungpyun by colloid mill (W-C). In dry milling method, the relative retrogration of Jeungpyun by jet mill (D-J) was lower than Jeungpyun by micro mill(D-M). The relative retrogradation of Jeungpyun by DSC method was similar to the diastase method. The relative retrogradation of Jeungpyun was decreased with decreasing particle size and setback value for amylogram and increasing damaged starch.

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An Analysis on the RFI of Non-GSO/MSS System into M/W Radio Stations (M / W 무선국에 미치는 비정지궤도 이동위성 시스템의 전파간섭 분석)

  • 이성수;이형수;강영흥
    • The Journal of Korean Institute of Electromagnetic Engineering and Science
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    • v.8 no.5
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    • pp.504-515
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    • 1997
  • In this paper, interference of non-GSO/MSS system into M/W radio stations has been analyzed as two aspects. One is that PDF(Power Flux Density) levels, which are received by M/W radio stations from non-GSO satellites, were simulated and compared with the threshold level specified in ITU-R SF.357. The other is that C/I values, which have been utilized in estimating interference between conventional fixed services, were simulated and analyzed by means of calculating excess time percent and duration below the C/I protection ratio. As the results, it was shown that interference levels received by M/W stations from non- GSO/MSS satellites don't exceed above the threshold level at all, even if changing parameters related with M/W stations. In addition, the excess percent time below the interference protection ratio is a long term of 32% in the case of Iridium interfering into a M/W stations route, but only a short term of 1.71% in the case of Globalstar interfering into a M/W stations route.

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A Distribution Function Analysis of Photopic and Scotopic Curves (Photopic과 Scotopic 곡선의 분포함수 유도 및 분석)

  • Kim, Yong Geun
    • Journal of Korean Ophthalmic Optics Society
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    • v.5 no.2
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    • pp.157-161
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    • 2000
  • The Eye sensitivity in the difference conditions of a light source intensity consists of two functions by the receptor of cone and rod according to a wavelength. We derived a distribution function of $P({\lambda})=A{\cdot}e^{-({\lambda}-{\lambda}_0)^2/2W^2}$ using a respond probability of the receptor of cone-rod for a photon. It was well applied for a CIE eye's sensitivity curve of a wavelength, we obtained values in case of a relative sensitivity. A = 106.4, ${\lambda}_0=559.2$, W = 83.5 for a photopic and A = 99.3 ${\lambda}_0=502.6$, W = 79.5 for a scotopic, and in case of a sensitivity curve using 1m/W units. $A=7.2{\times}10^4$, ${\lambda}_0=559.2$, W = 83.5 for a photopic and $A=1.6{\times}10^5$, ${\lambda}_0=502.6$. W = 79.5 for a scotopic.

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Failure Analysis and Accelerated Life Test of MoxW1-xSi2 Haters Fabricated by SHS process (SHS 공정으로 제조된 MoxW1-xSi2 발열체의 가속수명시험과 고장분석)

  • Lee, Dong-Won;Lee, Sang-Hun;Kim, Yong-Nam;Lee, Heesoo;Lee, Sung-Chul;Koo, Sang-Mo;Oh, Jong-Min
    • Journal of IKEEE
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    • v.21 no.3
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    • pp.252-255
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    • 2017
  • $Mo_xW_{1-x}Si_2$ heaters were fabricated by self-propagating high-temperature synthesis (SHS) process and post sintering process. To validate the reliability of the $Mo_xW_{1-x}Si_2$ heaters, the accelerated life test (ALT) was conducted, and then lifetime to $Mo_xW_{1-x}Si_2$ heaters was estimated by using Minitab programs. Also, the failure analysis of $Mo_xW_{1-x}Si_2$ heaters after ALT was performed through electrical and structural properties. As the results, it was confirmed that the dominant failure mode of $Mo_xW_{1-x}Si_2$ heaters is the crack formation in heaters and the delamination of protective $SiO_2$ layers.

The anti-histamine effect of water soluble alkaloids extracted from solanum nigrum L. (용규에서 추출된 수용성 알칼로이드성분의 항히스타민 효과)

  • Shen, Chang Zhe;Park, Jung Keun;Kim, Choul Goo;Chun, Hyun Ja;Kim, Il Kwang
    • Analytical Science and Technology
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    • v.29 no.4
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    • pp.186-193
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    • 2016
  • The whole herbs of solanum nigrum L were extracted in boiling water (SNL-W), and the extracts were separated with butyl alcohol fraction (SNL-W/B) and aqueous fraction (SNL-W/W) by the solvent extraction method. The total alkaloid and total saponin content mensuration were used to identify the alkaloid composition of methanol fraction extracted from the aqueous fraction. The venom of honey bee was used to induce the rat peritoneal mast cell to secreting the histamine. The results show that the water soluble alkaloid composition of solanum nigrum L (SNL-W/W/M) has a significant inhibitory effect on the histamine release.

Effects of Lysozyme, Clupeine, Sucrose, and Sodium Chloride on the Foaming Properties of Egg Albumen and Powdered Beef Plasma (Lysozyme, Clupeine, Sucrose 및 Sodium Chloride가 난백 및 분말 우혈장의 거품성에 미치는 영향)

  • 양승택;최정민
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.24 no.1
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    • pp.82-91
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    • 1995
  • This study was designed to elucidate the effects of lysozyme, clupeine, sucrose, and sodium chloride on the foaming properties of egg albumen and podered beef plasma. Surface tensions of egg albumen(5%, w/w) and powdered beef plasma(5%, w/w) adding to lysozyme, clupeine, sucrose, and sodium chloride were 46.8$\pm$0.379~52.4$\pm$ 0.404dyne/cm(control, 51.5$\pm$0.416dyne/cm) and 54.6$\pm$0.231~60.7$\pm$0.467dyne/cm(control, 53.9$\pm$0.153dyne/cm), respectively. Turbidities of the solutions were 77.0$\pm$0.058~97.9$\pm$ 0.058(control, 91.2$\pm$0.153) and 90.3$\pm$0.058~98.5$\pm$0.115 (control, 82.7$\pm$0.100), respectively. Surface hydrophobicities of the solutions were 524~811(control, 485) and 5102~ 7128(control, 4665), respectively. The solution with high hydrophobicity revealed good foaming properties. Analysis of egg albumen and powdered beef plasma foam by electrophoresis showed that lysozyme was retained for a long time in foam. The optimal concentraitons of lysozyme and clupeine for foaming properties were 0.5% and 0.3% in egg albumen(5%, w/w) and 0.5% and 0.5% in powdered beef plasma(5%, w/w), respectively. In case of egg albumen, sodium chloride dominantly enhanced the action of clupeine. The addition of 0.3% clupeine with sodium chloride(2.0M) to egg albumen(5%, w/w) increased overrun and foam stability by 119.5% and 70.9%, respectively. The addition of 0.5% clupeine to powdered beef plasma(5%, w/w) also increased overrun and foam stability by 43.7% and 127.3%, respectively.

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Effects of Methanol Extract of Prosomillet on Cholesterol and Fatty Acid Metabolism in Rat

  • Cho, Sung-Hee;Jung, Seung -Eun;Lee, Hye-Kyung;Ha, Tae-Youl
    • Preventive Nutrition and Food Science
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    • v.4 no.3
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    • pp.188-192
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    • 1999
  • To study effects of methanol extract of prosomillet on lopid metabolism , five groups of male Sprang-Dawley rats weighing 116$\pm$9 g were fed test diets for four weeks. The five diets consisted of one low fat(5% w/w) diet containing starch as carbohydrate source(normal) and four high fat diets(15% w/w) containing 40.5%(w/w)sucrose(control) and additional 80% nethanol extractof prosomillet at the levels of 0.3% and 1%(w/w) or prosomillet powder at the level of 20%(w/w). Serum level of total cholesterol was a little higher but that of triglyceride was 41% lower in 20% (w/w) prosomillet powder group than in the control group. The cholesterol levels of two Liver cholesterol levels were lower and phospolipid levels higher in all three prosomillet powder group . Fecal excretionof bile acid was most increased in the prosomillet powder group among all five test groups. Acitivity of liver microsomal 3-hydroxy-3-methylglutaryl coenzyme A (HMG CoA) reductase was significantly lower in 0.3% methanol extract fed group than the control and also appeared to be reduced in 1% extract fed one, wherease those of 20 cholesterol 7$\alpha$-hydroxylase were not different among the five groups. Activities of liver cytosilic glucose-6-phosphate dehydrogenase(G6PDH) and malic enzyme were decreased in 0.3% prosomillet methanol extract and 20% powder groups. The results indicate that in addition to fiber, certain active components in prosomillet have potential to exert hypolipidemic effects via regulating hepatic cholesterogenesis and lipogenesis.

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Reflectance and Flexural Modulus of ABS/TiO2 Composite Sheets (ABS/TiO2 복합체 쉬트의 반사율과 굴곡 탄성률)

  • Kim, Jun Hong;Yoon, Kwan Han
    • Polymer(Korea)
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    • v.38 no.1
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    • pp.103-107
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    • 2014
  • Poly(acrylonitrile-butadiene-styrene) (ABS) composite sheets containing titanium dioxide ($TiO_2$), barium sulfate ($BaSO_4$), calcium carbonate ($CaCO_3$) were prepared by using a co-rotating twin screw extruder, and the reflectance and flexural modulus of the composite sheets were measured. The fillers were well dispersed in ABS matrix. The reflectance of composite sheet was increased with increasing $TiO_2$ and $BaSO_4$ content. Sheet having $TiO_2$ 20 wt% composition, with 5~20 wt% $BaSO_4$ resulted in more than 95% of reflectance. The flexural modulus of composite sheet was increased from 1864 MPa for $ABS/TiO_2/BaSO_4$ 85/10/5 (w/w/w) to 3134 MPa for $ABS/TiO_2/BaSO_4$ 55/20/25 (w/w/w).