• Journal of Food Hygiene and Safety
• /
• v.10 no.3
• /
• pp.169-174
• /
• 1995

Piperine, component of pure ground black pepper, has strong stimulative and hot. Analytical method for piperine was developed by high performance liquid chromatography. Analytical conditions are as follows, mobile phase is 70% methanol, detector UV 343 nm (0.05 AuFs), column is Novapak 5 C18 (15 cm $\times$ 4.6mm), flow rate is 1.0ml/min, chart speed is 0.25 cm/min and injection volume is 20 ul. Analytical results are as follows that relative standard deviation is 1.15%, calibration curve is y=170473.1x-7848.5 (R2=0.999) that shows good linearity. Standard solution of piperine is stable up to 10 hr and content of piperine in pureground black pepper is 4.97$\pm$0.86% Retention time of piperine in HPLC method is about 7 min. Therefore, the developed HPLC method including simple pretreatment of sample will be contribute to quality mangement.

• Proceedings of the Korea Association of Crystal Growth Conference
• /
• 1998.06a
• /
• pp.49-54
• /
• 1998

The growth of diamond films in plasma enhanced chemical vapor deposition(PECVD) processes requires high substrate temperatures and gas pressures, as well as high-power excitation of the gas source. Thus determining the substrate temperature in this severe environment is a challenge. The issue is a critical one since substrate temperature is a key parameter for understanding and optimizing diamond film growth. The precise Si substrate temperature calibration based on rapid-scanning spectroscopic ellipsometry have been developed and utilized. Using the true temperature of the top 200 ${\AA}$ of the Si substrate under diamond growth conditions, real time spectroellipsometry (RTSE) has been performed during the nucleation and growth of nanocrystallind thin films prepared by PECVD. RTSE shows that a significant volume fraction of nondiamond(or{{{{ {sp }^{2 } -bonded}}}}) carbon forms during thin film coalescence and is trapped near the substrate interface between ∼300 ${\AA}$ diamond nuclei.

• Transactions of the Korean Society of Mechanical Engineers A
• /
• v.30 no.6 s.249
• /
• pp.713-721
• /
• 2006

Micro-drill wear deteriorates accuracy and productivity of the micro components. In order to improve productivity and qualify of micro components, it is required to investigate micro-drill wear exactly. In this study, a machine vision system is proposed to measure the wear of micro-drills using a precision servo stage. Calibration experiments are conducted to compensate for the machine vision system. In this paper, worn volume, area and length are defined as wear amounts. Micro-drill wear is reconstructed as the 3D topography and the quantized wear amount by using the shape from focus (SFF) method and wear parameters. Experiments have been conducted with HSS twist micro-drills and SM45C carbon steel workpieces. Validity of the proposed machine vision system is confirmed through experiments.

• YAKHAK HOEJI
• /
• v.35 no.4
• /
• pp.288-294
• /
• 1991

A new fluorescent derivatizing reagent was developed to be used in HPLC for the trace determination of primary and secondary amines. This new reagent, 1-(N,N-dimethylamino)pyrene-6-sulfonyl chloride, was synthesized by the chlorination of sodium 1-(N,N-dimethylamino)pyrene-6-sulfonate which was obtained from 1-(N,N-dimethylamino)pyrene after sulfonation. Ephedrine and norephedrine were derivatized quantitatively by this reagent. The optimum conditions for the derivatization such as pH, reagent concentration, reaction time and reaction temperature ware examined. The structures of derivatives were identified by IR, $^{1}$H-NMR and MS methods. The fluorescence properties and the stability of the derivatives were examined. The derivatives were separated on silica column with an isocratic elution using the mixture of n-hexane and ethylacetate and monitored by fluorescene detector. Linear calibration curves were obtained and detection limits in a 10 $\mu$l injection volume were 5 picomole for ephedrine and norephedrine.

• Proceedings of the Korean Society for Noise and Vibration Engineering Conference
• /
• 2000.06a
• /
• pp.587-593
• /
• 2000

The background noise and transmission loss of wall were measured on site for the multiplex cinema. The results from the simulation analysis was compared with the measurements from the site for different frequencies to review the acoustical parameters, and the analysis results in the relatively small error. Therefore, it is concluded that the reliable estimation can be made once accurate data such as sound source and sound absorption coefficient of interior material is utilized during the simulation process. However, the calibration is necessary for the test room with the small room volume.

• Proceedings of the Korean Geotechical Society Conference
• /
• 1988.06c
• /
• pp.71-123
• /
• 1988

The aim of this paper is to examine the end bearing capacity of a pile in cohesionless soils. The ode of failure of soil due to pile installation is assumed from experimental observation of actual soil deformation. A new solution is proposed complying with the assumed mode of failure by employing the theory of cavity expansion. The effect of curvature of failure envelope is studied in relation to tile proposed solution. The influence of a curved failure envelope becomes larger with increasing degree of curvature and the level of confining stress. This effect in some cases or reduce the end bearing capacity by tore the 80 percent compared with that given by a straight failure envelope. For practical application of tile proposed solution, the method of determining the average volume change in the plastic zone is re-evaluated. The proposed solution is confirmed by comparing the theoretical values with experimental results obtained from model pile tests in a calibration chamber. The comparison shows that the proposed solution provides a reasonable prediction of end bearing capacity for both weak and strong grained soils.

• Proceedings of the KIEE Conference
• /
• 2015.07a
• /
• pp.1429-1430
• /
• 2015

The present study developed an air flow generator system with standard syringes usually adapted for spirometer calibration. It consisted of servo-motor, driver, linear robot, and controller operating as a whole integrated system capable of generating air flows at different speeds on two identical 3L syringes. Experiments demonstrated high accuracy in both flow and volume generation as required such that relative errors were approximately 2.1% and 0.5%, respectively.

• Transactions of the Korean Society of Mechanical Engineers B
• /
• v.25 no.4
• /
• pp.561-571
• /
• 2001

The standard uncertainty of flowrate measurement is obtained by combining that of independent variables. Gravimetric and volumetric method were applied to determine the flowrate and the standard uncertainties of flowrate measurement by both methods were evaluated in accordance with the procedure recommended by International Organization for Standardization. The combined standard uncertainties of determining the flowrate were estimated from the sensitivity coefficient and the standard uncertainty of independent variables. For practical application, the methods for evaluating and expressing uncertainty in flow measurement were discussed. It was found that the uncertainties of the weighing and time measurement in gravimetric method, the volume and time measurement in volumetric method have dominant influence on that of flowrate measurement. With the quantitative analysis of the sensitivity coefficient, the contribution of the each variable uncertainty to the combined standard uncertainty of flowrate measurement is shown clearly.

• Applied Microscopy
• /
• v.46 no.2
• /
• pp.71-75
• /
• 2016

The scanning electron microscope (SEM) offers two-dimensional (2D) micrographs of three-dimensional (3D) objects due to its inherent operating mechanisms. To overcome this limitation, other devices have been used for quantitative morphological analysis. Many efforts have been made on the applications of software-based approaches to 3D reconstruction and measurements by SEM. Based on the acquisition of two stereo images, a multi-view technique consists of two parts: (i) geometric calibration and (ii) image matching. Quantitative morphological parameters such as height and depth could be nondestructively measured by SEM combined with special software programs. It is also possible to obtain conventional surface parameters such as roughness and volume of biomedical specimens through 3D SEM surface reconstruction. There is growing evidence that conventional 2D SEM without special electron detectors can be transformed to 3D SEM for quantitative measurements in biomedical research.

• Journal of Institute of Control, Robotics and Systems
• /
• v.8 no.2
• /
• pp.151-157
• /
• 2002

A 3-dimenstional automatic solder paste inspection system is described that can be used to find defects occurring in solder paste printing process. This system extracts height and volume information very fast as well as area of solder paste printed, using multiple slit ray projection and Galvano-mirror scanning. Methods are presented on calibration of camera and slit projector, real-time image processing of multiple slit images, determination of reference height, and extraction of paste height information are proposed. Performance of the system was successfully demonstrated through field tests.