• Title/Summary/Keyword: Volatile organic acid

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Characteristics of Beeswax-treated Hanji Aged by Closed and Ventilated Chamber (밀폐 및 배기조건에서 열화된 밀랍지의 열화특성 분석)

  • Kang, Yeong Seok;Yang, Eun Jeong
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.44 no.6
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    • pp.9-14
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    • 2012
  • Currently a variety of efforts to conserve and restore the injured the Annal of the Joseon Dynasty are continued and many studies about the aging pathway of the beeswax-treated volume have being progressed. In this study, two chambers were set up to assess the influence of VOCs(Volatile Organic Compounds) generated in process of beeswax deterioration. One chamber was closed and the other was continuously ventilated in order to remove the VOCs. In results, the acid compounds of beeswax-treated Hanjis aged in closed chamber was more than that aged in ventilated chamber. The folding endurance of beeswax-treated Hanjis aged in closed chamber was lower than that aged in ventilated chamber. Accumulated acid compounds of beeswax-treated Hanji in closed chamber may cause accelerated aging and strength decrease. In conclusion, accumulated acid compounds can accelerate the aging of beeswax-treated Hanji and cause the severe deterioration of inside of beeswax-treated volume. Therefore, to preserve more safely beeswax-treated volumes of the Annals of the Joseon Dynasty, it is essential that VOCs emitted from beeswax-treated volume are ventilated.

Effect of Organic Acid Salts and Chitosan on Case-Ready Packed Ground Beef and Pork Patties

  • Park, Seon-Hee;Chung, Seung-Hee;Lee, Sung-Ki;Lee, Keun-Taik
    • Food Science of Animal Resources
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    • v.30 no.4
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    • pp.674-684
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    • 2010
  • The effects of ascorbic acid (AA) alone or in combination with sodium acetate/calcium lactate (AA+SACL) and chitosan (AA+CH) on the physicochemical properties and microbial growth of beef and pork patties stored at $5^{\circ}C$ were investigated. The patties were case-ready packed in an air-containing polypropylene (PP) tray and sealed with polyethylene terephthlate (PETP)/casted polypropylene (CPP) top film. Treatments with AA, AA+SACL and AA+CH were effective in inhibiting total aerobic bacteria from day 4 compared to the control. In general, thiobarbituric acid, volatile basic nitrogen, and hue values in treated samples were lower than the control over the storage, whereas Hunter ${\alpha}^*$ (redness) values and sensory scores for surface color and off-odor were higher. Regarding quality and shelf-life extension, ground beef and pork patties treated with AA+SACL produced the most desirable results among all treatments during storage.

Changes on the Chemical Components of Dongchimi Added with Ginseng and Pineneedle (인삼과 솔잎첨가에 따른 동치미의 성분 변화)

  • 김일경;신승렬;정진호;김광수
    • Journal of the Korean Society of Food Science and Nutrition
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    • v.26 no.3
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    • pp.397-403
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    • 1997
  • This study examined the changes of chemical components in Dongchimi when ginseng and pineneedle were added 0.1% and 0.3%, respectively. Those were fermented at room temperature for the first day and at 4$^{\circ}C$ from the second to 29th day. The contents of reducing sugar was significantly increased during fermentation, and showed the highest content in Dongchimi added pineneedle. The contents of proteins were also increased in the Dongchimi with pineneedle during 8 days of fermentation, while the others increased throughout 29 days of fermentation. The contents of non-volatile organic acids were 2.79~4.80 mg/100 ml at the end of fermentation, and the content of lactic acid was the highest among them. Free sugars of the Dongchimi were composited sucrose, glucose and fructose, and the contents of those were in the range of 227.4~247.0 mg/100ml in 8 days of fermentation, then increased to 705.2~943.7mg/100ml in 29 days. the Dongchimi contained 17 kinds of free amino acids except lysine, arginine were the majority of them, and sarcosine, $\beta$-aminoisobutyric acid and ${\gamma}$-aminoisobutyric acid were the major portion of amino acid dervatives.

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Determination of total iodide in seawater by gas chromatography-mass spectrometry (Gas chromatography-mass spectrometry를 이용한 해수 중 총 요오드 정량분석)

  • Shin, Ueon-Sang
    • Analytical Science and Technology
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    • v.15 no.5
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    • pp.445-450
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    • 2002
  • A sensitive gas chromatographic method has been established for the determination of total iodide in seawater as their volatile organic derivative. The method is based on the formation of 4-iodo-2,6-dimethylphenol with 2,6-dimethylphenol in matrix and a single-step extraction of the derivative with ethyl ether, which are then measured by gas chromatography-mass spectrometry (selected ion monitoring). Iodate in sea water was completely reduced to iodide with ascorbic acid and acetic acid. The detection limit was 0.1 ng/mL in seawater and the calibration curve showed good linearity with r=0.9997. The method was sensitive, reproducible and simple enough to permit the reliable routine analysis of total iodide in seawater. Total iodide in sea water was found about 30 ng/ml.

Effect of Tannin and Species Variation on In vitro Digestibility, Gas, and Methane Production of Tropical Browse Plants

  • Gemeda, Belete Shenkute;Hassen, A.
    • Asian-Australasian Journal of Animal Sciences
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    • v.28 no.2
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    • pp.188-199
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    • 2015
  • Nineteen tanniferous browse plants were collected from South Africa to investigate their digestibility, gas production (GP) characteristics and methane production. Fresh samples were collected, dried in forced oven, and ground and analyzed for nutrient composition. In vitro GP and in vitro organic matter digestibility (IVOMD) were determined using rumen fluid collected, strained and anaerobically prepared. A semi-automated system was used to measure GP by incubating the sample in a shaking incubator at $39^{\circ}C$. There was significant (p<0.05) variation in chemical composition of studied browses. Crude protein (CP) content of the species ranged from 86.9 to 305.0 g/kg dry matter (DM). The neutral detergent fiber (NDF) ranged from 292.8 to 517.5 g/kg DM while acid detergent fiber (ADF) ranged from 273.3 to 495.1 g/kg DM. The ash, ether extract, non-fibrous carbohydrate, neutral detergent insoluble nitrogen, and acid detergent insoluble nitrogen and CP were negatively correlated with methane production. Methane production was positively correlated with NDF, ADF, cellulose and hemi-cellulose. Tannin decreased GP, IVOMD, total volatile fatty acid and methane production. The observed low methanogenic potential and substantial ammonia generation of some of the browses might be potentially useful as rumen manipulating agents. However, a systematic evaluation is needed to determine optimum levels of supplementation in a mixed diet in order to attain a maximal depressing effect on enteric $CH_4$ production with a minimal detrimental effect on rumen fermentation of poor quality roughage based diet.

Quality Characteristics of Cheongsoo Grape Wine by Freeze Concentration Fermented with Different Yeasts (효모의 종류를 달리하여 제조한 동결 농축 청수 와인의 품질 특성)

  • Park, Hyejin;Park, Eui Kwang;Choi, Sungyeol;Shin, Hyerim;Kim, Min-Ja;Park, Jung-Mi
    • The Korean Journal of Food And Nutrition
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    • v.33 no.5
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    • pp.512-523
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    • 2020
  • The objective of this study was to investigate the quality characteristics of Cheongsoo wine using freeze concentration fermented with 5 kinds of yeast strains (Saccharomyces cerevisiae EJ18, EJ30, HK22, HK32 and Fermivin). We compared the characteristics, volatile flavor component and physiological activity of 5 wines. The freeze concentration can increase the sugar concentration in grape juice by reducing its water content and the alcohol content of freeze-cententrated Cheongsoo wines ranged between 15.0~15.8%. The pH of wines ranged from 2.92 to 2.94 and the total acidity and soluble solid of wines ranged from 12.40~13.27. °Brix. The major organic acid in the wines was tartaric acid (4.49~5.11 mg/mL) and malic acid (7.00~7.97 mg/mL). It contains higher functional compounds in wine fermented with yeast (EJ18, EJ30, HK22, HK32) than wine fermented with fermivin. α-glucosidase and tyrosinase inhibitory activity had the highest values (78.87% and 62.25%) in wine fermented with HK22 and EJ18 yeast, respectively. 16 volatile flavor compounds (alcohols, esters, ketones, acids, and others) were detected in the Cheongsoo wines by freeze concentration. These results provide useful information that the quality characteristics of wine developed by the freeze-concentration method using grapes cultivated in Korea.

The Effect of the Addition of Carbohydrate on the Concentration of Odorous Compounds in Pig Slurry (양돈 슬러리에 첨가된 발효탄수화물의 종류별 악취물질 농도 비교)

  • Hwang, Ok Hwa;Yang, Seung Hak;Jeon, Jung Hwan;Kwag, Jeong Hoon;Choi, Dong Yun;Yang, Seung Bong;Kim, Doo Hwan;Cho, Sung Back
    • Journal of Animal Environmental Science
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    • v.19 no.1
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    • pp.1-8
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    • 2013
  • Slurry treatments included peanut shell, palm golden fiber, almond hull, which was added 2% of the amount of slurry, and non-treatment control (n=4 each group). Levels of odorous compounds were measured from the liquid slurry incubated in $20^{\circ}C$ for 2 wk in chamber whose structure is similar to slurry pit. Concentration of phenols and indoles was higher (p<0.05) in control (48.4, 4.0 ppm) compared to almond hull (31.5, 1.4 ppm) or palm golden fiber (29.1, 1.6 ppm) group. Short chain fatty acid (SCFA) level was lowest (p<0.05) in control (2,121 ppm) but highest in peanut shell group (3,640 ppm). Branched chain fatty acid (BCFA) concentration was highest (p<0.05) in peanut shell (296 ppm), but lowest in almond hull (90 ppm). Taken together, concentration of odorous compounds was decreased by addition of almond hull in pig slurry by which crude fiber and non-digestible fiber (NDF) may act as a carbon source.

Physicochemical Properties and Volatile Compounds in Jeonju Moju (전주 모주의 이화학적 특성 및 휘발성 화합물 성분)

  • Kwon, Young-Hee;Jo, Sung-Jin;Kim, Hye-Ryun;Lee, Hyang-Jeong;Kim, Jae-Ho;Ahn, Byung-Hak
    • Korean Journal of Food Science and Technology
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    • v.41 no.5
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    • pp.503-508
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    • 2009
  • The principal objective of this study was to evaluate the physicochemical properties and volatile compound contents of Moju acquired from 12 restaurants in Jeonju. The alcohol contents were lower than 2.1%, and the pH values ranged from 3.85 to 4.38. Total acidity, $^{\circ}Bx$, and UV absorbance values differed among the samples according to the type of side materials added. Reducing sugar contents were found to be substantially superior to other commercial takju variants. Malic and lactic acid contents were higher than the contents of other organic acids, and the free sugar contents were as follows: maltose>glucose>fructose. Overall, the high b (yellowness) and cP values were attributable to the turbid yellow and heavy condition of the samples. The volatile compound contents of Moju were analyzed via GC and GC/MSD. 30 components were identified, including 3 alcohols, 12 esters, 7 hydrocarbons, and 4 aldehydes. Among the alcohol compounds, benzeneethanol levels were higher than the levels of isoamyl alcohol. Ethyl caprate, ethyl palmitate, and ethyl linoleate, which were fundamentally attributable to origin liquor, were highest among the 12 esters. (E)-cinnamaldehyde, which was the most abundant among 7 hydrocarbons, and (E)-cinnamyl acetate contents were attributed to the presence of cinnamon, a common supplement in the processing of Moju.

Characteristics of Anaerobic Digestion using Food waste leachate under Increased Organic Loading rate (유기물부하량 증가에 따른 음폐수 혐기성소화의 특성 분석)

  • Jae-Hoon Jeung;Woo-Jin Chung;Soon-Woong Chang;Jin-Tea Kim;Seong-Yeob Jeong;Seung-Youn Yang
    • Journal of Environmental Science International
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    • v.31 no.12
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    • pp.1127-1134
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    • 2022
  • Herein , the effect of changes in the organic loading rate in anaerobic digestion was evaluated. The experiment was carried out by a laboratory -scale semi-continuous stirred tank reactor, and feedstock was food-waste leached. The organic loading rate was increased by 0.5 kgVS/m3 in each phase from 1.0 kgVS/m3 to 4.0 kgVS/m3. At the end of the operation, to check the failure of the reactor, the organic loading rate was increased by 1.0 kgVS/m3 in each phase and reached 6.0 kgVS/m3. This shows that the biogas yield decreased as organic loading rate increased. Biogas production seemed to be unstable at 3.5-6.0 kgVS/m3. Moreover, biogas production dramatically fell to approximately 0 mL at 6.0 kgVS/m3, which was decided as the operation failure on the 16th day of the las tphase. The result of the reactor analysis shows that the cumulation of volatile fatty acid increased as the organic loading rate increased. This seems to occur due to the decreasein pH in the reactor and led to extinction of anaerobic bacteria, which were the biogas products. Although the buffer compound (alkalinity) could prevent the decline in pH, the concentration of alkalinity was found to be lacking at a high organic loading rate

Nutrient Removal Using Fermented Organic Acids Derived from the Primary Sludge in the Intermittent Aeration Activated Sludge Process

  • Weon, Seung-Yeon;Lee, Sang-Il;Lee, Chan-Won
    • Environmental Engineering Research
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    • v.16 no.4
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    • pp.213-218
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    • 2011
  • The two-stage intermittent aeration activated sludge process (IAP) and dynamic-flow intermittent aeration activated sludge process (DFP) were investigated for the nutrient removal of domestic wastewater. Three sets of IAP and one set of DFP were operated. The fermented settled sludge taken from the primary settling tank was added to two IAP and one DFP as an external electron donor, with one IAP, in which an external carbon source was not added, as a control. All the systems were operated at a sludge retention time of 20 days and a hydraulic retention time of 12 hr. A Higher denitrification rate was observed with the fermented settled sludge for the denitrification compared to the process without the addition of the organic source. The result indicates that the fermented acid from the primary domestic sludge has been proved to be an excellent electron donor for denitrification and biological phosphorus removal with IAP and DFP in treating relatively low C/N ratio(Carbon / Nitrogen ratio) wastewater. Phosphate accumulating organisms have a capability of competing with denitrifiers in the presence of volatile organic acids under anoxic conditions.