• 한국분말재료학회지
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• 제21권6호
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• pp.429-433
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• 2014

This study investigated the magnetic properties and frequency dispersion of complex permeability of Ni-Zn-Co ferrites used for magnetic shielding in near field communication (NFC) system. The sintered specimens of $(Ni_{0.7}Zn_{0.3})_{1-x}Co_xFe_2O_4$ composition were prepared by the conventional ceramic processing. The coercive force and saturation magnetization were measured by vibrating sample magnetometer. The complex permeability was measured by RF impedance analyzer in the range of 1 MHz~1.8 GHz. The coercive force increased and saturation magnetization decreased with increasing the Co substitution. The real and imaginary parts of complex permeability decreased and the resonance frequency increased with Co substitution, which was attributed to the increase in crystal anisotropy field and reduction in saturation magnetization. The effect of Co substitution could be found in reducing the magnetic loss to nearly zero at the operating frequency of NFC (13.56 MHz).

• Journal of Magnetics
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• 제1권1호
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• pp.19-23
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• 1996

In the present study, the $Sm_2Fe_{17}N_x$-type interstitial materials have been prepared by reaction between Nb-free or Nb-containing $Sm_2Fe_{17}$-type alloy and $N_2$ gas. Nitrogenation behaviour of the $Sm_2Fe_{17}N_x$-type material and disproportionation characteristics of the nitrogenated materials have been studied by means of differential thermal analysis (DTA) and thermopiezic analysis (TPA). Magnetic properties of the produced $Sm_2Fe_{17}N_x$-type interstitial materials were characterised in vibrating sample magnetometer (VSM) or thermomagnetic analyser (TMA). Epoxy-bonded or Zn-bonded $Sm_2Fe_{17}N_x$-type magnets were prepared, and their magnetic properties were investigated. It has been found that nitrogenation kinetics of the Sm2Fe17Nx-type alloy is improved significantly by the Nb-substitution for Fe in the alloy. The Nb-substitution is also found to enhance thermal stability of the $Sm_2Fe_{17}N_x$-type interstitial material. Hard magnetic properties of the interstitial materials produced from Nb-free orNb-containing alloy is high enough (intrinsic coercivity : over 7 kOe) for application as bonded permanent magnets. The good hard magnetic properties of the interstitial material are maintained in the epoxy-bonded magnet. Intrinsic coercivity of the Zn-bonded magnets is improved significantly as post-bonding annealing time increases.

• Journal of Magnetics
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• 제12권4호
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• pp.133-136
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• 2007

We have carried out the study of magnetocaloric effect for as-quenched and annealed $Fe_{91-x}Y_xZr_9$ alloys. Samples were prepared by arc melting the high-purity elemental constituents under argon gas atmosphere and by single roller melt spinning. These alloys were annealed one hour at 773 K in vacuum chamber. The magnetization behaviours of the samples were measured by vibrating sample magnetometer. The Curie temperature increases with increasing Y concentration (x=0 to 8). Temperature dependence of the entropy variation ${\Delta}S_M$ was found to appear in the vicinity of the Curie temperature. The results show that annealed $Fe_{86}Y_5Zr_9$ and $Fe_{83}Y_8Zr_9$ alloys a bigger magnetocaloric effect than that those in as-quenched alloys. The value is 1.23 J/kg K for annealed $Fe_{86}Y_5Zr_9$ alloy and 0.89 J/kg K for as-quenched alloy, respectively. In addition, the values of ${\Delta}S_M$ for $Fe_{83}Y_8Zr_9$ alloy is 0.72 J/Kg K for as-quenched and 1.09 J/Kg K for annealed alloy, respectively.

• Journal of Magnetics
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• 제21권2호
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• pp.164-167
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• 2016

The effect of the B additions on glass formation and magnetic properties is reported for the $Fe_{(87-x-y)}Co_yTi_7Zr_6B_x$ (x = 2, 4, 6 and y = 35, 40) alloy system. The ribbon samples with the width of 2 mm for each composition were prepared by the melt spinning technique; furthermore, their phase information was obtained from X-ray diffraction. Glass formation and magnetic properties were measured using differential scanning calorimetry and vibrating sample magnetometer respectively. The $Fe_{45}Co_{40}Ti_7Zr_6B_2$ (x = 2 and y = 40) system has the nanocrystalline phase identified as ${\alpha}-Fe$, as well as the amorphous phase, whereas all other alloys are fully amorphous. It is associated with the role of B on the glass formation. The widest supercooled liquid region is obtained as 71 K at x = 4 (both y = 35 and 40). The saturation magnetization decreases with the increase of the amount of the B addition, and the highest value is 1.59 T as x = 2 and y = 35 for this alloy system.

• 한국재료학회지
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• 제30권11호
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• pp.589-594
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• 2020

Many electronic applications require magnetic materials with high permeability and frequency properties. We improve the magnetic permeability of soft magnetic powder by controlling the shape magnetic anisotropy of the powders and through the preparation of amorphous nanoparticles. For this purpose, the effect of the shape magnetic anisotropy of amorphous Fe-B-P nanoparticles is observed through a magnetic field and the frequency characteristics and permeability of these amorphous nanoparticles are observed. These characteristics are investigated by analyzing the composition of particles, crystal structure, microstructure, magnetic properties, and permeability of particles. The composition, crystal structure, and microstructure of the particles are analyzed using inductively coupled plasma optical emission spectrometry-, X-ray diffraction, scanning electron microscopy and focused ion beam analysis. The saturation magnetization and permeability are measured using a vibrating sample magnetometer and an LCR meter, respectively. It is confirmed that the shape magnetic anisotropy of the particles influences the permeability. Finally, the permeability and frequency characteristics of the amorphous Fe-B-P nanoparticles are improved.

• 한국전기전자재료학회논문지
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• 제11권5호
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• pp.418-422
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• 1998

The Co-Cr films are one of the most suitable candidates for perpendicular magnetic recording media. The facing targets sputtering(FTS) system has a advantage of preparing films over a wide range of working gas pressure on plasma-free substrate. In this study, we investigated the possibility of employing FTS system for depositing Co-Cr films. The Co-Cr thin films were deposited with various sputter gas pressure($P_Ar$, 0.1~10mTorr) by using FTS apparatus at temperature of $40^{\circ}C and 220^{\circ}C$, respectively. Crystallographic and magnetic characteristics were evaluated by x-ray diffractometry (XRD) and vibrating sample magnetometer(VSM), respectively. Under argon gas pressure at 0.1mTorr, films with morphologically dense microstructure, good c-axis orientation and higher coercivity were obtained. It has been confirmed that the FTS system is very useful for preparing Co-Cr thin film recording media.

• 한국산학기술학회논문지
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• 제4권1호
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• pp.27-30
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• 2003

자수정은 우리나라에서 산출되어 수출시장이 큰 준보석이다. 원석을 가공하여 최종 장신구제품을 제작하는데 실제 원석에서는 연수정, 자수정, 백수정이 함께 산출되어 이들의 품위를 정량적으로 평가하여 원석가격을 산출하는 것과 아직 확보되지 않은 자수정의 정량적 감정 기술이 필요하다. 이제까지는 아쉽게도 육안 판별과 경험에 의존하였으나 투과전자 현미경과 진동시편자력계측정을 통하여 3가지 원석의 특성을 명확히 구별하는 것이 가능하였다. 또한 FTIR(Fourier transformation infra-red) 측정을 통하여 고가 자수정의 정량품질 확인도 가능하였다. 이러한 방법은 원석의 품위를 확인하는데 효과적이고 최초 원석 상태에서의 고가 자수정의 함량을 평가할 수 있는 우수한 지표가 될 수 있었다.

• 대한전기학회논문지:전기기기및에너지변환시스템부문B
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• 제49권11호
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• pp.729-736
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• 2000

This paper deals with the characteristic analysis of magnetizer for convergence purity magnet by the finite element method. The analysis utilizes combined method of the time-stepped finite element analysis and the Preisach model with hysteresis phenomena. In the finite element analysis, the non-linearity and the eddy current of the magnetizing fixure and permanent-magnet are taken account. The magnetization distribution in the permanent magnet is determined by using Preisach model which are composed of Everett function table and the first order transition curves is obtained by the Vibrating Sample Magnetometer. The calculated flux density values on the surface of the permanent magnet are led to the approximated gauss density values measured by the gauss meter. As a result, winding current, copper loss, eddy current loss of the magnetizing yoke, flux plot, surface gauss plot, temperature rise of the coil and resistor variation, vector diagram of magnetization distribution are shown.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 2005년도 하계학술대회 논문집 Vol.6
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• pp.278-279
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• 2005

The crystallization of FePt/MgO(100) magnetic thin films of various thicknesses has been studied using synchrotron x-ray scattering, atomic force microscope, and vibrating sample magnetometer. In film with a 500-${\AA}$-thick, ordered (fct) FePt phase was dominantly crystallized into perpendicular (001) grains keeping the magnetically easy c-axis normal to the film plane during annealing. In film with a 812-${\AA}$-thick, however, longitudinal (110) grains keeping the c-axis parallel to the film plane were grown on top of the perpendicular (001) grains. The behavior of the magnetic properties was consistent with the thickness dependence of the crystallization. We attribute the thickness dependence of the crystallization to the substrate effect, which prefers the growth of the c-axis oriented perpendicular grains near the film/substrate interfacial area.

• 방사선산업학회지
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• 제9권1호
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• pp.15-20
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• 2015

Carbon fiber has received much attention owing to its properties, including a large surface-to-volume ratio, chemical and thermal stability, high thermal and electrical conductivity, and high mechanical strengths. In particular, magnetic nanopowder dispersed carbon fiber has been attractive in technological applications such as the electrochemical capacitor and electromagnetic wave shielding. In this study, the nickel-oxide-nanoparticle dispersed polyacrylonitrile (PAN) fibers were prepared through an electrospinning method. Electron beam irradiation was carried out with a 2.5 MeV beam energy to stabilize the materials. The samples were then heat-treated for stabilization and carbonization. The nanofiber surface was analyzed using a field emission scanning electron microscope (FE-SEM). The crystal structures of the carbon matrix and nickel nanopowders were analysed using X-ray diffraction (XRD). In addition, the magnetic and electrical properties were analyzed using a vibrating sample magnetometer (VSM) and 4 point probe. As the irradiation dose increases, the density of the carbon fiber was increased. In addition, the electrical properties of the carbon fiber improved through electron beam irradiation. This is because the amorphous region of the carbon fiber decreases. This electron beam effect of PAN fibers containing nickel nanoparticles confirmed their potential as a high performance carbon material for various applications.