• Title/Summary/Keyword: Vacuum filtration

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Fabrication and Characterization of Carbon Nanotube/Carbon Fiber/Polycarbonate Multiscale Hybrid Composites

  • Cho, Beom-Gon;Hwang, Sang-Ha;Park, Young-Bin
    • Composites Research
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    • v.29 no.5
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    • pp.269-275
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    • 2016
  • Multiscale hybrid composites, which consist of polymeric resins, microscale fibers and nanoscale reinforcements, have drawn significant attention in the field of advanced, high-performance materials. Despite their advantages, multiscale hybrid composites show challenges associated with nanomaterial dispersion, viscosity, interfacial bonding and load transfer, and orientation control. In this paper, carbon nanotube(CNT)/carbon fiber(CF)/polycarbonate(PC) multiscale hybrid composite were fabricated by a solution process to overcome the difficulties associated with controlling the melt viscosity of thermoplastic resins. The dependence of CNT loading was studied by varying the method to add CNTs, i.e., impregnation of CF with CNT/PC/solvent solution and impregnation of CNT-coated CF with PC/solvent solution. In addition, hybrid composites were fabricated through surfactant-aided CNT dispersion followed by vacuum filtration. The morphologies of the surfaces of hybrid composites, as analyzed by scanning electron microscopy, revealed the quality of PC impregnation depends on the processing method. Dynamic mechanical analysis was performed to evaluate their mechanical performance. It was analyzed that if the position of the value of tan ${\delta}$ is closer to the ideal line, the adhesion between polymer and carbon fiber is stronger. The effect of mechanical interlocking has a great influence on the dynamic mechanical properties of the composites with CNT-coated CF, which indicates that coating CF with CNTs is a suitable method to fabricate CNT/CF/PC hybrid composites.

The Evaluation of Drainage Characteristics Using a New Drainage Tester (새로운 탈수측정 설비를 이용한 탈수 특성 평가)

  • 김용식;원종명
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.32 no.3
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    • pp.1-9
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    • 2000
  • The MDDA (Modified Dynamic Drainage Analyzer) was developed to evaluate the drainage characteristics on paper machine. The initial forming vacuum velocity was decreased with the increase of stock consistency and there were no significant effects of the applied vac-uum. On the other hand the initial forming drainage velocity was rapidly decreased with the increase of stock consistency above the 0.35 bar of applied vacuum. The final drainage time and wet web permeability showed similar trends under 0.075% consistency but increased rapidly at the higher consistencies. SFR(Specific Filtration Resistance) and drainage obtained for different vacuum level applied and deposited weights measured by using MDDA showed the linear relationship.

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A Study of High Temperature Filtration Performance Test on Low Density Cylindrical Ceramic Filters (저밀도 원통형 세라믹 필터의 고온 여과 성능시험 연구)

  • 이동섭;홍민선;최종인
    • Journal of Korean Society for Atmospheric Environment
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    • v.17 no.2
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    • pp.213-222
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    • 2001
  • Cylindrical type ceramic filers, that is 60 O.D$\times$10t$\times$600L and 60 O.D$\times$10t$\times$1,000L were manufactured by vacuum forming processes using ceramic ray materials. For cylindrical type ceramic filters, porosity and bulk density were measured for, 80 to 90% and 0.3 to 0.4 g/㎤, respectively at uniform pore size of 41 to 45${\mu}{\textrm}{m}$. Bench scale candle filters (60$\psi$ $\times$10t$\times$600L) were tested using different dusts collected from many industries including chemical processing, glass processing and metal manufacturing pants. Collection efficiencies found out to range from 99.87% to 99.90%, while resistance coefficients from 1.1$\times$10(sup)11/$m^2$ to 1.7$\times$10(sup)11/$m^2$ . Full scale low density ceramic filters (60$\psi$ $\times$10t$\times$1,000L) were also tested at 1 atm, $600^{\circ}C$ to reveal the filtration efficiency, conditioning, and resistance coefficients using two different types of dust as chemical processing and metal refined processing. Darcys law resistance coefficients were measured to range 1.44$\times$10(sup)11/$m^2$ to 2.74$\times$10(sup)11/$m^2$, and collection efficiencies on the range 99.84 to 99.96%, Finally, results of long term performance test showed that filters were conditioned after 170hrs. Experimental conditions for effective filtration were examined under the condition 10 cm/sec face velocity, 3kg/$\textrm{cm}^2$ pulsing pressure, 5 min filtration cycle, and 300msec pulse opening time.

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Study of Factors for development of Advanced Media filter for Ballast water Treatment (밸러스트 수 처리용 메디아 필터 개발을 위한 여과특성에 관한 연구)

  • Park, Seon-Jeong;Lim, Jae-Dong;Kim, Dong-Geun;Kim, In-Soo
    • Journal of Navigation and Port Research
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    • v.32 no.6
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    • pp.499-503
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    • 2008
  • As the conference result of MEPC in IMO, development of ballast water management system corresponding to newly established ballast water management standard (D2 regulation) of shipping is being made an active progress over the whole world. The ballast water management system should treat particular material of more than $10{\mu}m$ in high capacity of more than 500t per hour in the event of filtration process. Also, it is very difficult to develop a practical management system since a limited element which a narrow space of the ship should be designed in the minimal volume is assumed. Therefore, the study promoted a study on the next generation auto back wash media filter to overcome such a limited element. Also, the study performed pressure and flux measurement test followed by thickness of each filter medium for filtration by each size to grasp a relation between absorption and pressure at the time of vacuum filtration and mechanical analysis and turbidity change observation of filtered water after vacuum filtration.

Drainage Simulation in Fourdrinier Paper Machine (장망초지기에서 탈수 시뮬레이션)

  • 김용식;원종명
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.32 no.3
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    • pp.10-17
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    • 2000
  • The MDDA(Modified Dynamic Drainage Analyzer) was developed to evaluate the drainage at hydrofoil table roll and low vacuum devices on fourdrinier paper machine MB-former. Comparison of the results was obtained using a computer simulation system based on Taylor's equation and filtration equation and by measuring the consistency profile in a paper machine presented an agreement within 10.7% This device can evaluate the dewatering pro-file on wire for various stock properties adjust dewatering devices on fourdrinier paper machine and control the dosage of retention aids for improving paper structural properties and runnability of papermachine.

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Facile Synthesis of Pt Nanoparticle and Graphene Composite Materials: Comparison of Electrocatalytic Activity with Analogous CNT Composite

  • Lee, Jihye;Jang, Ho Young;Jung, Insub;Yoon, Yeoheung;Jang, Hee-Jeong;Lee, Hyoyoung;Park, Sungho
    • Bulletin of the Korean Chemical Society
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    • v.35 no.7
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    • pp.1973-1978
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    • 2014
  • Here, we present a facile method to synthesize Pt nanoparticles (NPs) and graphene composite materials (Pt/G) via vacuum filtration. Anodic aluminum oxide (AAO) templates were used to separate Pt/G composite and liquid phase. This method can be used to easily tune the mass ratio of Pt NPs and graphene. Pt NPs, graphene, and carbon nanotubes (CNTs) as building blocks were characterized by a variety of techniques such as scanning electron microscopy, UV-Vis spectroscopy, and Raman spectroscopy. We compared the electrocatalytic activities of Pt/G with Pt NP and CNT films (Pt/CNT) by cyclic voltammetry (CV), CO oxidation, and methanol oxidation. Pt/G was much more stable than pure Pt films. Also, Pt/G had better electrochemical activity, CO tolerance and methanol oxidation than Pt/CNT loaded with the same amount of Pt NPs due to the better dispersion of Pt NPs on graphene flakes without aggregation. We further synthesized Au@Pt disk/G and Pt nanorods/G to determine if our synthetic method can be applied to other NP shapes such as nanodisks and nanorods, for further electrocatalysis studies.

Preparation and Performance of Aluminosilicate Fibrous Porous Ceramics Via Vacuum Suction Filtration

  • Qingqing Wang;Shaofeng Zhu;Zhenfan Chen;Tong Zhang
    • Korean Journal of Materials Research
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    • v.34 no.1
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    • pp.12-20
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    • 2024
  • This study successfully prepared high-porosity aluminosilicate fibrous porous ceramics through vacuum suction filtration using aluminosilicate fiber as the primary raw material and glass powder as binder, with the appropriate incorporation of glass fiber. The effects of the composition of raw materials and sintering process on the structure and properties of the material were studied. The results show that when the content of glass powder reached 20 wt% and the samples were sintered at the temperature of 1,000 ℃, strong bonds were formed between the binder phase and fibers, resulting in a compressive strength of 0.63 MPa. When the sintering temperatures were increased from 1,000 ℃ to 1,200, the open porosity of the samples decreased from 89.08 % to 82.38 %, while the linear shrinkage increased from 1.13 % to 10.17 %. Meanwhile, during the sintering process, a large amount of cristobalite and mullite were precipitated from the aluminosilicate fibers, which reduced the performance of the aluminosilicate fibers and hindered the comprehensive improvement in sample performance. Based on these conditions, after adding 30 wt% glass fiber and being sintered at 1,000 ℃, the sample exhibited higher compressive strength (1.34 MPa), higher open porosity (89.13 %), and lower linear shrinkage (5.26 %). The aluminosilicate fibrous porous ceramic samples exhibited excellent permeability performance due to their high porosity and interconnected three-dimensional pore structures. When the samples were filtered at a flow rate of 150 mL/min, the measured pressure drop and permeability were 0.56 KPa and 0.77 × 10-6 m2 respectively.

Characteristic Analysis of Electret Filters made by Electrospinning (전기방사를 통한 정전필터제조 및 특성분석)

  • Ahn, Young-Chull;Kim, Gil-Tae;Kim, Seong-Kon;Lee, Jae-Keun;Kim, Jong-Won
    • Proceedings of the SAREK Conference
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    • 2008.06a
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    • pp.1134-1138
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    • 2008
  • Electret filter media are used in general ventilation filters, disposable respirators, vehicle cabin filters, vacuum cleaners and room air cleaners. There are basic mechanisms of interception, inertial impaction, diffusion, gravitational settling, electrostatic attraction by which an aerosol particle can be deposited onto a fiber in a filter. The ability of fine particle removal strongly depends on the electrostatic forces between particles and polarized fibers. Thus, the stability of the fiber polarization is a major factor in the reliability of electret filters. In this study, electrical properties and filtration performance of electrospun filter media are quantitatively investigated. Electrical properties of electrospun filters have been studied on surface charge potential and surface charge density. Also the filtration performance of the electret filters are evaluated on collection efficiency. Electrospun filters show same collection efficiency with low pressure drop compare to commercialized HEPA filters. Surface charge potential and surface charge density of electrospun filters are increased with increasing applied voltage. Also collection efficiency of electrospun filters is increased with increasing surface charge potential and surface charge density.

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Preparation of Bucky Paper using Single-walled Carbon Nanotubes Purified through Surface Functionalization and Investigation of Their Field Emission Characteristics (기능화에 의한 단일벽 탄소나노튜브 정제 및 페이퍼 제조와 전계방출 특성 연구)

  • Goak, Jeung-Choon;Lee, Seung-Hwan;Lee, Han-Sung;Lee, Nae-Sung
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
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    • v.21 no.5
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    • pp.402-410
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    • 2008
  • Single-walled carbon nanotubes (SWCNTs) were currently produced together with some contaminants such as a metallic catalyst, amorphous carbon, and graphitic nanoparticles, which should be sometimes purified for their applications. This study aimed to develop efficient, scalable purification processes but less harmful to SWCNTs. We designed three-step purification processes: acidic treatment, surface functionalization and soxhlet extraction, and heat treatment. During the soxhlet extraction using tetrahydrofuran, specifically, carbon impurities could be easily expelled through a glass thimble filter without any significant loss of CNTs. Finally, SWCNTs were left as a bulky paper on the filter through membrane filtration. Vertically aligned SWCNTs on one side of bulky paper were well developed in a speparation from the filter paper, which were formed by being sucked through the filter pores during the pressurized filtration. The bucky paper showed a very high peak current density of field emission up to $200\;mA/cm^2$ and uniform field emission images on phosphor, which seems very promising to be applied to vacuum microelectronics such as microwave power amplifiers and x-ray sources.

Development and Performance Evaluation of Positively Charged Porous Filter media for Water Purification System (정수 설비를 위한 양전하가 부가된 다공성 수처리 필터 개발과 성능평가)

  • Lee, Chang-Gun;Joo, Ho-Young;Lee, Jae-Keun;Ahn, Young-Chull;Park, Seong-En
    • Proceedings of the SAREK Conference
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    • 2006.06a
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    • pp.95-98
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    • 2006
  • Filtration by fibrous filter is one of the Principle methods used for removing pollutant particles in the liquid. Because of the increasing need to protect both human health and valuable devices from exposure to fine particles, filtration has become more important. Filters have been developed with modified surface charge characteristics to capture and adsorb particles by electrokinetic interaction between the filter surface and particles contained in water. The main purposes of this study are to develop and evaluate the performance evaluation of the apparatus for making a positively charged porous filter media and to analyze the surface characteristics of the filter media for capturing negavitely charged contaminants mainly bacteria and virus from water. The experimental apparatus consists of a mixing tank, a vacuum pumping system, a injection nozzle, a roller press and a controller. The filter media is composed of glass fiber(50-750 nm), cellulose($10-20{\mu}m$) and colloidal charge modifier. The characteristics of filter media is analyzed by SEM(Scanning Electron Microscopy), AFM(Atomic Force Microscopy) and quantified by measuring the zeta potential values.

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