• Title/Summary/Keyword: Uncertainty measurement

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Preparation and characterization of the primary gas standards for isoprene (아이소프렌 일차표준가스의 제조 및 특성 평가)

  • Kim, Taesu;Kang, Chul-Ho;Kim, Yong Doo;Lee, Seungho;Kim, Dalho
    • Analytical Science and Technology
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    • v.27 no.6
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    • pp.357-363
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    • 2014
  • Isoprene is a one of the biogenic volatile organic compounds (BVOCs) and it is known as a source of the tropospheric ozone and formaldehyde. In addition, isoprene is a trace component of the exhaled breath and it is a potential biomarker for the diagnosis of diseases such as lung cancer. In these regards, isoprene gas standards are required for the accurate measurement of isoprene in air samples. To establish a standard for isoprene gas, gravimetric preparation and characterization of primary gas standards were studied. The primary gas standards were produced independently in 4 aluminum cylinders and concentrations were examined by GC-FID. As a result, the uncertainty of the gravimetric preparations including purity of the raw material was 0.01% and reproducibility of the preparation of independent 4 cylinders was 0.08%. The primary gas standards for isoprene showed 14 months of long-term stability. The relative expended uncertainty of 2.8% (95% of confidence level, k=1.96) was assigned to the certified value of 10 ${\mu}mol$/mol level of isoprene based on the quantitative evaluation of the purity, weighing, reproducibility, adsorption and long-term stability.

Research on Measurement Condition Establishment of a Liquid Scintillation Counter System (액체섬광계수기 장비의 계측조건 확립에 관한 연구)

  • Park, Eung-Seop;Han, Sang-Jun;Lee, Seung-Jin;Kim, Hee-Gang;Lee, Na-Young;Mun, Ji-Yeon
    • Journal of Radiation Protection and Research
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    • v.31 no.3
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    • pp.155-164
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    • 2006
  • It is judged that there could be certainty in every process of analyzing environmental samples using Liquid Scintillation Counter. Therefore, this study focuses on quantitative evaluation on uncertainty in an effort to analyze comparatively accurately environmental samples. For this, after parameters which can have an effect on uncertainty was derived, the evaluation on each parameter was tamed out. The results of analysis of each parameter showed that the effect according to the weight difference of Teflon vial did not appear, and that standard deviations of SQP(E) averages reached saturation point at $75{\sim}90$ sec at the result of making increases step by step the irradiation time of External standard, and that values measured by repeat method produces good results compared with replicate. Also, conclusion was derived that analysis on sample after it is left in cold and dark room at least above 1,000 minutes have to be carried out, and the result of carrying out verification on results measured as well as equipment itself using radioactivity-error-analysis and chi-square test, resonable result was derived.

Robust Filter Based Wind Velocity Estimation Method for Unpowered Air Vehicle Without Air Speed Sensor (대기 속도 센서가 없는 무추력 항공기의 강인 필터 기반의 바람 속도 추정 기법)

  • Park, Yong-gonjong;Park, Chan Gook
    • Journal of the Korean Society for Aeronautical & Space Sciences
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    • v.47 no.2
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    • pp.107-113
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    • 2019
  • In this paper, a robust filter based wind velocity estimation algorithm without an air velocity sensor in an air vehicle is presented. The wind velocity is useful information for the air vehicle to perform precise guidance and control. In general, the wind velocity can be obtained by subtracting an air velocity which is obtained by an air velocity sensor such as a pitot-tube, and a ground velocity which is obtained by a navigation equipment. However, in order to simplify the configuration of the air vehicle, the wind estimation algorithm is necessary because the wind velocity can not be directly obtained if the air velocity measurement sensor is not used. At this time, the aerodynamic coefficient of the air vehicle changes due to the turbulence, which causes the uncertainty of the system model of the filter, and the wind estimation performance deteriorates. Therefore, in this study, we propose a wind estimation method using $H{\infty}$ filter to ensure robustness against aerodynamic coefficient uncertainty, and we confirmed through simulation that the proposed method improves the performance in the uncertainty of aerodynamic coefficient.

Calibration of Discharge Coefficient of Sonic Nozzle Using CVFM (정적형 유량계를 이용한 소닉노즐 유출계수 교정 방법에 관한 연구)

  • Shin, J.H.;Kang, S.B.;Park, K.A.;Lim, J.Y.;Cheung, W.S.
    • Journal of the Korean Vacuum Society
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    • v.19 no.4
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    • pp.243-248
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    • 2010
  • Sonic nozzles have been a standard device for measurement of steady state gas flow, as recommended in ISO 9300. This paper introduces two sonic nozzles of diameter ${\Phi}$ 0.03 mm and ${\Phi}$ 0.2 mm precisely machined according to ISO 9300. The constant volume flow meter(CVFM), readily set up in the Vacuum center of KRISS. was used to calibrate the discharge coefficients of both nozzles. The calibration results were shown to determine them within the 3% expanded measurement uncertainty. Calibrated sonic nozzles were found to be applicable for precision measurement of steady state gas flow in the vacuum process in the ranges of 0.6~1,800 cc/min. Those flow conditions are equivalent to the fine gas flow with Reynolds numbers of 26~12,100. Those encouraging results confirm that calibrated sonic nozzles enable precision measurement of extremely low gas flow encountered very often in th vacuum processes. Both calibrated sonic nozzles are proven to provide the precision measurement of the volume flow rate of the dry vacuum pump within one percent difference in reference to CVFM. Calibrated sonic nozzles are applied to a new 'in-situ and in-field' equipment designed to measure the volume flow rate of vacuum pumps in the semiconductor and flat display processes. Furthermore, they can provide other applications to flow control devices in vacuum, such as MFC, etc.

Development of Environmental Safety Real-Time Monitoring System by Living Area (생활권역별 환경안전 실시간 모니터링 시스템의 개발)

  • Lee, Joo-Hyun;Kim, Joo-Ho;Lee, Seung-Ho
    • Journal of IKEEE
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    • v.23 no.3
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    • pp.1088-1091
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    • 2019
  • In this paper, a real-time monitoring system for environmental safety by living area is proposed. The proposed system is designed to measure radiation, fine dust and basic living information (temperature) using fixed and mobile measuring equipment, and constitutes a web database that stores data received from the equipment. It also develops web programs for displaying received data on PCs and mobile phones. The results of testing the performance of the system by an authorized testing agency showed that the radiation measurement range was measured in the range of $10{\mu}Sv/h$ to 10mSv/h, which is comparable to the world's highest level, and that the accuracy was measured between ${\pm}6.7$ and ${\pm}8.7$ percent of the measurement uncertainty was measured and normal operation at or below the international standard of ${\pm}15$ percent. In addition, the temperature test was conducted on a section of $-20^{\circ}C$ to $50^{\circ}C$ and normal operation was confirmed in response to the temperature change. Stability of radiated electromagnetic waves was ensured by a suitable judgment. The product's testing in general and high and low temperature environments for about four months after the prototype was made confirmed to be more than five years of durability. The measurement range and accuracy of fine dust sensors are compared with those of companies that measure the air environment, and the performance level is similar through the air quality measurement register.

Measurement of Methane Production from Ruminants

  • Bhatta, Raghavendra;Enishi, Osamu;Kurihara, Mitsunori
    • Asian-Australasian Journal of Animal Sciences
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    • v.20 no.8
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    • pp.1305-1318
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    • 2007
  • On a global scale agriculture and in particular enteric fermentation in ruminants is reported to produce about one fourth (21 to 25%) of the total anthropogenic emissions of methane ($CH_4$). Methane is produced during the anaerobic fermentation of hydrolyzed dietary carbohydrates in the rumen and represents an energy loss to the host besides contributing to emissions of greenhouse gases into the environment. However, there appears to be uncertainty in the $CH_4$ estimation from livestock due to the limited availability of data to document the variability at the farm level and also due to the significant impact of diet on the enteric $CH_4$ production. The methane mitigation strategies require robust prediction of emissions from rumen. There are many methods available which would be suitable for measuring $CH_4$ produced from the various stages of animal production. However, several factors need to be considered in order to select the most appropriate technique like the cost, level of accuracy required and the scale and design of the experiments to be undertaken. Selection of any technique depends on the accuracy as each one has its advantages and disadvantages. Screening of mitigation strategies may be evaluated using individual animal before large-scale trials on groups of animals are carried out. In this review various methods for the estimation of methane production from ruminants as well as for the determination of methane production potential of ruminant feeds are discussed. The advantages and disadvantages of the methods starting from respiration chamber, ventilated hood, facemask, sulphur hexafluoride ($SF_6$) tracer technique, prediction equations and meteorological methods to in vitro methods are detailed.

Construction and Measurement of Normal Spectral Emissivity Device using Fourier Transform Infrared Spectrometer (퓨리에 변환 적외선 분광기를 이용한 수직 분광 복사율 측정 장치의 제작과 측정)

  • Jeon, Sang-Ho;Yoo, Nam-Joon;Jo, Jae-Heung;Park, Chul-Woung;Park, Seung-Nam;Lee, Geun-Woo
    • Korean Journal of Optics and Photonics
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    • v.19 no.6
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    • pp.400-407
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    • 2008
  • An Instrument to measure normal spectral emissivity is built using a Fourier Transform-Infrared (FT-IR) spectrometer. The instrument is composed of four main parts, reference blackbody, sample furnace, optics system, and FT-IR spectrometer. Measurement ranges of temperature and wavelength are $200^{\circ}C{\sim}500^{\circ}C$ and $3.5{\mu}m{\sim}20{\mu}m$, respectively. Measured emissivity of the reference blackbody is greater than 0.9993 with combined relative uncertainty less than 0.69%, which can be considered an ideal blackbody. We studied the emissivity of opaque alumina, graphite, anodized aluminum, and steel (IMS 200). It is shown that emissivity increases with the roughness of the steel (IMS 200) surface.

Absolute $^{56}Mn$ Activity Measurement by $4{\pi}{\beta}-{\gamma}$ Conincidence Counting Technique ($4{\pi}{\beta}-{\gamma}$ 동시계수기술에 의한 $^{56}Mn$방사능 절대측정)

  • Hwang, Sun-Tae;Choi, Kil-Oung;Oh, Pil-Jae;Lee, Kyung-Ju;Lee, Kun-Jai
    • Journal of Radiation Protection and Research
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    • v.12 no.2
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    • pp.19-27
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    • 1987
  • In order to determine the $^{56}Mn\;{\gamma}$-detection efficiency of a $MnSO_4$ bath system, it is essential to do the absolute activity measurement of $^{56}Mn$ solution. For the fabrication of $^{56}Mn$ samples, a 13.718 mg of $^{56}Mn$ metal flake with 99.99% purity was irradiated for 12 minutes at the thermal neutron field of about $10^{13}n/cm^2s$ of flux density. The neutron activated $^{56}Mn$ metal sample was dissolved in 50 ml of 0.1 N-HCl solution. The $^{56}Mn$ samples were fabricated by using the dissolved stock solution and the activity of each of them was measured by the $4{\pi}{\beta}-{\gamma}$ coincidence counting technique. The obtained result was 408.070 kBq/mg with total uncertainty of 0.366% at reference date, 0 h on October 15, 1987.

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Gertler-Hagen Hydrodynamic Model Based Velocity Estimation Filter for Long-term Underwater Navigation Without External Position Fix (수중 자율이동체의 장시간 수중항법 성능 개선을 위한 표준 수력학 모델 기반 속도 추정필터 설계)

  • Lee, Yunha;Ra, Won-Sang;Kim, Kwanghoon;Ahn, Myonghwan;Lee, Bum-Jik
    • The Transactions of The Korean Institute of Electrical Engineers
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    • v.65 no.11
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    • pp.1868-1878
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    • 2016
  • This paper proposes a novel velocity estimator for long-term underwater navigation of autonomous underwater vehicles(AUVs). Provided that an external position fix is not given, a viable goal in designing a underwater navigation algorithm is to reduce the divergence rate of position error only using the sporadic velocity information obtained from Doppler velocity log(DVL). For such case, the performance of underwater navigation eventually depends on accuracy and reliability of external velocity information. This motivates us to devise a velocity estimator which can drastically enhance the navigation performance even when the DVL measurement is unavailable. Incorporating the Gertler-Hagen hydrodynamics model of an AUV with the measurement models of velocity and depth sensors, the velocity estimator design problem is resolved using the extended Kalman filter. Different from the existing methods in which an AUV simulator is regarded as a virtual sensor, our approach is less sensitive to the model uncertainty often encountered in practice. This is because our velocity filter estimates the simulator errors with sensor aids and furthermore compensates these errors based on the indirect feedforward manner. Through the simulations for typical AUV navigation scenarios, the effectiveness of the proposed scheme is demonstrated.

Development and Calibration of a Plate Type Eddy Current Standard (평판형 와전류 표준 시험편의 개발 및 교정)

  • Kim, Young-Joo;Kim, Young-Gil;Ahn, Bong-Young;Yoon, Dong-Jin
    • Journal of the Korean Society for Nondestructive Testing
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    • v.27 no.5
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    • pp.393-397
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    • 2007
  • Eddy current standard including an artificial slot for the calibration of absolute type surface probe was fabricated. Developed eddy current standard has the electric conductivity and dimensions, and contains artificial slot as established in ASTM E 1629. The width and depth of artificial slot are 0.1 mm and 0.5 mm respectively. This slot was only possible to measure the depth on the two side edges, and impossible for the middle part with general measurement tools. The ultrasonic test method was applied for measuring depth of the middle part of the artificial slot in the standard. Using this method the dimension could be measured successfully with uncertainty about $15\;{\mu}m$. Calibration of eddy current standard for the absolute probe can be performed by this technique.