• 제목/요약/키워드: Uncertainty measurement

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Calibration by Comparison and Uncertainty Assessment of Industrial Thermometers at the Boiling Point of Nitrogen (질소의 끓는점에서의 산업용 온도계 비교 교정과 불확도 평가)

  • Yang, Inseok;Gam, Kee Sool;Joung, Wukchul;Kim, Yong-Gyoo
    • Journal of Sensor Science and Technology
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    • v.22 no.6
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    • pp.404-409
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    • 2013
  • We devised calibration procedure for industrial thermometers by a comparison method at the boiling point of nitrogen (${\sim}-196^{\circ}C$). The uncertainty of the calibration was 4 mK (k = 2). As experimentally demonstrated in this work, the effect of the atmospheric pressure on the boiling point of nitrogen can be easily detected by the thermometer. Therefore, when the boiling point of nitrogen is used for calibration of thermometer by comparison, either a reference thermometer must be used to provide the reference temperature or the effect of atmospheric pressure should be carefully considered. The use of a copper block with a large thermal mass soaked into the liquid nitrogen was proven to be more reliable, and the stability of the temperature immersed into the copper block was 1.4 mK. The temperatures at the thermometer wells, evaluated by the crossed-measurement method to compensate for the inaccuracy of the thermometers and the linear drift of the temperature of the copper block, were equivalent within 0.23 mK of standard uncertainty.

Method Validation and Uncertainty Estimation for Toluene Measurement in Biological Fluids by HS-GC (HS-GC에 의한 생체 시료내 톨루엔 분석에 대한 방법의 유효화와 불확도 추정)

  • Heo, Sangcheol;Min, Ji-Sook;Park, Jongseo;Lim, Mi-Ae;Park, Sungwoo
    • Analytical Science and Technology
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    • v.17 no.6
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    • pp.443-453
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    • 2004
  • Toluene is currently used as a major organic solvent of glues which are abused by the youngster for its hallucinogenic effect. In this study, toluene determination method using headspace gas chromatography (HS-GC) in the biological fluids like blood, urine and saliva of glue sniffers was validated and related uncertainties were estimated. LOD of $0.01{\mu}g/mL$ in saliva and LOQ of $0.1{\mu}g/mL$ in blood were the highest among LODs and LOQs in urine, blood and saliva. Other performance characteristics such as linearity, working range, accuracy, precision and recovery were also measured. The uncertainty at toluene concentration of $1{\mu}g/mL$ was estimated to be 0.13, 0.09 and $0.17{\mu}g/mL$ for blood, urine and saliva, respectively, and the uncertainty contribution from the least linear regression was dominant at the lower concentration of toluene.

The Effect of Emotional Certainty on Attitudes in Advertising

  • Bok, Sang Yong;Min, Dongwon
    • Asia Marketing Journal
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    • v.14 no.4
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    • pp.57-75
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    • 2013
  • It is a well-established theory that emotion is influential in cognitive processing. Extensive prior research on emotion has shown that emotional factors, such as affect, mood, and feeling, play as information indicating whether he or she has enough knowledge. Most of their findings focused on the effect of emotional valence (i.g., one's subjective positivity or negativity related with the emotion). Recently, several studies on emotion suggest that there is another dimension of emotion, which affects the type of cognitive processing. The studies argue that emotional certainty facilitates heuristic processing, whereas emotional uncertainty promotes systematic processing. Based on the findings, current study examines the effect of certainty on attitudes and recall. Specifically, the authors investigate the effect of certainty on how much effort individuals use to process advertising information and how certainty affects attitude formation toward the advertised product. The authors also focus on recall to clarify the working mechanism of certainty on attitudes, because recall performance reflects the depth of information processing. Based on previous findings, the authors hypothesize that uncertainty (vs. certainty) leads to more favorable attitudes as well as better recall, and conduct an experiment using a fictitious advertisement with 218 participants. The results confirm the predicted effects of certainty only on attitudes not recall. A possible explanation of this discrepancy between attitudes and recall lies in the measurement method, unaided recall. To rule out this possibility, the authors perform an additional analysis with the participants who recall any correct information of the target advertisement. The results show certainty has a negative effect on both attitudes and recall. A bootstrapping test reveals that recall mediates the effect of certainty on attitudes. This result confirms that certainty decreases elaboration, which in turn leads to less favorable attitudes relative to uncertainty. Additionally, our data shows the association among certainty, recall, and attitudes by showing the indirect effect of certainty on attitudes via recall. This research encourages practitioners in the field to emphasize that they should focus on target audiences' emotional certainty before they provide the persuasive message, by showing that uncertainty promotes effortful processing, which in turn leads to better memory and more favorable attitudes.

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Calculation and Uncertainty Estimation of the Volume of Reverberation Chamber with Indeterminate Form (부정형 잔향실의 체적 산출과 체적 불착도 평가)

  • Suh, Jae-Gap;Suh, Sang-Joon
    • The Journal of the Acoustical Society of Korea
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    • v.26 no.8
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    • pp.375-380
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    • 2007
  • A reverberation chamber should be designed and constructed so as to satisfy its purposes and available space. However, it is somewhat difficult to meet the intended design requirements due to various errors from construction process. So, the post-construction measurement of its volume and surface areas is very essential to check the actual volume and volume uncertainty of a reverberation chamber These values should be carefully calculated and accurately estimated since they are used not only to evaluate the acoustic characteristics of building materials but also to calculate uncertainties for other acoustic characteristics. In this work, the method for the calculation and uncertainty estimation of the volume of a reverberation chamber is presented. To this end, the coordinates of all corners was measured with Total Station after construction. The results showed that the calculated volume of the measured reverberation chamber differs by 5 % from the design specification. The expanded volume uncertainty was also estimated to be about 2 % of the total calculated volume.

Analyses of the Basic Inquiry Process in Korean 3-10 Grade Science Textbooks: Focused on Observation and Measurement (우리나라 3-10학년 과학 교과서에 나타난 기초탐구과정 분석: 관찰 및 측정 탐구요소를 중심으로)

  • Park, Bo-Hwa;Kim, Hee-Kyong;Lee, Bong-Woo
    • Journal of The Korean Association For Science Education
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    • v.27 no.5
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    • pp.421-431
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    • 2007
  • The purpose of this study was to examine the characteristics of observation and measurement inquiry process in the Korean science textbooks. For the inquiry process of observation, the higher grade textbooks contained more 'comparative observation' rather than 'simple observation'. Students should express their observation results in written words rather than verbal descriptions in the higher grade. For the inquiry process of measurement, the temperature measurement was the most frequent measurement activity. 'Measurement design' was found more frequently in the lower grade textbooks. The uses of measurement tools were not presented systematically and were presented restrictively when the relevant experiment wanted to use these tools. The higher grade textbooks include 'quantitative measurements' rather than 'qualitative measurements' and 'operation measurement' rather than 'simple measurement'. In the application of measurement results, we had difficulty in finding the activities related with the usage of unit, unit conversion, significant figure, error and uncertainty.

Influence factor analysis on the measurement of smoke density from floor materials in rolling stock (철도차량 바닥재 연기밀도 측정의 영향인자분석)

  • Kwon, Tae-Soon;Lee, Duck-Hee;Park, Won-Hee
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.17 no.11
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    • pp.629-634
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    • 2016
  • In this study, we investigated the effect of factors that influence the measurement of smoke density using synthetic rubber flooring. The characteristics of rolling stock in an enclosed environment can cause enormous loss of life by smoke inhalation during fires inside passenger cars. The amount of smoke generation from interior materials for rolling stock is strictly restricted domestically and in other countries. Precise measurement of smoke density is therefore required to assess the fire performance of interior materials. Major factors that influence the measurement of smoke density include the uniformity of the specimen, the variations in conditions and instruments, and the operational and maintenance environment of the instruments. The contribution of factors was analyzed by estimating the uncertainty to investigate the contribution ratios of the major factors. The results show a contribution ratio of about 86% for the variation from the measurement of light transmission using a photomultiplier tube. Thus, this factor was the most representative for the measurement of smoke density. The contribution ratio of the other factors was low at about 11%, including irradiant flux conditions (${\pm}0.5 kW/m^2$) and the influence of the operational and maintenance environment of the instrument. These results were obtained using specimens with high uniformity.

Optimization of Contaminated Land Investigation based on Different Fitness-for-Purpose Criteria (조사목적별 기준에 부합하는 오염부지 조사방법의 최적화 방안에 관한 연구)

  • Jong-Chun Lee;Michael H. Ramsey
    • Economic and Environmental Geology
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    • v.36 no.3
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    • pp.191-200
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    • 2003
  • Investigations on the contaminated lands due to heavy metals from mining activities or hydrocarbons from oil spillage for example, should be planned based on specific fitness-for-purpose criteria(FFP criteria). A FFP criterion is site specific or varies with situation, based on which not only the data quality but also the decision quality can be determined. The limiting factors on the qualities can be, for example, the total budget for the investigation, regulatory guidance or expert's subjective fitness-for-purpose criterion. This paper deals with planning of investigation methods that can satisfy each suggested FFP criterion based on economic factors and the data quality. To this aim, a probabilistic loss function was applied to derive the cost effective investigation method that balances the measurement uncertainty, which estimates the degree of the data quality, with the decision quality. In addition, investigation planning methods when the objectives of investigations do not lie in the classification of the land but simply in producing the estimation of the mean concentration of the contaminant at the site(e.g. for the use in risk assessment), were also suggested. Furthermore, the efficient allocation of resources between sampling and analysis was also devised. These methods were applied to the two contaminated sites in the UK to test the validity of each method.

Development of Contact-Type Thickness Measurement Machine using LVDT Sensors (LVDT센서를 이용한 접촉식 두께자동측정기 개발)

  • Shin, Ki-Yeol;Hwang, Seon
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.14 no.4
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    • pp.151-159
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    • 2015
  • In this study, we developed an automated contact-type thickness measurement machine that continuously and precisely measures the thickness of a PCB module product using multi-LVDT sensors. The system contains a measurement part to automatically measure the thickness in real time according to the set conditions with an alignment supply unit and unloading unit to separate OK and NG products. The sensors were calibrated before assembly in the measuring machine, and precision and accuracy performance tests were also performed to reduce uncertainty errors in the measurement machine. In the calibration test, the precision errors of the LVDT sensor were determined to be $1-3{\mu}m$ as 0.1% at the measuring range. A measurement error of 0.8 mm and 1.0 mm thickness test standards were found to be $1{\mu}m$ and $4{\mu}m$, and the standard deviations of two 1.0 mm products were measured as $14{\mu}m$ and $8{\mu}m$, respectively. In the measurement system analysis, the accuracies of test PCB standards were found to be $2{\mu}m$ and $3{\mu}m$, respectively. From the results of gage repeatability and reproducibility (R & R) crossed, we found that the machine is suitable for the measurement and process control in the mass production line as 7.92% of total gage R & R and in seven distinct categories. The maximum operating speed was limited at 13 pcs/min, showing a value good enough to measure.

Measurement of Cortisol in Human Serum by Isotope Dilution Liquid Chromatography/Mass Spectrometry and a Comparison through a Proficiency Testing

  • Lee, Hwa-Shim;Shin, Hye-Sun;Park, Sang-Ryoul;Park, Chang-Joon
    • Bulletin of the Korean Chemical Society
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    • v.31 no.5
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    • pp.1149-1154
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    • 2010
  • Liquid chromatography/mass spectrometry using isotope dilution method has been established as a primary method for the measurement of cortisol in human serum. Verification of this method was accomplished by the participation in Consultative Committee for Amount of Substance-Metrology in Chemistry (CCQM) pilot study. Two levels of cortisol certified reference materials were prepared and certified by the established method. They were used as sample materials for the proficiency testing. The expanded uncertainty in the measurement of cortisol in human serum was approximately 1.2% at 95% confidence level. The results of the proficiency testing showed a good precision among the participants, but some bias to the certified values. This means that commercial field laboratories should keep traceability chain to SI unit through available reference measurement procedures and/or available reference materials.

An international Comparison Measurement of Silicon Wafer Sheet Resistance using the Four-point Probe Method

  • Kang, Jeon-Hong;Ying, Gao;Cheng, Yuh-Chuan;Kim, Chang-Soo;Lee, Sang-Hwa;Yu, Kwang-Min
    • Journal of Electrical Engineering and Technology
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    • v.10 no.1
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    • pp.325-330
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    • 2015
  • With approval from the Asia Pacific Metrology Program Working Group on Materials Metrology (APMP WGMM), an international comparison for sheet resistance standards for silicon wafers was firstly conducted among Korea Research Institute of Standards and Science (KRISS) in Korea, CMS/ITRI in Taiwan, and NIM in China, which are national metrology institutes (NMIs), from August 2011 to January 2012. The sheet resistance values of the standards are $10{\Omega}$, $100{\Omega}$, and $1000{\Omega}$; the measurement was conducted in sequence at KRISS, CMS/ITRI, NIM, and KRISS again using the four-point probe method with single and dual configuration techniques. The reference value for the measurement results of the three NMIs was obtained through averaging the values of the three results for each sheet resistance range. The differences between the reference value and the measured values is within 0.22% for $10{\Omega}$, 0.17% for $100{\Omega}$, and 0.12% for $1000{\Omega}$. Therefore, the international consistency for conducting sheet resistance measurements is confirmed within 0.22% through the APMP WGMM approved comparison.