• Title/Summary/Keyword: Ultrasonic Material

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Synthesis and Characterization of a Ternary Nanocomposite Based on CdSe Decorated Graphene-TiO2 and its Application in the Quantitative Analysis of Alcohol with Reduction of CO2

  • Ali, Asghar;Biswas, Md Rokon Dowla;Areerob, Yonrapach;Nguyen, Dinh Cung Tien;Oh, Won-Chun
    • 한국세라믹학회지
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    • 제55권4호
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    • pp.381-391
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    • 2018
  • In this work, photocatalytic $CO_2$ reduction over a CdSe-graphene-$TiO_2$ nanocomposite has been studied. The obtained material was successfully fabricated via ultrasonic technique. The physical properties of the as-synthesized materials were characterized by some physical techniques. The $TiO_2$ and CdSe dispersed graphene nanocomposite showed excellent results of strong reduction rates of $CO_2$ compared to the results of bare $TiO_2$ and binary CdSe-graphene. An outstanding point of the combination of CdSe-$TiO_2$ and graphene appeared in the form of great photocatalytic reduction capability of $CO_2$. The photocatalytic activity of the asfabricated composite was tested by surveying for the photoreduction of $CO_2$ to alcohol under UV and visible light irradiation, and the obtained results imply that the as-prepared CdSe-graphene-$TiO_2$ nanocomposite is promising to become a potential candidate for the photocatalytic $CO_2$ reduction.

Design of a Valveless Type Piezoelectric Pump for Micro-Fluid Devices

  • Kim, Hyun-Hoo;Oh, Jin-Heon;Yoon, Jae-Hun;Jeong, Eui-Hwan;Lim, Kee-Joe
    • Transactions on Electrical and Electronic Materials
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    • 제11권2호
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    • pp.65-68
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    • 2010
  • The operation principle of a traveling wave rotary type ultrasonic motor can be successfully applied to the fluidic transfer mechanism of the micro-pump. This paper proposes an innovative valveless micro-pump type that uses an extensional vibration mode of a traveling wave as a volume transportation means. The proposed pump consists of coaxial cylindrical shells that join the piezoelectric ceramic ring and metal body, respectively. In order to confirm the actuation mechanism of the proposed pump model, a numerical simulation analysis was implemented. In accordance with the variations in the exciting wave mode and pump body dimension, we analyzed the vibration displacement characteristics of the proposed model, determined the optimal design condition, fabricated the prototype pump from the analysis results and evaluated its performance. The maximum flow rate was approximately $595\;{\mu}L/min$ and the highest back pressure was 0.88 kPa at an input voltage of $130\;V_{rms}$. We confirmed that the peristaltic motion of the piezoelectric actuator was effectively applied to the fluid transfer mechanism of the valveless type micro pump throughout this research.

Assessment of London underground tube tunnels - investigation, monitoring and analysis

  • Wright, Peter
    • Smart Structures and Systems
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    • 제6권3호
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    • pp.239-262
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    • 2010
  • Tube Lines has carried out a "knowledge and investigation programme" on the deep tube tunnels comprising the Jubilee, Northern and Piccadilly lines, as required by the PPP contract with London Underground. Many of the tunnels have been in use for over 100 years, so this assessment was considered essential to the future safe functioning of the system. This programme has involved a number of generic investigations which guide the assessment methodology and the analysis of some 5,000 individual structures. A significant amount of investigation has been carried out, including ultrasonic thickness measurement, detection of brickwork laminations using radar, stress measurement using magnetic techniques, determination of soil parameters using CPT, pressuremeter and laboratory testing, installation of piezometers, material and tunnel segment testing, and trialling of remote photographic techniques for inspection of large tunnels and shafts. Vibrating wire, potentiometer, electro level, optical and fibre-optic monitoring has been used, and laser measurement and laser scanning has been employed to measure tunnel circularity. It is considered that there is scope for considerable improvements in non-destructive testing technology for structural assessment in particular, and some ideas are offered as a "wish-list". Assessment reports have now been produced for all assets forming Tube Lines' deep tube tunnel network. For assets which are non-compliant with London Underground standards, the risk to the operating railway has to be maintained as low as reasonably practicable (ALARP) using enhanced inspection and monitoring, or repair where required. Monitoring techniques have developed greatly during recent years and further advances will continue to support the economic whole life asset management of infrastructure networks.

레이저를 이용한 웨이퍼 다이싱 특성 (Characteristics of Laser Wafer Dicing)

  • 이용현;최경진;유승열
    • 반도체디스플레이기술학회지
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    • 제5권3호
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    • pp.5-10
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    • 2006
  • This paper investigates cutting qualities after laser dicing and predicts the problems that can be generated by laser dicing. And through 3 point bending test, die strength is measured and the die strength after laser dicing is compared with the die strength after mechanical sawing. Laser dicing is chiefly considered as an alternative to overcome the defects of mechanical sawing such as chipping on the surface and crack on the back side. Laser micromachining is based on the thermal ablation and evaporation mechanism. As a result of laser dicing experiments, debris on the surface of wafer is observed. To eliminate the debris and protect the surface, an experiment is done using a water soluble coating material and ultrasonic. The consequence is that most of debris is removed. But there are some residues around the cutting line. Unlike mechanical sawing, chipping on the surface and crack on the back side is not observed. The cross section of cutting line by laser dicing is rough as compared with that by mechanical sawing. But micro crack can not be seen. Micro crack reduces die strength. To measure this, 3 point bending test is done. The die strength after laser dicing decreases to a half of the die strength after mechanical sawing. This means that die cracking during package assembly can occur.

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유기 초음파화학. 초음파가 히드라진, 철, 활성탄을 이용한 방향족 니트로기의 환원반응에 미치는 영향 (The Effects of Sonic Waves on the Reduction of Aromatic Nitro Groups Using Iron, Hydrazine Hydrate and Activated Carbon)

  • 신대현;한병희;조성윤
    • 대한화학회지
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    • 제30권1호
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    • pp.105-108
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    • 1986
  • 초음파(50KHz)가 상온 상압하에서 히드라진 철 활성탄을 이용한 방향족 니트로기를 방향족 아미노기로의 환원반응을 크게 가속시켜 3시간만에 100% 전환율을 얻을 수 있었다. 활성탄은 탈색이나 반응성이 큰 물질의 분말을 섞는데 사용되어 왔으나 히드라진 철을 이용한 방향족 니트로기의 환원반응에서는 활성탄 없이는 반응이 전혀 일어나지 않으며 활성탄의 증가에 따라 환원율이 높아지는 결과를 얻었다.

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소컷 및 원공 주위의 피로균열 형태변화와 층간분리거동 (I) - 아라미드섬유 강화 금속적층재의 경우 - (Fatigue Crack and Delamination Behavior in the Composite Material Containing n Saw-cut and Circular Hole (I) - Aramid Fiber Reinforced Metal Laminates -)

  • 송삼홍;김철웅
    • 대한기계학회논문집A
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    • 제27권1호
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    • pp.58-65
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    • 2003
  • The aramid fiber reinforced metal laminates(AFRMLs) used for the wing part fair flight suffer the cyclic bending moment of variable amplitude during service. The fatigue crack propagation and delamination behavior in AFRMLs containing a saw-cut and circular hole was investigated using the average stress criterion(ASC) model. Mechanical tests were carried out using the cyclic bending moment of 4.9 N . m and delamination was observed by ultrasonic C-scan images. In case of AFRMLs containing a saw-cut fatigue crack propagated in aluminum matrix, inducing delamination. However, in case of AFRMLs containing a circular hole, delamination formed with two types under cyclic bending moment of 4.9 N . m. First, delamination formed along the fatigue crack in aluminum matrix. Second, delamination formed without any fatigue crack around the circular hole. Therefore, delamination was formed depending on the stress distribution near the circular hole.

Stochastic Estimation of Acoustic Impedance of Glass-Reinforced Epoxy Coating

  • Kim, Nohyu;Nah, Hwan-Seon
    • 비파괴검사학회지
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    • 제34권2호
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    • pp.119-127
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    • 2014
  • An epoxy coating applied to the concrete surface of a containment building deteriorates in hazardous environments such as those containing radiation, heat, and moisture. Unlike metals, the epoxy coating on a concrete liner absorbs and discharges moisture during the degradations process, so it has a different density and volume during service. In this study, acoustic impedance was adopted for characterizing the degradation of a glass-reinforced epoxy coating using the acoustic reflection coefficient (reflectance) on a rough epoxy coating. For estimating the acoustic reflectance on a wavy epoxy coating surface, a probabilistic model was developed to represent the multiple irregular reflections of the acoustic wave from the wavy surface on the basis of the simulated annealing technique. A number of epoxy-coated concrete specimens were prepared and exposed to accelerated aging conditions to induce an artificial aging degradation in them. The acoustic impedance of the degraded epoxy coating was estimated successfully by minimizing the error between a waveform calculated from the mathematical model and a waveform measured from the surface of the rough coating.

용융탄산염 연료전지 양극용 다공성 cermet 전극제조에 관한 연구 (A study on the fabrication of porous cermet electrode for molten carbonate fuel cell anode)

  • 이규환;장도연;김만;강성군
    • 한국표면공학회지
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    • 제26권6호
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    • pp.291-298
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    • 1993
  • In order to substitute for porous nickel anode in Molten Carbonate Fuel Cell(MCFC), porous cermet elec-trode was fabricated with Ni and Ni-P coated ceramic powder. Ni and Ni-P were coated by electroless plat-ing method in the nickel solution containing of hydrazine and sodium hypophosphate as a reducing agent. The plating solution was stirred by air and mechanical agitator. Ultrasonic irradiation was applied to the plating bath to improved the effect of agitation and coating speed. Electorde was formed by pressing method and doc-tor blade method followed by sinterd at$ 800^{\circ}C$ for 6 hours in H2 environment. Anode performance test carried out by potentiodynamic polarization technique in the MCFC operating condition and 154-161mA/$\textrm{cm}^2$ as ob-tained as a anode current density at the+100mV overpotential.

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초음파에 의해 무화된 케로신 분무연소에서의 OH 라디칼 및 CH 라디칼 자발광 특성 (OH-and CH-Radical Chemiluminescence Characteristics in the Spray Combustion of Ultransonically Atomized Kerosene)

  • 김민철;김정수
    • 한국추진공학회지
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    • 제22권1호
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    • pp.72-79
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    • 2018
  • 초음파 진동자에 의해 미립화된 케로신 분무연소의 OH 라디칼과 CH 라디칼의 자발광 특성을 고찰하기 위한 실험이 수행되었다. ICCD 카메라를 이용하여 분무화염의 자발광 강도를 측정하였으며, 연소 시 소모된 연료량은 정밀유량측정법으로 계측하였다. 그 결과, 연료소모율은 수송기체인 공기 공급유량에 선형적으로 증가하였으며, 분무연소의 특징인 전형적인 그룹 연소가 관찰되었다. OH 라디칼과 CH 라디칼을 분석한 결과, 분사방향으로의 유량 증가에 따라 라디칼 방사강도의 최댓값은 감소하고 그 위치는 후류로 이동하여 반응대의 폭은 증가하였다.

이중 초음파 조사 시스템에서 진동부 사이의 거리가 초음파 화학 반응에 미치는 영향 (The Effect of Distance between Two Transducers on Sonochemical Reactions in Dual Irradiation Systems)

  • 김은경;손영규
    • 한국지하수토양환경학회지:지하수토양환경
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    • 제18권5호
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    • pp.39-45
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    • 2013
  • Many researchers have studied the effectiveness of ultrasound in chemical and environmental engineering fields including material synthesis, pollutant removal, cleaning, extraction, and disinfection. Acoustic cavitation induced by ultrasound irradiation in aqueous phase can cause various sonophysical and sonochemical reactions without any chemicals. However most of the previous studies focused only on the relationships between ultrasonic conditions and the results of sonochemical reactions in lab-scale sonoreactors. As a results of this, only a few studies have been devoted to design and optimization of industrial scale sonoreactors. In this study, the effect of the distance between two opposite transducer modules on sonochemical reactions was investigated in single and dual irradiation systems (334 kHz) for four distances including 50, 100, 150, and 200 mm using KI dosimetry. It was found that the dual irradiation systems provided higher performance in terms of the zeroth reaction coefficient and the cavitation yield compared to the single irradiation systems. The sonochemiluminescence (SCL) images for the visualization of the cavitation field showed that cavitation active zone was larger and sonochemical reaction intensity was much higher in the dual irradiation system than in the single irradiation system.