• Title/Summary/Keyword: Transgranular

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Characteristics of Fatigue Crack Propagation and Changes in Strain Induced Martensite α' of STS 304 Stainless Steel (LNG 304 스테인레스강의 피로균열전파특성과 변형유발 마르텐사이트 함량의 변화)

  • Kim, Song-Hee;Pak, Hyung-Rae;Lee, Hyun-Seung
    • Journal of Industrial Technology
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    • v.21 no.B
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    • pp.341-348
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    • 2001
  • The effect of initial ${\alpha}^{\prime}$ in STS 304 Stainless Steel on fatigue resistance, and fatigue crack propagation behavior was studied with using C-T specimens. Higher ${\Delta}K_{th}$ was observed in the specimens with the content of 0% initial ${\alpha}^{\prime}$ than in the contents of 2% and 33% initial ${\alpha}^{\prime}$. The difference of da/dN at the same level of ${\Delta}K$ was distinctive in low and intermediate level of ${\Delta}K$ however became less different as the level of ${\Delta}K$ increased. It is because the formation of strain induced martensite occurred readily in lower ${\alpha}^{\prime}$ at the vicinity of the fatigue crack tip, which causes compressive residual stresses resulting in the enhancement of crack closure. In general fatigue cracks propagated transgranular mode and many segments of ridges were observed on the fracture surfaces. At the higher contents of initial ${\alpha}^{\prime}$ appeared the smaller size of ridge segments. Slips in austenite were blocked more frequently by the martensite colonies formed in austenite.

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Cracking Susceptibility of Laser Cladding Process with Co-Based Metal Matrix Composite Powders (레이저 클래딩 공정 조건이 코발트 합금-텅스텐 카바이드 혼합 코팅층의 균열 발생에 미치는 영향)

  • Lee, Changmin;Park, Hyungkwon;Lee, Changhee
    • Journal of Welding and Joining
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    • v.32 no.6
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    • pp.41-46
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    • 2014
  • In this study, cracking susceptibility of laser cladding was investigated according to the processing parameters such as laser power, scan speed and feeding rate with blended powders of stellite#6 and technolase40s (WC+NiCr). The solidification microstructure of clad was composed of Co-based dendrite structures with ${\gamma}+Cr7C3$ eutectic phases at the dendritic boundaries. The crack propagation showed transgranular fracture along dendritic boundaries due to brittle chrome carbide at the eutectic phases. From results of fractography experiments, the fracture surface was typical cleavage brittle fracture in the clad and substrate. The number of clad cracks, caused by a tensile stress after the solidification, increased with increase of laser power, scan speed and feeding rate. Increase of the laser power caused large pores by facilitating WC decarburizing reaction. And the pores affected increase of crack susceptibility. High scan speed caused increment of clad cracks due to thermal stress and WC particle fractures. Also, increase of the feeding rate accompanied an amount of WC particles causing crack initiation and decarburizing reaction.

A Study on the Ceria Stabilized Tetragonal Zirconia Polycrystals(Ce-TZP)(III) : Effect of Al2O3 Addition on the Mechanical Properities and Microstructures of Ce-TZP (CeO2안정화 정방정 Zirconia 다결정체(Ce-TZP)에 관한 연구(III) : Ce-TZP의 기계적성질 및 미세조직에 미치는 Al2O3첨가의 영향)

  • 김문일;박정현;강대석;문성환;안계원
    • Journal of the Korean Ceramic Society
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    • v.27 no.1
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    • pp.55-61
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    • 1990
  • Effect of Al2O3 addition on the mechanical properties and microstructure of Ce-TZP were studied. 12, 14, 16Ce-TZP containing 0-40wt% Al2O3 were prepared by sintering at 155$0^{\circ}C$ for 2h. in air. Density, linear shrinkage, bending strength, Vickers hardness, microstructuer and the amount of stress induced phase transformation were examined. Vickers hardness increased linearly with increasing amounts of Al2O3. The amount of transformation and fracture toughness decreased linearly with increasing amount of Al2O3. Linear shrinkage and relative density decreased with increasing Al2O3 content in all composition of Ce-TZP. Grain growth of Ce-TZP was inhibited by Al2O3 dispersion and fracture mode of Ce-TZP/Al2O3 composites transformed from intergranular to transgranular fracture as the amount of Al2O3 increased. TEM observation revealed that Al2O3 particles were located mainly at grain boundaries of ZrO2.

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Stress Corrosion Cracking Susceptibility Evaluation by Small Punch Test (소형펀치시험법에 의한 응력부식균열 감수성평가에 관한 연구)

  • 유효선;이송인;정세희
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.17 no.8
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    • pp.2033-2042
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    • 1993
  • In conventional SCC susceptibility test, there are constant strain test, constant load test, slow strain rate test(SSRT) and K$_{ISCC}$ test. Among them, the SSRT method is much more aggressive in producing SCC than the other tests, so that the test time of it is considerably reduced. But this SSRT method has mostly been worked using the uniaxial tensile specimen untill now. Therefore, the SSRT method using the tensile specimen(Ten-SSRT) has much difficulty in SCC susceptibility evaluation of a localized region like weldment and the advantage material of high order. Recentely, the small punch(SP) test method using miniaturized small specimen is the very effective test method for fracture strength evaluation of a localized region like weldment and fusion reactor wall irradiated in the nuclear power plant. This paper investigated the possibility of SCC susceptibility evaluation by the SP-SSRT method using the miniaturized small specimen. Therefore, we obtained the result that the SP-SSRT had the possibility for the evaluations of SCC susceptibility for shorter time to corrosive environment compare to Ten-SSRT which was conventional method.

A Study on Laser Assisted Machining for Silicon Nitride Ceramics (IV) - Mechanism and Application of LAM for Silicon Nitride Ceramics - (질화규소 세라믹의 레이저 예열선삭에 관한 연구 (IV) - 질화규소 세라믹의 레이저예열선삭 메커니즘 및 적용 -)

  • Kim, Jong-Do;Lee, Su-Jin;Park, Seo-Jeong;Lee, Jae-Hoon
    • Journal of Welding and Joining
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    • v.28 no.6
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    • pp.40-44
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    • 2010
  • Laser assisted machining (LAM) has been researched in order to machine the silicon nitride ceramics economically and effectively. LAM is an effective machining method by local heating of the cutting part to the softening temperature of the silicon nitride using laser beam. When silicon nitride ceramics is heated using a laser beam, the surface of silicon nitride ceramic is softened, oxidized and decomposed. And then surface hardness is decreased. Through machining in low viscosity and hardness conditions, silicon nitride was machined effectively and the life span of tool was increased. The plastic deformation was occurred due to softening of amorphous YSiAlON above $ 1,000^{\circ}C$. Transgranular fracture of ${\beta}-Si_3N_4$ was occurred when YSiAlON was not softened, but mostly intergranular fracture was occurred by the plastic deformation of softened YSiAlON.

Study on Surface Crack Propagation Behaviour of Mild Steel Weldment in Synthetic Sea Water (인공해수중에서 연강 용접부의 표면구열 성장거동)

  • 이종기;정세희
    • Transactions of the Korean Society of Mechanical Engineers
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    • v.14 no.2
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    • pp.492-501
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    • 1990
  • It was known that the fracture incidences of offshore structure were mostly originated from the surface defects. Especially, in the case of the welded structures, since the welded region has some defects and incomplete beads which are apt to behave like the surface cracks, it has been necessary to evaluate the environmental effects on crack growth at HAZ for the design crack growth behaviour at multi-pall HAZ for SWS41 steel under free corrosion and cathodic protection(-0.9V vs Ag/Agcl) conditions. The results are summarized as follows ; (1) Crack growth rate of the as weld in air was faster than that of the parent and PWHT specimens over all .DELTA.K rang. (2) In free corrosion test, surface crack growth rate of the as welded was decreased in comparison with that of the parents. (3) In fatigue test under cathodic protection, cathodic electric potential(-0.9V vs Ag/Agcl) for the SWS41 steel parent was effective, while for the as welded ineffective. (4) There was a tendency that the exponent(m) of the Paris' equation was decreased in order of microhardness magnititude in air and under cathodic protection conditions and vise versa in free corrosion. (5) Fracture surface has dimples and ductile striations in air test, but transgranular cracks and brittle striations under cathodic protection test.

Effects of B and Si Additions on the $DO_3{\rightleftharpoons}B2$ Transition Temperature, Microstructure and Corrosion Behavior of Fe-25at%Al Alloys (Fe-25at%Al합금의 $DO_3{\rightleftharpoons}B2$ 천이온도, 미세조직 및 부식거동에 미치는 B, Si의 영향)

  • Choi, Dap-Chun;Hwang, Keum-Yeon
    • Journal of Korea Foundry Society
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    • v.12 no.2
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    • pp.131-138
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    • 1992
  • The effects of B additions, alone or in combination with Si, on the microstructure, $DO_3{\rightleftharpoons}B2$ transition temperature($T_c$) and corrosion behavior of Fe-25at%Al alloys were investigated. The raw materials were arc-melted in vacuum and then subjected to the following heat treatments to maximize the $DO_3$ order : homogenized at $1000^{\circ}C$ for 48hrs, slowly cooled to $500^{\circ}C$, and held at that temperature for 24hours. Results showed that the B addition to Fe-25at%Al alloys does indeed refine the grain and change from intergranular to transgranular fracture mode at room temperature, indicating a strengthening of grain boundaries. The Fe-25at% Al-1at% B-3at% Si alloy showed the highest $T_c$(${\Delta}T_c=150^{\circ}C$) in this work. However, the effectiveness of Si in raising $T_c$ decreased with more than 5at% Si additions combined with B. Since the preferential corrosion occurs at the precipitates, the corrosion resistance decreased due to the increased amount of precipitates with alloying additions.

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Failure Analysis of a Ball in the Nuclear Fuel Exchanger

  • Kim, H.P.;Kim, D.J.;Hwang, S.S.;Joung, M.K.;Lim, Y.S.;Kim, J.S.
    • Corrosion Science and Technology
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    • v.4 no.5
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    • pp.211-216
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    • 2005
  • Failure analysis of the latch ram ball and the C-ram ball with the trade name AFBMA Gr. 50 Colmonoy No. 6, has been performed to identify the root cause of the failure. The study required the extraction of the both failed and normal balls from the nuclear fuel exchanger. Microstructures of both balls were examined after polishing and etching. Breaking tests of both the ball revealed similarity in cleavage surfaces. Fracture surfaces of both failed ball and normal ball after breaking test were examined with SEM and EDX. Microstructure of the ball revealed an austenite phase with coarse Cr rich precipitate. Indented marks observed on the surface of the failed ball are believed to be produced by overloading. In the light of the afore mentioned observations and studies, the failure mechanism of the ball in nuclear fuel exchanger seem to be caused by impact or mechanical overloading on ball.

Cyclic Creep Properties of Nicoseal(Fe-29Ni-17Co) Alloy (Nicoseal(Fe-29Ni-17Co) 합금의 Cyclic 크리프 특성)

  • Park, Yong-Gwon;Choi, Jae-Ha
    • Journal of the Korean Society for Heat Treatment
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    • v.18 no.3
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    • pp.177-182
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    • 2005
  • The steady state cyclic mechanism, and the behaviour of Nicoseal(Fe-29Ni-17Co) have been examined under the condition of square wave stress cyclic tension creep test at the temperature, stress and frequency range of $430{\sim}470^{\circ}C$($0.41{\sim}0.43T_m$), 353~383 MPa, and 3 cpm, respectively. Also, the relationship between cyclic creep and static creep have been examined. The stress exponents(n) for the static creep deformation of this alloy were 11.6, 10.0, 8.4 and 7.9 at the temperature of 430, 445, 460 and $470^{\circ}C$, respectively. The apparent activation energies (Q) for the static creep deformation were 54.2, 51.8, 49.7 and 46.8 kcal/mole for the stress of 353, 363, 373 and 383 MPa, From the above results, it could be considered that the cyclic creep accelaration phenomena was obtained and that the cyclic deformation for Nicoseal seemed to be controlled by dislocation climb over the range of experimental conditions. Nicoseal alloy under the cyclic creep conditions was obtained as P=(T+460)(logt+17). The failure plane observed by SEM showed up transgranular fracture at all range.

Microstructural Study of Creep-Fatigue Crack Propagation for Sn-3.0Ag-0.5Cu Lead-Free Solder

  • Woo, Tae-Wuk;Sakane, Masao;Kobayashi, Kaoru;Park, Hyun-Chul;Kim, Kwang-Soo
    • Journal of the Microelectronics and Packaging Society
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    • v.17 no.3
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    • pp.33-41
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    • 2010
  • Crack propagation mechanisms of Sn-3.0Ag-0.5Cu solder were studied in strain controlled push-pull creepfatigue conditions using the fast-fast (pp) and the slow-fast (cp) strain waveforms at 313 K. Transgranular cracking was found in the pp strain waveform which led to the cycle-dominant crack propagation and intergranular cracking in the cp strain waveform that led to the time-dominant crack propagation. The time-dominant crack propagation rate was faster than the cycle-dominant crack propagation rate when compared with J-integral range which resulted from the creep damage at the crack tip in the cp strain waveform. Clear recrystallization around the crack was found in the pp and the cp strain waveforms, but the recrystallized grain size in the cp strain waveform was smaller than that in the pp strain waveform. The cycle-dominant crack propagated in the normal direction to the specimen axis macroscopically, but the time-dominant crack propagated in the shear direction which was discussed in relation with shear micro cracks formed at the crack tip.