• 제목/요약/키워드: Time Determination

검색결과 2,982건 처리시간 0.031초

Structure Determination of Syndecan-4 Transmembrane Domain using PISA Wheel Pattern and Molecular Dynamics simulation

  • Choi, Sung-Sub;Jeong, Ji-Ho;Kim, Ji-Sun;Kim, Yongae
    • 한국자기공명학회논문지
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    • 제18권2호
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    • pp.58-62
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    • 2014
  • Human transmembrane proteins (hTMPs) are closely related to transport, channel formation, signaling, cell to cell interaction, so they are the crucial target of modern medicinal drugs. In order to study the structure and function of these hTMPs, it is important to prepare reasonable amounts of proteins. However, their preparation is seriously difficult and time-consuming due to insufficient yields and low solubility of hTMPs. We tried to produce large amounts of Syndecan-4 transmembrane domain (Syd4-TM) that is related to the healing wounds and tumor for a long time. In this study, we performed the structure determination of Syd4-TM combining the Polarity Index at Slanted Angle (PISA) wheel pattern analysis based on $^{15}N-^1H$ 2D SAMPI-4 solid-state NMR of expressed Syd4-TM and Molecular Dynamics (MD) simulation using Discovery Studio 3.1.

Determination of Optimal Cell Capacity for Initial Cell Planning in Wireless Cellular Networks

  • Hwang, Young-Ha;Noh, Sung-Kee;Kim, Sang-Ha
    • Journal of Information Processing Systems
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    • 제2권2호
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    • pp.88-94
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    • 2006
  • In wireless cellular networks, previous researches on admission control policies and resource allocation algorithm considered the QoS (Quality of Service) in terms of CDP (Call Dropping Probability) and CBP (Call Blocking Probability). However, since the QoS was considered only within a predetermined cell capacity, the results indicated a serious overload problem of systems not guaranteeing both CDP and CBP constraints, especially in the hotspot cell. That is why a close interrelationship between CDP, CBP and cell capacity exists. Thus, it is indispensable to consider optimal cell capacity guaranteeing multiple QoS (CDP and CBP) at the time of initial cell planning for networks deployment. In this paper, we will suggest a distributed determination scheme of optimal cell capacity guaranteeing both CDP and CBP from a long-term perspective for initial cell planning. The cell-provisioning scheme is performed by using both the two-dimensional continuous-time Markov chain and an iterative method called the Gauss-Seidel method. Finally, numerical and simulation results will demonstrate that our scheme successfully determines an optimal cell capacity guaranteeing both CDP and CBP constraints for initial cell planning.

흡착벗김 전압전류법적 지르코늄의 정량 (Adsorptive Stripping Voltammetrical Determination of Zirconium)

  • 최원형;이진식;김도훈;김종철
    • 분석과학
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    • 제6권5호
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    • pp.425-433
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    • 1993
  • oxine을 리간드로 이용하여 흡착벗김 전압전류법으로 극미량의 지르코늄을 정량하는 방법을 연구하였다. 이때 지지전해질은 $2.5{\times}10^{-3}M$ borax 완충용액을 사용하였고, oxine의 농도가 $4{\times}10^{-8}M$로 되도록 하여 실험하였다. accumulation potential을 -0.2V, accumulation time을 400sec로 하고 scan rate를 4mV/sec로 하여 실험한 결과 지르코늄의 농도가 $1{\sim}100{\mu}g/L$ 범위에서 얻은 검정곡선은 직선성을 나타내었다.

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SRM 컨버터에서 자기동조 방식에 의한 턴오프 각의 결정 (Determination of Optimal Turn-off Angle for SRM Converter Using Self-Tuning Method)

  • 장도현;문진영
    • 전력전자학회논문지
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    • 제3권4호
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    • pp.418-425
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    • 1998
  • 본 논문에서는 위상각 제어에서 주어진 턴온 각에서 최대의 토크를 유지하기 위한 적절한 턴오프 각을 자기동조방식(self-tuning method)에 의해 결정하는 방식을 제안하였다. 엔코더에 의해 샘플링 시간(sampling time)동안 구해진 펄스 수는 바로 이전의 샘플링시간 동안 구해진 펄스 수와 비교하여 턴오프 각을 앞으로 또는 뒤로 이동한다. 이러한 과정을 되풀이함으로서 최대 토크를 발생하는 턴오프 각을 결정하게 된다. 실제 회로에서는 원 칩 마이크로프로세서에 의해 처리되었으며 실험을 통해 턴온 각이 변하더라도 자기동조방식에 의해 턴오프 각을 조정하면 빠른 속도가 유지됨을 보여 주었다.

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HPLC를 이용한 carbamate계 농약의 다성분 동시분석 (A study on simultaneous determination of carbamate pesticides by HPLC)

  • 송영각;서영철;현공율;조우영;이종인
    • 한국동물위생학회지
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    • 제26권2호
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    • pp.145-149
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    • 2003
  • To explore the most sensitive and useful method for simultaneous determination of 8 carbamate pesticides in livestock productions, the mixture of 8 carbonates was determined by HPLC with scanning fluorescence detector. For mobile phase water, acetonitrile and methanol program gradient showed more applicable sensitivity than water and acetonitrile program gradient used ExW 339 nm and EmW 445 nm for fluorescence detector. On using carbamate columns, the retention time was within 4 to 20 minutes. And this made it possible to separate and detect simultaneously. therefore we could analyze it exactly and efficiently and reduce time. The preparation process of MSPD method showed that the high recovery rate was more than 88.5% in most of the carbamate pesticides. Therefore we could say that it was an efficient and fast method analyzing out of lots of samples.

수익률을 고려한 수용가측 전자전력저장시스템의 최적용량 선정 (Determination of Optimal sizes of Battery Energy Storage System Considering Rate-Of-Return for Customers-side)

  • 홍종석;김재철;최준호;손학식
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 2001년도 추계학술대회 논문집 전력기술부문
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    • pp.146-148
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    • 2001
  • This paper discusses the optimal sizes of BESS. The goal must be optimized electricity charge of the customers-side with choosing the time-of-use rates. Therefore the cost is minimized by BESS installed the customers-side. Feasible ROR that means the ratio of capital costs to economic effect owned the optimal BESS sizes is determined the suitable domestic condition based on the battery cost and power converter system cost. Payback period times can be presented by BESS through the ROR. Multi-Pass Dynamic Programming(MPDP) algorithm is applied to the customer for the optimal sizes determination in this paper. It is to solve the optimal solution under the constraints. To investigate the efficiencies of the constraints, it is applied the typical load curve to the high-voltage customer owned Time-Of-Use(TOU) whether BESS is installed or not. Well, The result is obtained that feasible BESS sizes can be achieved the suitable customers-side of meter through the ROR.

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Dielectrophoretic Levitation을 이용한 세포막의 전기적 특성 결정 (Determination of Electric Parameters of Cell Membranes Using Dielectrophoretic Levitation)

  • 김용욱;이상욱;이상훈;김용권
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 1994년도 하계학술대회 논문집 A
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    • pp.183-185
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    • 1994
  • A new method for determination of electric parameter of cell membranes is proposed. Two circular electrodes is designed to have repulsive force. From the potential energy analysis, stable points where a cell is levitated between electrodes exist and move as frequency or voltage change. The levitated cell in the stable point fall freely when DEP force is zero. The DEP force is dependent on the frequency and the force is zero at the critical frequency. The critical frequency is determined by measuring the difference between the time taken at zero-applied voltage and the time taken at the frequency and the voltage. For example, the critical frequency and stable points of N.crassa slime cell is numerically evaluated. In the exeriment, polystyrene in water is levitated at the stable point. We show that the stable point move as the applied voltage is changed.

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NMR을 이용한 홍삼의 용적밀도 측정 및 내부 조직 판별 (Determination of Bulk Density and Internal Structure of Red Ginseng Root Using NMR)

  • 장기철
    • Journal of Ginseng Research
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    • 제22권2호
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    • pp.96-101
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    • 1998
  • This paper describes the determination of bulk density and the discrimination of internal structure of red ginseng by nuclear magnetic resonance (NMR). The 102 red ginseng roots were tested for bulk density. The NMR properties measured by NMR parameters such as spin-lattice relaxation time ($T_1$) and spin-spin relaxation time ($T_2$) were determined using the low field proton NMR analyzer. Bulk density of red ginseng root showed a highly negative significant correlation (r=-0.8934) with the value of $T_1$, but a highly positive significant correlation (r=0.7672 and 0.5909) with the value of T21 (short T2) and T22 (long T2), respectively. Multiple regression equation, Y=-0.0069.$T_1$+0.3044.$T_{21}$-0.0156.$T_{22}$-0.6368, using the MNR parameter values of 80 red ginseng roots can effectively predict the bulk density of 22 red ginseng roots with the correlation coefficient of 0.9396 and the standard error of 0.086. The differences in the internal structure of normal and inside white part of red ginseng were easily found by the signal intensity of NMR image based on magnetic properties of proton nucleus.

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Extraction Equilibria and Solvent Sublation for Determination of Ultra Trace Bi(Ⅲ), In(Ⅲ) and TI(Ⅲ) in Water Samples by Ion-Pairs of Metal-2-Naphthoate Complexes and Tetrabutylammonium Ion

  • Kim, Young-Sang;Choi, Yoon-seok;Lee, Won
    • Bulletin of the Korean Chemical Society
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    • 제23권10호
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    • pp.1381-1391
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    • 2002
  • The solvent sublation using ion pairs of metal-2-naphthoate(2-HNph) and tetrabutyl ammonium ($TBA^+$) ion has been studied for the concentration and determination of ultra trace Bi(III), In(III) and Tl(Ⅲ) ions in water samples. The partition coefficients ($K_p$) and the extraction percentages of 2-HNph and the ion pairs to methyl isobutyl ketone (MIBK) were obtained as basic data. After the ion pair $TBA^+$·M$(Nph)_4^-$ was formed in water samples, the analytes were concentrated by the solvent sublation and the elements were determined by GF-AAS. The pH of the sample solution, the amount of the ligand and counter ion added and stirring time were optimized for the efficient formation of the ion pair. The type and amount of optimum surfactant, bubbling time with nitrogen and the type of solvent were investigated for the solvent sublation as well. 10.0 mL of 0.1 M 2-HNph and 2.0 mL of 0.1 M $TBA^+$ were added to a 1.0 L sample solution at pH 5.0. After 2.0 mL of 0.2%(w/v) Triton X-100 was added, the ion pairs were extracted into 20.0 mL MIBK in a flotation cell by bubbling. The analytes were determined by a calibration curve method with measured absorbances in MIBK, and the recovery was 80-120%.

Determination of Ag(Ⅰ) Ion at a Modified Carbon Paste Electrode Containing N,N'-Diphenyl Oxamide

  • Won, Mi-Sook;Yeom, Jeong-Sik;Yoon, Jang-Hee;Jeong, Euh-Duck;Shim, Yoon-Bo
    • Bulletin of the Korean Chemical Society
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    • 제24권7호
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    • pp.948-952
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    • 2003
  • New approach for the determination of Ag(I) ion was performed by using a carbon paste electrode (CPE) containing N,N'-Diphenyl oxamide (DPO) with anodic stripping voltammetry. The CMEs have been prepared by making carbon paste mixtures containing an appropriate amount of DPO salt coated onto graphite particles to analyze trace metal ions via complexation followed by stripping voltammetry. Various experimental parameters affecting the response, such as pH, deposition time, temperature, and electrode composition, were carefully optimized. Using differential pulse anodic stripping voltammetry, the logarithmic linear response range for the Ag(I) ion was 1.0 × $10^{-7}$ - 5.0 × $10^{-9}$ M at the deposition time of 10 min, with the detection limit was 7.0 × $10^{-10}$ M. The detection limit adopted from anodic stripping differential pulse voltammetry was 7.0 × $10^{-10}$ M for silver and the relative standard deviation was ± 3.2% at a 5.0 × $10^{-8}$ M of Ag(I) ion (n = 7). The proposed electrode shows a very good selectivity for Ag(I) in a standard solution containing several metals at optimized conditions.