• Title/Summary/Keyword: Time Determination

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Prediction of the Optimum Conditions for Microwave-Assisted Extraction of the Total Phenolic Content and Antioxidative and Nitrite-scavenging Abilities of Grape Seed (포도씨의 총페놀 성분, 항산화능 및 아질산염소거능에 대한 마이크로웨이브 추출조건 예측)

  • Lee, Eun-Jin;Kim, Jeong-Sook;Kim, Hyun-Ku;Kwon, Joong-Ho
    • Food Science and Preservation
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    • v.18 no.4
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    • pp.546-551
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    • 2011
  • Response surface methodology (RSM) was used for the microwave-assisted extraction (MAE) of the effective components of grape seed, such as its antioxidative and nitrite-scavenging abilities. Microwave power (2,450 MHz, 0-160W), ethanol concentration (0-100%), and MAE time (1-5 min) were used as independent variables (Xi) for the central composite design to yield 16 different MAE conditions. The optimum MAE conditions were predicted for the dependent variables of the extracts, such as the total phenolic content ($Y_1$) antioxidative ability ($Y_2$), and nitrite-scavenging ability ($Y_3$), depending on different microwave powers, ethanol concentrations, and MAE times. The determination coefficients ($R^2$) of the regression equations for the dependent variables ranged from 0.8024 to 0.9498. The maximal values of each dependent variable were predicted at different MAE conditions, as follows: 3.19% total phenolic content at 142.32W, 44.30% ethanol, and 4.36 min, and 1.22 antioxidative ability at 84.44W, 56.60% ethanol, and 3.28 min. More than 99.5% nitrite-scavenging ability was predicted at pH 1.2-3.0, 30.80-106.58W, 49.32-55.18% ethanol, and 3.72-4.58min, respectively. The results indicated that the total phenolic content and anti oxidative ability showed a higher correlation with each other in that they were more influenced by microwave power than by the other variables, while the nitrite-scavenging ability was largely influenced by the ethanol concentration.

Optimization on preparation conditions of beverage using Opuntia ficus-indica stem (손바닥 선인장을 이용한 음료 제조조건의 최적화)

  • Lee, Gee-Dong
    • Food Science and Preservation
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    • v.20 no.4
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    • pp.502-509
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    • 2013
  • This study was conducted in order to monitor the extraction conditions for a gel-state beverage development of the Opuntia ficus-indica stem. Moreover, the organoleptic properties of the beverage prepared by the extract were optimized using the response surface methodology (RSM). The determination coefficient ($R^2$) value for the extraction yield of the stem was 0.95 (p<0.01). The maximum extraction yield was obtained at an extraction temperature of $93.02^{\circ}C$, 123 min of extraction time and 22.57 mL/g of water to sample. The beverage was prepared with the addition of xanthan gum, sugar and persimmon vinegar to the extract with a central composite design. The maximum organoleptic color of the beverage was obtained at 0.38% xanthan gum, 7.91% sugar and 0.76% persimmon vinegar. The maximum organoleptic flavor was obtained at 0.30% xanthan gum, 7.06% sugar and 1.26% persimmon vinegar. The maximum organoleptic taste was obtained at 0.22% xanthan gum, 10.36% sugar and 0.90% persimmon vinegar. The maximum overall palatability (3.92 score) of the gel-state beverage was obtained at 0.35% xanthan gum, 10.83% sugar and 1.21% persimmon vinegar.

A Study on the Policy Implication on the Addiction of Social Media Service User : Focusing on the Proposal of Korean SNS Addiction Index (KSAI) (소셜미디어 사용자의 중독에 관한 정책적 함의 연구 : 한국형 SNS 중독지수(KSAI) 제안을 중심으로)

  • Lee, Sang-Ho
    • Journal of Digital Convergence
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    • v.11 no.1
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    • pp.255-265
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    • 2013
  • This study deals with the policy proposals focusing on the addiction for the rapidly growing social media service (SNS) and its diagnosis. Researcher intends to define the SNS addiction and develops a diagnostic measure, which is a valuable subject. The reason is why the SNS becomes more convenient with prevalence of smart phones and the SNS addiction becomes enough severe to suggest internet addiction policy. Researcher presents the subjects into three parts. Firstly, the SNS addiction variables are derived and validated. Secondly, the path model between the SNS addiction variables is verified and discussed. Thirdly, researcher proposes the diagnostic results and the group comparison. Therefore, the result of this study is that the SNS addiction can be measured by the four elements, which are the failure in stopping the use of the SNS, time tolerance, living disability, withdrawal and anxiety. Researcher verifies the sequential impact of each variable and figures out the SNS addict through the presentation of a realistic measurement for the addiction index and the determination of the level of the addiction. By the above result, the researcher proposes the public relations of the government policy for the sound usage of the SNS and the self management of user. Finally, various proposed in this study will help to prevent juvenile crime, social problems in the future.

A Qualitative Case Study on Rights-Based Social Work Practice in a Residential Facility for People with Intellectual Disabilities (인권관점에 기초한 사회복지실천 경험에 관한 질적 사례연구 - 장애인거주시설의 종사자 경험을 중심으로 -)

  • Kim, Mi-Ok;Kim, Kyung-Hee
    • Korean Journal of Social Welfare
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    • v.63 no.1
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    • pp.29-55
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    • 2011
  • This study aims to understand the experiences of rights-based social work practice in a residential facility for people with intellectual disabilities. A representative residential facility practicing a human rights perspective was selected by recommendation of professional groups. Using a qualitative case study method, data was collected and analysed. In detail, it explores the experiences of rights-based social work practice at both organizational and individual levels respectively, and then discusses ethical dilemmas that arise from workers in the process of rights-based social work practice. According to results at the organizational level, rights-based social work practice of the residential facility began from workers' interests in needs of users with intellectual disabilities. Some trials to apply human rights in social work practice resulted in regulations for people with intellectual disabilities and stepped up organizational culture on human rights perspectives. And, at the individual level, self determination and choice of users with intellectual disabilities were stressed among various forms of human rights. As the results of rights-based social work practice, it appeared to be improved for the participation of the users, workers' human rights sensitivity, and qualities of rights-based activities. However, ethical dilemmas still existed. Hence, rights-based social work practice should understand a process of dynamic interaction between users and workers, which require workers to endeavor continuously. This study is significant in that it explored rights-based social work practice, focusing on field experiences for the first time in Korea, and suggested practical tasks to settle it down in the future.

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Preparation of the Proteus vulgaris Bacterial Electrodes for the Determination of Urea and Their Application (요소 정량을 위한 Proteus vulgaris 박테리아 전극의 개발과 그 응용)

  • Gwon-Shik Ihn;Bong-Weon Kim;Sohn Moo-Jeong;Ihn-Tak Kim
    • Journal of the Korean Chemical Society
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    • v.32 no.4
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    • pp.323-332
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    • 1988
  • The bacteria containing urease convert each molecule of urea into two molecules of ammonia and one molecule of carbon dioxide gas. Bacterial electrodes have been constructed by immobilizing the Proteus vulgaris on an ammonia and a carbon dioxide gas-sensors, and were investigated for the effects of pH, temperature, buffer solution, bacterial amounts and interferences, and life time. NH3-bacterial electrode based on ammonia gas-sensor had linearity in the range of $7.0{\times}10^{-4}\;-\;3.0{\times}10^{-2}$M urea in pH 7.4, 0.05M phosphate buffer at $25^{\circ}C$ with a slope of 116.7 mV/decade. While $CO_{2-}$bacterial electrode based on carbon dioxide gas-sensor bad linearity in the range of $7.0{\times}10^{-4}\;-\;5. 0{\times}10^{-2}$M urea in pH 7.0, 0.1M phosphate buffer at $30^{\circ}C$with a slope of $45.4{\times}45.7mV/decade$. As the clinical application, urea in urine was determined by these devices and this result was compared with spectrophotometric method. Consequently, these electrodes could be used for the analysis of many samples because of simplicity, rapidity and convenience of the experimental procedure.

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Effect of Ultrasonic Pretreatment on Analysis of Potassium Ion in Human Urine Using 15-Crown-5-Anthracene-based Membrane (15-Crown-5-Anthracene 막을 이용한 요 중의 칼륨이온 분석에 미치는 초음파 전처리의 효과)

  • Lee, Ji-Young;Chang, Hye-Young;Bae, Zun-Ung
    • Journal of the Korean Chemical Society
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    • v.47 no.1
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    • pp.13-18
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    • 2003
  • The effect of ultrasonic decomposition was introduced to develop a pretreatment method for the analysis of potassium ion in human urine by potentiometry. N-(4’-benzo-15-crown-5)-anthracene-9-imine, which has a good selectivity coefficient for potassium against ammonium, was used as an ion-selective material for the determination of potassium in urine with relatively high concentration of $NH_4{^+}$. Protenis in urine be removed by 85.1% when the sample acidified with 1.0 M $HNO_3$ was preteated for 100 s by sonication. Potential response of the membrane electrode in the pretreated urine had a slope of 54.6(${\pm}0.2,\;n=5$) mV/decade over the linear range of log $[K^+]$=-5~-1(r=0.9997). When an oxidant, $H_2O_2$, was addwd to the urine sonicated with $HNO_3$, the deproteinization increased 10% more than that in case if only $HNO_3$ and then the maximum ratio of ca. 95% was obtained. Moreover, the Nernstian slope for $K^+$ added to the urinary sample increased to 56.7(${\pm}0.1,\;n=3$) mV/decade. When the calibration curves were measured, the slopes did not vary even after the electrode was successively used 20 times with ultrasonic cleaning. The results showed that an ultrasonic pretreatment method provides simplicity in use, reduced treatment time and improved potentiometric characteristics of the membrane as the method effectively removes ca. 95% of proteins in urine.

Hydrologic and Environmental Assessment of an Infiltration Planter for Roof Runoff Use (지붕 빗물이용을 위하여 개발된 침투화분의 환경·수문학적 평가)

  • Moon, So-Yeon;Choi, Ji-Yeon;Hong, Jung-Sun;Yu, Gi-Gyung;Jeon, Je-Chan;Flores, Precious Eureka D.;Kim, Lee-Hyung
    • Journal of Wetlands Research
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    • v.17 no.4
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    • pp.325-331
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    • 2015
  • Due to urbanization and increase in impervious area, changes in natural water circulation system have become a cause of groundwater recharge reduction, streamflow depletion and other hydrological problems. Therefore, this study developed the infiltration planter techniques applied in an LID facility treating roof stormwater runoff such as, performance of small decentralized retention and infiltration through the reproduction of natural water circulation system and use of landscape for cleaning water. Assessment of an infiltration planter was performed through rainfall monitoring to analyze the water balance and pollutant removal efficiency. Hydrologic assessment of an infiltration planter, showed a delay in time of effluent for roof runoff for about 3 hours and on average, 79% of facilities had a runoff reduction through retention and infiltration. Based on the analysis, pollutant removal efficiency generated in the catchment area showed an average of 97% for the particulate matter, 94% for the organic matter and 86-96% and 92-93% for the nutrients and heavy metals were treated, respectively. Comparative results with other LID facilities were made. For this study, facilities compared the SA/CA to high pollutant removal efficiency for the determination to of the effectiveness of the facility when applied in an urban area.

Free-air anomaly from Airborne Gravity Surveying (항공중력측정에 의한 프리에어 이상 산출)

  • Lee, Ji-Sun;Kwon, Jay-Hyoun;Lee, Bo-Mi;Hong, Chang-Ki
    • Journal of the Korean Society of Surveying, Geodesy, Photogrammetry and Cartography
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    • v.27 no.2
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    • pp.139-147
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    • 2009
  • The gravity data collected and reserved in Korea is seriously biased in its distribution. That is, only the west-southern part of the peninsula including Chungcheong and Jeonla area has dense distribution while only a part is covered in Gyoungsang area. Especially, the low density of the gravity data in mountainous area basically limits the accuracy of the gravimetric geoid in Korea. As one of the solution to overcome the problem, an airborne gravity survey were conducted from Dec. 2008 $\sim$ Jan. 2009. In this study, free-air gravity anomaly derived from the airborne gravity data which has consistent quality are presented. The data processing for the airborne gravity is composed of several corrections of errors such as errors from gravity measurement, errors from flight dynamics, errors from GPS, and errors from time synchronization. We presented detailed explanations on the data processing with the final cross-over results. The free-air anomaly from airborne gravity finally shows the cross-over accuracy of 2.21mGal which reflects the precision of each track is 1.56mGal. It is expected that the result from this study will play a role as input data in precision geoid determination with ground and ship-borne gravity data after appropriate fusion process.

Kinetics of Thermal Inactivation of Peroxidases and Polyphenol Oxidase in Pineapple (Ananas comosus)

  • Lee, Ting Hun;Chua, Lee Suan;Tan, Eddie Ti Tjih;Yeong, Christina;Lim, Chew Ching;Ooi, Siew Yin;Aziz, Ramlan bin Abdul;Aziz, Azila binti;Sarmidi, Mohd Roji bin
    • Food Science and Biotechnology
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    • v.18 no.3
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    • pp.661-666
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    • 2009
  • The heat tolerance and the inactivation kinetics of peroxidase (POD) and polyphenol oxidase (PPO) in pineapples (Ananas comosus) were studied in the temperature range $45-95^{\circ}C$. The kinetic parameters, such as deactivation rate constant (k), activation energy ($E_a$), and decimal reduction rate (D) of the thermal inactivation process, were determined. POD in pineapples showed biphasic inactivation behavior at temperatures range $45-75^{\circ}C$ but was monophasic at $85-95^{\circ}C$. This indicate that POD has 2 isozymes, namely heat labile and heat resistant, with $E_a$ of 68.79 and 93.23 kJ/mol, respectively. On the other hand, the heat denaturation of pineapple PPO could be described as simple monophasic first-order behavior with $E_a$ of 80.15 kJ/mol. Thus, the results of this study is useful in blanching technology where it shows a shortened time with higher temperature can be applied. The determination of the heat tolerance and inactivation POD and PPO, at different temperature range as done in the present work, was very important to improve the blanching process. This also will help to optimize the pineapple canning process which is one of the most important food industries in many tropical regions.

Capacity determination for a rainfall harvesting unit using an optimization method (최적화 기법을 이용한 빗물이용시설의 저류 용량 결정)

  • Jin, Youngkyu;Kang, Taeuk;Lee, Sangho;Jeong, Taekmun
    • Journal of Korea Water Resources Association
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    • v.53 no.9
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    • pp.681-690
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    • 2020
  • Generally, the design capacity of the rainwater harvesting unit is determined by trial and error method that is repeatedly calculating various analysis scenarios with capacity, reliability, and rainwater utilization ratio, etc. This method not only takes a lot of time to analyze but also involves a lot of calculations, so analysis errors may occur. In order to solve the problem, this study suggested a way to directly determine the minimum capacity to meet arbitrary target reliabilities using the global optimization method. The method was implemented by simulation model with particle swarm optimization (PSO) algorithms using Python language. The pyswarm that is provided as an open-source of python was used as optimization method, that can explore global optimum, and consider constraints. In this study, the developed program was applied to the design data for the rainwater harvesting constructed in Cheongna district 1 in Incheon to verify the efficiency, stability, and accuracy of the analysis. The method of determining the capacity of the rainwater harvesting presented in this study is considered to be of practical value because it can improve the current level of analytical technology.