• Journal of the Korean institute of surface engineering
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• v.44 no.5
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• pp.196-200
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• 2011

The Ni-based superalloy, Inconel 713, was oxidized at $800{\sim}1100^{\circ}C$ for 50 and 100 hours in air. It displayed excellent oxidation resistance, forming a few micrometer-thick scales. The major scale was ${\alpha}-Al_2O_3$. Other scales formed were $TiO_2$, $NiAl_2O_4$ and $Cr_2O_3$. Generally, uniform oxidation occurred over the alloy surface, resulting in the formation of ${\alpha}-Al_2O_3$ with and without $Cr_2O_3$. Other oxides such as $TiO_2$ and $NiAl_2O_4$ sometimes also formed. Locally, nodular oxidation occurred at the nodules that consisted of diverse alloying elements. The scales were adherent at $800^{\circ}C$. However, they spalled a little at $900{\sim}1100^{\circ}C$.

• Earthquakes and Structures
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• v.23 no.5
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• pp.431-444
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• 2022

The unique thermomechanical properties of shape memory alloys (SMAs) make it a versatile material for strengthening and repairing structures. In particular, several research studies have already demonstrated the effectiveness of using the heat activated shape memory effect of nickel-titanium (Ni-Ti) based SMAs to actively confine concrete members. Despite the proven effectiveness and wide commercial availability of Ni-Ti SMAs, however, their high cost remains a major obstacle for applications in real structural engineering projects. In this study, the shape memory effect of a new, much more economical iron-based SMA (Fe-SMA) is characterized and the compressive behavior of concrete confined with Fe-SMA strips is investigated. Tests showed the Fe-SMA strips used in this study are capable of developing high levels of recovery stress and can be easily formed into hoops to provide effective active and passive confining pressure to concrete members. Compared to concrete cylinders confined with conventional carbon fiber-reinforced polymer (CFRP) composites, Fe-SMA confinement yielded significantly higher compressive deformation capacity and residual strength. Overall, the compressive behavior of Fe-SMA confined concrete was comparable to that of Ni-Ti SMA confined concrete. This study clearly shows the potential for Fe-SMA as a robust and cost-effective strengthening solution for concrete structures and opens possibilities for more practical applications.

• Transactions of the Korean Society of Automotive Engineers
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• v.2 no.2
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• pp.95-102
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• 1994

Aluminum sheet application to automobile body panels has now become an important objective to meet the requirements of automobile weight reduction. As the Mg content in Al-Mg based alloys increased up to 7.19%, the strength and elongation increased. For instance. Al-7.19Mg alloy had a high strength of 305MPa and a high elongation of 35%. A study was also made to investigate the interrelation between grain size and tensile properties with varying the contents of Mg, Ti and Zr elements and annealing conditions. The yield stress decreased as the grain size increased, which increased the uniform elongation. The strain hardening exponents n increased as the Mg content increased, which depended on the increasing difficulties of the cross slip of dislocation.

• Journal of Welding and Joining
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• v.15 no.5
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• pp.46-55
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• 1997

This study has evaluated the liquation cracking behavior in the heat affected zone of several Ni base superalloys (Incoloy 825, Inconel 718 and Inconel 600). 304 and 310S austenitic stainless steels were also included for comparison. In addition, the mechanism of liquation cracking in the HAZ was postulated based on the extensive microstructural examinations with SEM, EDAX and TEM. The liquation cracking resistance of Ni base alloys was found to be far inferior to that of austenitic stainless steels. The liquation cracking of Incoloy 825 and Inconel 718 was believed to be closely related with the Laves-austenite(Ti rich in 825 and Nb rich in 718) and MC-austenitic eutectic phases formed along the grain boundaries by constitutional liquation and incipient melting under rapid welding thermal contraction. Further, liquation cracking resistance of the HAZ was dependent not only upon the type and amount of low melting phases but also on the grain size.

• Smart Structures and Systems
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• v.30 no.3
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• pp.255-261
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• 2022

When no extensometer is available in a generic tensile-compression test carried out by a universal testing machine (for instance the model BIONIX from Material Testing Systems (MTS)), the test results only provide the relative displacement between the machine grips. The test does not provide any information on the local behaviour of the material. This contribution presents the potential of an application of Digital Image Correlation (DIC) toward the reconstruction of the behaviour along the specimen. In particular, the authors test a Ni-Ti shape memory alloys (SMA) specimen with emphasis on the coupling of the two measurement techniques.

• Laser Solutions
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• v.18 no.3
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• pp.1-5
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• 2015

A 3D printer based on laser powder deposition (LPD), also known as DED (direct energy deposition), has been developed for fabricating metal parts. The printer uses a ytterbium fiber laser (1070nm, 1kW) and is equipped with an Ar purge chamber, a three-dimensional translation stage and a powder feeding system composed of a powder chamber and delivery nozzles. To demonstrate the performance of the printer, a tapered cylinder of 320mm in height has been fabricated successfully using Ti-6Al-4V powders. The process parameters including the laser output power, the scan speed, and the powder feeding rate have been optimized. A 3D printed test specimen shows mechanical properties (yield strength, ultimate tensile strength, and elongation) exceeding the criteria to employed in a variety of Ti alloy applications.

• Proceedings of the Korean Society for Technology of Plasticity Conference
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• 2009.05a
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• pp.158-163
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• 2009

Titanium alloy sheets have excellent specific strength and corrosion resistance as well as good performance at high temperature. Recently, titanium alloys are widely employed not only aerospace parts but also bio prothesis and motorcycle. However, due to the low formability and large spring back at room temperature, titanium alloy sheets were usually formed by slow forming or hot forming with heating die and specimen. In the sheet metal forming area, FE simulation technique to optimize forming process is widely used. To achieve high accuracy FE simulation results, Identification of material properties and deformation characteristic such as yield function are very important. In this study, uniaxial tensile and biaxial tensile test of Ti-6Al-4V alloy sheet with thickness of 1.0mm were performed at elevated temperature of 873k. Biaxial tensile tests with cruciform specimen were performed until the specimen was breakdown to characterize the yield locus of Ti-6Al-4V alloy sheet. The experimental results for yield locus are compared with the theoretical predictions based on Von Mises, Hill, Logan-Hosford, and Balat's model. Among these Logan-Hosford's yield criterion well predicts the experimental results.

• Journal of the Korean Ceramic Society
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• v.45 no.1
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• pp.1-29
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• 2008

In last two decades, an impressive progress has been recorded in terms of developing new materials or refining existing material composition/microstructure in order to obtain better performance in biomedical applications. The success of such efforts clearly demands better understanding of various concepts, e.g. biocompatibility, host response, cell-biomaterial interaction. In this article, we review the fundamental understanding that is required with respect to biomaterials development, as well as various materials and their properties, which are relevant in applications, such as hard tissue replacement. A major emphasize has been placed to present various design aspects, in terms of materials processing, of ceramics and polymer based biocomposites, Among the bioceramic composites, the research results obtained with Hydroxyapatite (HAp)-based biomaterials with metallic (Ti) or ceramic (Mullite) reinforcements as well as $SiO_2-MgO-Al_2O_3-K_2O-B_2O_3-F$ glass ceramics and stabilized $ZrO_2$ based bioinert ceramics are summarized. The physical as well as tribological properties of Polyethylene (PE) based hybrid biocomposites are discussed to illustrate the concept on how can the physical/wear properties be enhanced along with biocompatibility due to combined addition of bioinert and bioactive ceramic to a bioinert polymeric matrix. The tribological and corrosion properties of some important orthopedic metallic alloys based on Ti or Co-Cr-Mo are also illustrated. At the close, the future perspective on orthopedic biomaterials development and some unresolved issues are presented.

• Journal of the Korean Society for Heat Treatment
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• v.17 no.1
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• pp.17-22
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• 2004

In the present study, newly developed spark plasma sintering(SPS) technique was introduced to refine the grain size of ${\gamma}$-based TiAl intermetallic compounds. Ti-46Al-1.5Mo and Ti-46Al-1.5Mo-0.2C(at%) prealloyed powders were produced by mechanical milling(MM) in high-energy attritor. The mechanically milled powders were characterized by XRD and SEM for the microstructural evolution as a function of milling time. And then, the MMed powders were sintered by both spark plasma sintering and hot pressing in vacuum (HP). After the sintering process, MM-SPSed specimens were heat-treated in a vacuum furnace (SPS-VHT) and in the SPS equipment(MM-SPS) for microstructural control. It was found from microstrutural observation that the microstructure consisting of equiaxed ${\gamma}$-TiAl with a few hundred nanometer in average size and ${\alpha}_2-Ti_3Al$ particles were formed after both sintering processes. It was also revealed from hardness test and three-point bending test that the effect of grain refinement on the hardness and bending strength is much higher than that of carbon addition. The fully lamellar microstructures, which is less than $80{\mu}m$ in average grain size was obtained by SPS-VHT process, and the fully lamellar microstructure which is less than $100{\mu}m$ in average grain size was obtained by MM-SPS for a relatively shorter heat-treatment time.

• Korean Journal of Materials Research
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• v.23 no.7
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• pp.353-358
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• 2013

To improve coating ability and the life of the coating, Ti based composite materials with hydroxyapatite(HA) should be developed. The raw materials of Ti-26wt%, Nb-1wt%, and Si with 10wt% HA were mixed for 24 h by a mixing machine and milled for 1 h to 6 h by planetary mechanical ball milling. Ti-26%Nb-1%Si-(10%HA) composites, composed of nontoxic elements, were fabricated successfully by spark plasma sintering(SPS) at $1000^{\circ}C$ under 70MPa. The relative density of the sintered Ti-Nb-Si-HA composites using the 24 h mixed powder, and the 6 h milled powder, was 91% and 97 %, respectively. The effects of HA contents and milling time on microstructure and mechanical properties were investigated by SEM and hardness tester, respectively. The Vickers hardness of the composites increased with increasing milling time and higher HA content. The Young's modulus of the sintered Ti-26%Nb-1%Si-10%HA composite using the 6 h-milled powder was 55.6 GPa, as obtained by compression test. Corrosion resistance of the Ti-26wt%Nb-1wt%Si composite was increased by milling and by the addition of 10wt%HA. Wear resistance was improved with increasing milling time. Biocompatibility of the Ti-Nb-Si alloys was improved by the addition of HA.