• Proceedings of the Korean Powder Metallurgy Institute Conference
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• 2006.09a
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• pp.113-113
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• 2006

• Proceedings of the Korean Powder Metallurgy Institute Conference
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• 2005.11a
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• pp.41-42
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• 2005

• Structural Engineering and Mechanics
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• v.61 no.4
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• pp.519-526
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• 2017

In the present paper, the effects of cutting parameters and coating material on the performances of cutting tools in turning of AISI 52100 steel are discussed experimentally. A comparative study was carried out between uncoated and coated (with TiCN-TiN coating layer) cermet tools. The substrate composition and the geometry of the inserts compared were the same. A mathematical model was developed based on the Response Surface Methodology (RSM). ANOVA method was used to quantify the effect of cutting parameters on the machining surface quality and the cutting forces. The results show that feed rate has the most effect on surface quality. However, cutting depth has the significant effect on the cutting force components. The effect of coating layers on the surface quality was also studied. A lower surface roughness was observed when using PVD (TiCN-TiN) coated insert. A second order regression model was developed and a good accuracy was obtained with correlation coefficients in the range of 95% to 97%.

• Journal of Biomedical Engineering Research
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• v.25 no.2
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• pp.157-163
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• 2004

Nitrogen ion implantation and ion plating techniques were applied for improvement of the wear resistance of metallic implant materials. In this work, the wear dissolution behaviour of a nitrogen ion implanted super stainless steel (S.S.S, 22Cr-20Ni-6Mo-0.25N) was compared with those of S.S.S, 316L SS and TiN coated 316L SS. The amounts of Cr and Ni ions worn-out from the specimens were Investigated using an electrothermal atomic absorption spectrometry. Furthermore, the Ti(Grade 2) disks were coated with TiN, ZrN and TiCN by use of low temperature arc vapor deposition and the wear resistance of the coating layers was compared with that of titanium. The chemical compositions of the nitrogen ion implanted and nitride coated layers were examined with a scanting auger electron spectroscopy. It wat observed that the metal ions released from the nitrogen ion implanted S.S.S surface were significantly reduced. From the results obtained, it was shown that the nitrogen ion implanted zone obtained with 100 KeV ion energy was easily removed within 200,000 revolutions from a wear dissolution testing under a similar load condition when applied to artificial hip joint. The remarkable improvement in wear resistance weir confirmed by the nitrides coated Ti materials and the wear properties differ greatly according to the chemical composition of the coating layers. for specimens with the same coating thickness of about 3$\mu\textrm{m}$, TiCN coated Ti showed the highest wear resistance. However, after removing the coating layers, the wear rates of all nitrides coated Ti reverted to their normal rates of below 10,000 revolutions from Ti-disk-on-disk wear testing under the same load condition. From the results obtained, it is suggested that the insufficient depth of the 100 Kel N$\^$＋/ ion implanted zone and of the nitrides coated layers of 3$\mu\textrm{m}$ are subject to restriction when used as frictional parts of load bearing implants.

• Korean Journal of Materials Research
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• v.12 no.8
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• pp.676-681
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• 2002

Microstructure, mechanical properties, and oxidation resistance of TiAIN thin films deposited on quenched and tempered STD61 tool steel by arc ion plating were studied using XRD, XPS and micro-balance. The TiAIN film was grown with the (200) orientation. The grain size of TiAIN thin film decreased with increasing Al contents, while chemical binding energy increased with Al contents. When hard coating films were oxidized at $850^{\circ}C$ in air, oxidation resistance of both TiN and TiCN films became relatively lower since the surface of films formed non-protective film such as $TiO_2$. However, oxidation resistance of TiAIN film was excellent because its surface formed protective layer such as $_A12$$O_3$ and $_Al2$$Ti_{7}$$O_{15}$, which suppressed oxygen intrusion.

• Journal of the Korean Society for Precision Engineering
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• v.15 no.8
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• pp.33-38
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• 1998

TiYN coated high speed steel tools have been developed and their tool lifes were assessed. First yttrium alloyed titanium target was manufactured, then using the arc ion plating(AIP) technique TiYN coating was deposited onto high speed steel substrate. Three kinds of varying thickness of TiYN coated tools were prepared. Cutting tests were carried out with theses tools and for comparison with the commercially available uncoated, TiN, TiCN and TiAlN coated tools. During the cutting tests flank wear width vs. cutting time was measured. It has been revealed that the newly developed TiYN coated tools show superior tool life characteristics to others.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2000.05a
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• pp.779-782
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• 2000

This paper aimes to clarify the effects of tool geometry on the tool life in machining of STS 304. The main conclusions obtained were as follows. The lift of TiN coated cermet tool was the longest, exhibiting shorter life in the order of P2O, cermet, TiCN coated carbide and TiAIN coated carbide tools. S-type tool showed the best performance of all tools used in this tests due to preventing the boundary wear of the side cutting edge.

• Journal of the Korean Society for Precision Engineering
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• v.18 no.4
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• pp.182-189
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• 2001

TiCN based submicron cermet and similar ISO grad of the conventional cermets with TiCN of different particle size were produced by PM process, and their microstructure, mechanical properties and cutting performance were compared. The microstructure of submicron cermet was more homogeneous and showed much finer microstructure, resulting in better hardness and fracture toughness. The submicron cermet tools achieved excellent cutting performance such as wear resistance and toughness in comparison with two grades of the conventional cermets in millimg test. The relationship between microstrucure, mechanical properties and cutting performance of these cermet tools was discussed. The submicron cermet tools revealed for their potential to wide application range and interrupt cutting because of their superior wear resistance and toughness combinations.

• Proceedings of the Korean Powder Metallurgy Institute Conference
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• 2006.09b
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• pp.1037-1038
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• 2006

The increasing demand of PM parts for automobile and aerospace applications has caused a strong development of the aluminium based metal matrix composites (MMCs).Aluminium alloys are one of most widely used materials as matrix in MMCs, both in research and development as well as in industrial applications. In the present work, the influence of the ceramic reinforcement addition to a 2xxx series aluminium alloy is studied. Several percentages of TiCN have been added to the Al-Cu alloy using PM techniques, in order to analyze its influence on the liquid phase sintering process and on the final properties of the material.

• Bulletin of the Korean Chemical Society
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• v.18 no.6
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• pp.567-573
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• 1997

Photoinduced electron transfer from the charge-transfer excited states of Ru(tpy)(bpy(COOH)₂)$CN^+$, Ru(tpy)(bpy(COOH)₂)$Cl^+$, Ru(tpy)(bpy(COOH)₂)H₂+O², and Ru(tpy)(bqu(COOH)₂)$Cl^+$ to the conduction band of TiO₂ has been studied through photoelectrochemical methods. Ru(tpy)(bpy(COOH)₂)$CN^+$ produced the highest current density and open-circuit photovoltage, whereas Ru(tpy)(bqy(COOH)₂)$Cl^+$ produced the lowest values. A potential barrier was employed to explain the experimental result that the rate of the electron transfer increases with increasing the energy difference between the donor and acceptor. A sensitizer with a high current density yielded a high photovoltage and a high conversion efficiency. The reduction rate of the oxidized sensitizer decreased with the increases in the reduction potential of the sensitizer, resulting in a poor stability of a photoelectrochemical cell.