• Journal of the Korean institute of surface engineering
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• v.54 no.6
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• pp.331-339
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• 2021

Environmental barrier coatings(EBCs) are applied to the SiC/SiC ceramic matrix composites(CMCs) in order to protect CMCs from being corroded with water vapor by combustion gas in gas turbine engines. Ytterbium silicates, such as ytterbium monosilicate and ytterbium disilicate, are ones of the candidate materials for EBCs due to their excellent resistance to water vapor corrosion as well as thermal-expansion match with SiC. In this study, ytterbium silicates are fabricated with 2-step solid-state synthesis targeting ytterbium disilicate. After synthesizing ytterbium monosilicate, the mixtures of ytterbium monosilicate and SiO₂ are heat-treated and densified by using pressureless sintering or hot pressing with a variety of heating conditions. The phase formation, thermal expansion, and oxidation behavior are examined with fabricated specimens. The final densified bodies are found to be composites between ytterbium monosilicate and ytterbium disilicate with different ratios, which results in 4.43 to 6.72×10^-6/K range of coefficients of thermal expansion. The probability of these ytterbium silicates for EBC applications is also discussed.

• Journal of Sensor Science and Technology
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• v.27 no.5
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• pp.300-305
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• 2018

The uncooled microbolometer thermal sensor for low cost and mass volume was designed to target the new infrared market that includes smart device, automotive, energy management, and so on. The microbolometer sensor features 80x60 pixels low-resolution format and enables the use of wafer-level vacuum packaging (WLVP) technology. Read-out IC (ROIC) implements infrared signal detection and offset correction for fixed pattern noise (FPN) using an internal digital to analog convertor (DAC) value control function. A reliable WLVP thermal sensor was obtained with the design of lid wafer, the formation of Au80%wtSn20% eutectic solder, outgassing control and wafer to wafer bonding condition. The measurement of thermal conductance enables us to inspect the internal atmosphere condition of WLVP microbolometer sensor. The difference between the measurement value and design one is $3.6{\times}10-9$ [W/K] which indicates that thermal loss is mainly on account of floating legs. The mean time to failure (MTTF) of a WLVP thermal sensor is estimated to be about 10.2 years with a confidence level of 95 %. Reliability tests such as high temperature/low temperature, bump, vibration, etc. were also conducted. Devices were found to work properly after accelerated stress tests. A thermal camera with visible camera was developed. The thermal camera is available for non-contact temperature measurement providing an image that merged the thermal image and the visible image.

• Journal of the Korean institute of surface engineering
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• v.50 no.6
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• pp.460-464
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• 2017

As increasing thermal efficiency of the gas turbine, the performance improvement of thermal barrier coatings is also becoming important. Ytrria stabilized zirconia(YSZ) is the most popular materials for ceramic top coating because of its low thermal conductivity. In order to enhance the performance of thermal barrier coatings for hot sections in the gas turbine, suspension plasma spraying was developed in order to feed nano-sized powders. YSZ coatings formed by suspension plasma spraying showed better performance than YSZ coatings due to its exclusive microstructure. In this research, two YSZ coatings were deposited by suspension vacuum plasma spraying at 400 mbar and 250 mbar. Microstructures of YSZ coatings were analyzed by scanning electron image(SEM) on each spraying conditions, respectively. Crystalline structure transformation was not detected by X-ray diffraction. Thermal conductivity of suspension vacuum plasma sprayed YSZ coatings were measured by laser flash analysis. Thermal conductivity of suspension vacuum plasma sprayed YSZ coatings containing horizontally oriented nano-sized pores and vertical cracks showed $0.6-1.0W/m{\cdot}K$, similar to thermal conductivity of YSZ coatings formed by atmospheric plasma spraying.

• Economic and Environmental Geology
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• v.22 no.4
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• pp.371-379
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• 1989

Peak or near-peak metamorphic temperatures and pressures for Seosan area could be estimated from major element method. Temperatures calculated from garnet-biotite geothermoneter(Ferry and Spear, 1978; Ganguly and Saxena, 1984) are $620{\pm}40^{\circ}C$ and $520{\pm}20^{\circ}C$ for Seosan and Daesan Formation respectively. Presures derived from garnet-plagiciase-$Al_2Si_O_2$-quartz geobarometer(Newton and Haselton, 1981; Ganguly and Saxena, 1984)suggest 5-6kb for both of Seosan and Daesan Formation. These results suggest that under isobaric, Seosan Formation underwent relatively high temperature metamorphism compared with Daesan Formation. Chemical zonations of garnet for major elements such as Fe, Mg, and Mn in Seosan and Dasan Formation show different patterns each other probably caused by different thermal history.

• Korean Chemical Engineering Research
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• v.43 no.1
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• pp.125-128
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• 2005

Oil formation rate, composition of crude oil and formation of side products such as ${\alpha}-methyl$ styrene, ethyl benzene, benzene, toluene, dimer and trimer on thermal degradation of polystyrene were affected by various factors. Especially, formation of organic residue formed during reaction gave an important influence on formation of oil and composition of crude oil. Also, composition of formed crude oil showed a significant difference on reaction time. These results were caused by organic residue and carbonized solid formed during continuous reaction. Increase of residue and carbonized solid gave a decrease of yield of styrene and an increase of formation of ${\alpha}-methyl$ styrene, ethyl benzene, benzene, toluene. New reaction system was proposed for continuous operation at the thermal degradation of polystyrene.

• Proceedings of the Korean Nuclear Society Conference
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• 2004.10a
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• pp.987-988
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• 2004

• Journal of the Korean Ceramic Society
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• v.33 no.12
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• pp.1339-1346
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• 1996

• Proceedings of the Korean Vacuum Society Conference
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• 1995.06a
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• pp.37-37
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• 1995

• Proceedings of the Korean Fiber Society Conference
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• 2001.04a
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• pp.43-46
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• 2001

• Proceedings of the Korean Vacuum Society Conference
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• 2001.07a
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• pp.74-74
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• 2001