• Title/Summary/Keyword: Thermal Treatment

검색결과 2,711건 처리시간 0.033초

Thermal and mechanical properties of C/SiC composites fabricated by liquid silicon infiltration with nitric acid surface-treated carbon fibers

  • Choi, Jae Hyung;Kim, Seyoung;Kim, Soo-hyun;Han, In-sub;Seong, Young-hoon;Bang, Hyung Joon
    • Journal of Ceramic Processing Research
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    • 제20권1호
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    • pp.48-53
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    • 2019
  • Carbon fiber reinforced SiC composites (C/SiC) have high-temperature stability and excellent thermal shock resistance, and are currently being applied in extreme environments, for example, as aerospace propulsion parts or in high-performance brake systems. However, their low thermal conductivity, compared to metallic materials, are an obstacle to energy efficiency improvements via utilization of regenerative cooling systems. In order to solve this problem, the present study investigated the bonding strength between carbon fiber and matrix material within ceramic matrix composite (CMC) materials, demonstrating the relation between the microstructure and bonding, and showing that the mechanical properties and thermal conductivity may be improved by treatment of the carbon fibers. When fiber surface was treated with a nitric acid solution, the observed segment crack areas within the subsequently generated CMC increased from 6 to 10%; moreover, it was possible to enhance the thermal conductivity from 10.5 to 14 W/m·K, via the same approach. However, fiber surface treatment tends to cause mechanical damage of the final composite material by fiber etching.

Al-Mg-Si 합금에서 Cu 첨가와 자연시효 열처리가 열확산도에 미치는 영향 (Effect of Additional Cu and Natural Aging Treatment on Thermal Diffusivity in the Al-Mg-Si Alloy)

  • 김유미;최세원
    • 한국주조공학회지
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    • 제41권6호
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    • pp.528-534
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    • 2021
  • 본 연구는 Al-Mg-Si 합금에서 Cu가 첨가 후 자연시효와 인공시효에 따른 제2상 석출 반응이 합금의 열확산도 및 경도에 미치는 영향을 연구하였다. 연구에 사용된 Al-0.4Mg-0.2Si 합금과 Cu를 0.6 wt%, 1.0wt% 추가한 Al-Mg-Si-Cu 합금을 각각 중력 주조로 제작하고 열확산도 경도를 측정하고 석출 반응을 확인하기 위해 열량 분석을 실시 하였다. Al-Mg-Si 합금에 첨가된 Cu는 Q'상 및 θ'상과 같은 강화상 형성에 참여하여 합금의 경도와 고온 열확산도를 향상시켰다. 한편, 자연시효 시간 증가는 Al-Mg-Si-Cu 합금의 열확산도에는 큰 영향을 미치지 않았으나, 경도를 하락시키는 것으로 확인되었다.

질화탄소 표면층 및 열처리가 탄소 나노튜브 미세팁의 전계방출 및 장시간 안정성에 미치는 영향 (Effects of Carbon Nitride Surface Layers and Thermal Treatment on Field-Emission and Long-Term Stability of Carbon Nanotube Micro-Tips)

  • 노영록;김종필;박진석
    • 반도체디스플레이기술학회지
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    • 제9권1호
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    • pp.41-47
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    • 2010
  • The effects of thermal treatment on CNTs, which were coated with a-$CN_x$ thin film, were investigated and related to variations of chemical bonding and morphologies of CNTs and also properties of field emission induced by thermal treatment. CNTs were directly grown on nano-sized conical-type tungsten tips via the inductively coupled plasma-chemical vapor deposition (ICP-CVD) system, and a-$CN_x$ films were coated on the CNTs using an RF magnetron sputtering system. Thermal treatment on a-$CN_x$ coated CNT-emitters was performed using a rapid thermal annealing (RTA) system by varying temperature ($300-700^{\circ}C$). Morphologies and microstructures of a-$CN_x$/CNTs hetero-structured emitters were analyzed by FESEM and HRTEM. Chemical composition and atomic bonding structures were analyzed by EDX, Raman spectroscopy, and XPS. The field emission properties of the a-$CN_x$/CNTs hetero-structured emitters were measured using a high vacuum (below $10^{-7}$ Torr) field-emission measurement system. For characterization of emission stability, the fluctuation and degradation of the emission current were monitored in terms of operation time. The results were compared with a-$CN_x$ coated CNT-emitters that were not thermally heated as well as with the conventional non-coated CNT-emitters.

Box-Behnken 및 반응표면 분석법을 이용한 음식물류 폐수 부상 스컴의 혐기성 소화를 위한 열-알칼리 전처리 최적화 (Optimization of Thermal-alkaline Pre-treatment for Anaerobic Digestion of Flotation Scum in Food Waste Leachate Using Box-Behnken Design and Response Surface Methodology)

  • 이동영;최재민;김정광;한선기;이채영
    • 상하수도학회지
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    • 제29권2호
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    • pp.183-192
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    • 2015
  • Response surface methodology (RSM) based on a Box-Behnken Design (BBD) was applied to optimize the thermal-alkaline pre-treatment operating conditions for anaerobic digestion of flotation scum in food waste leachate. Three independent variables such as thermal temperature, NaOH concentration and reaction time were evaluated. The maximum methane production of 369.2 mL $CH_4/g$ VS was estimated under the optimum conditions at $62.0^{\circ}C$, 10.1% NaOH and 35.4 min reaction time. A confirmation test of the predicted optimum conditions verified the validity of the BBD with RSM. The analysis of variance indicated that methane production was more sensitive to both NaOH concentration and thermal temperature than reaction time. Thermal-alkaline pretreatment enhanced the improvement of 40% in methane production compared to the control experiment due to the effective hydrolysis and/or solubilization of organic matters. The fractions with molecular weight cut-off of scum in food waste leachate were conducted before and after pre-treatment to estimate the behaviors of organic matters. The experiment results found that thermal-alkaline pre-treatment could reduce the organic matters more than 10kD with increase the organic matters less than 1kD.

잉여슬러지의 열적가용화를 통한 가용화 및 혐기성소화 생분해도 향상 (Enhancement of Anaerobic Biodegradability and Solubilization by Thermal Pre-treatment of Waste Activated Sludge)

  • 정성엽;정석영;장순웅
    • 신재생에너지
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    • 제10권1호
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    • pp.20-29
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    • 2014
  • The present study investigated the effects of thermal pre-treatment on the enhancement of anaerobic biodegradability of waste activated sludge at varied TS concentration levels. The activated sludges were thermally oxidized for 30 minutes at $80{\sim}200^{\circ}C$ with varied TS concentrations (2%, 4% and 6%). and then, sludge characteristics, solubilization efficiency and methane production yield of thermally pre-treated sludges were analyzed. The higher the temperature in the thermal pre-treatment, the higher the concentration levels of dissolved matters such as $SCOD_{Cr}$, $NH_4{^+}$ and VFAs, which indicates that the thermal pre-treatment facilitates the hydrolysis and acid fermentation. Furthermore, the solubilization efficiency was increased in proportion to the temperature rise at all TS concentrations and was reached at 68.9%, 55.6% and 53.1%, respectively, at $200^{\circ}C$. In the BMP test of the pre-treated sludges, higher methane production yields were observed as 0.313. 0.314 and $0.299m^3\;CH_4/kg\;VS_{add}$ at the condition of TS 2% ($160^{\circ}C$), 4% ($160^{\circ}C$) and 6% ($180^{\circ}C$), respectively, and degradation rate was increased by 84%, 79% and 65% compared with non-pretreated waste activated sludge. These findings suggest the effectiveness of thermal pre-treatment of waste activated sludge for anaerobic biodegradable process.

열확산 프로세스에 의한 초전도 벌크 합성 (Fabrication of the Bulk Superconductor by Thermal Diffusion Process)

  • 이상헌
    • 한국전기전자재료학회논문지
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    • 제34권6호
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    • pp.461-465
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    • 2021
  • A diffusion heat treatment process for YBa2Cu3O7-y bulk superconductor in a Gd2O3 powder was attempted. As a result of measuring the critical temperature of the superconducting bulk, there was no change in the superconducting transition temperature as the Gd particles diffused into the YBa2Cu3O7-y lattice, resulting in dense microstructure. As a result of measuring the critical current, the critical current density (Jc) of the superconducting bulk having treated by the Gd thermal diffusion treatment at 0 T increased to 3×104 A/cm2 at 0 T, which was higher than that of the superconducting bulk without thermal diffusion treatment. The surface magnetic force of the superconducting bulk with Gd thermal diffusion treatment was observed at the center of the superconducting bulk with the maximum trapped magnetic force (Hmax) of 1.51 kG. This result means that the Gd thermal diffusion treatment contributes to improving the critical current density Jc of YBa2Cu3O7-y, and it is believed that Gd particles migrating into the superconducting bulk through thermal diffusion either fill the surface pores of YBa2Cu3O7-y superconductors or act as a flux pinning center.

Effects of Thermal Treatment on the Characteristics of Spiral Inductors on Bragg Reflectors

  • Mai, Linh;Lee, Jae-Young;Le, Minh-Tuan;Pham, Van-Su;Yoon, Gi-Wan
    • Journal of information and communication convergence engineering
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    • 제4권4호
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    • pp.155-157
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    • 2006
  • This paper presents the thermal technique to improve characteristic of planar spiral inductors. The spiral inductors were fabricated on silicon dioxide/silicon (SiO2/Si) wafer. The thermal treatment was done by annealing processes. The measure results showed a considerable improvement of return loss (Sl1). This thermal treatment seems very promising for enhancing spiral inductors based RF IC's.

Thermal Stability of Hydrogen Doped AZO Thin Films Prepared by r.f. Magnetron Sputtering

  • 박용섭;이수호;김중규;하종찬;홍병유;이준신;이재형
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2013년도 제44회 동계 정기학술대회 초록집
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    • pp.699-700
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    • 2013
  • Aluminum and hydrogen doped zinc oxide (AZHO) films were prepared by r.f. magnetron sputtering. The structural, electrical, and optical properties of the AHZO films were investigated in terms of the annealing conditions to study the thermal stability. The XRD measurements revealed that the degree of c-axis orientation was decreased and the crystallintiy of the films was deteriorated by the heat treatment. The electrical resistivity was significantly increased when the films were annealed at higher temperature. Although the optical transmittance of AHZO films didn't highly changed by heat treatment, the optical band gap was reduced, regardless of annealing temperature and duration. The thermal stability of AHZO films was worse compared to AZO films.

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수산화나트륨 수용액으로 처리한 흑연의 열/전기전도 특성 (Thermal / Electrical Conductivities of Graphites Treated in Aqueous NaOH Solution)

  • 송승원;민의홍;이동원;김정수;남대근;오원태
    • 한국전기전자재료학회논문지
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    • 제29권10호
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    • pp.659-664
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    • 2016
  • Thermal and electrical conductivities of the natural, artificial, and expandable graphites were analyzed after treatment in NaOH aqueous solution. In order to investigate the elimination of the oxidized groups and impurities on the graphite surfaces after NaOH treatment, the graphite samples were structurally characterized by using XRD, XPS, Raman, FE-SEM. The thermal and electrical conductivities of the graphite samples were significantly improved after NaOH treatment. These results were caused by the structural rehabiliation.

Influence of Sulfur Fertilization on the Antioxidant Activities of Onion Juices Prepared by Thermal Treatment

  • Koh, Eunmi;Surh, Jeonghee
    • Preventive Nutrition and Food Science
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    • 제21권2호
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    • pp.160-164
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    • 2016
  • Two onions (Sulfur-1 and Sulfur-4) cultivated with different sulfur applications were thermally processed to elucidate the effects of heat treatment on browning index and antioxidant activity. Sulfur-4 onion had higher sulfur content compared with the Sulfur-1 onion. After thermal processing, browning intensity was different between the two onions juices, with lower values observed for Sulfur-4 onion juice. This suggests that sulfur inhibits the Maillard browning reaction. The total reducing capacity of the juices increased at higher thermal processing temperatures; however, it was also lower in the Sulfur-4 onion juice. This suggests that the heat treatment of onions enhanced their antioxidant activity, but the effect was offset in the Sulfur-4 onion juice presumably due to higher sulfur content. This study indicates that sulfur, a core element for the functionality of onions, can decrease the antioxidant activity of thermally processed onions because of its potential as a Maillard reaction inhibitor.