• 한국진공학회:학술대회논문집
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• 한국진공학회 2014년도 제46회 동계 정기학술대회 초록집
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• pp.159.1-159.1
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• 2014

We report a simple method for preparing hydrophobic mesoporous silica and its use as a pre-concentrating agent of gas analytes. Hydrophobic mesoporous silica was prepared by coating PDMS (polydimethylsiloxane) thin layer on commercial mesoporous silica with thermal deposition method in a sealed chamber. By using this method, we were able to coat PDMS layer on inner-walls of pores larger than 15 nm. Also, contact angle measured on a surface consisting of PDMS-coated mesoporous silica exceeded $150^{\circ}$, implying that the surface has high water repellency. Pre-concentration ability of PDMS-coated mesoporous silica and baremesoporous silica was tested under dry and humid conditions. Adsorption and molecular desorption of gas analytes was much enhanced by PDMS-coating on mesoporous silica under both dry and humid conditions. Therefore we suggest that PDMS-coated mesoporous silica can be an efficient pre-concentration agent in order to enhance sensitivity of various detectors.

• 동력기계공학회지
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• 제9권4호
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• pp.137-142
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• 2005

The effects of temperature and initial crack length on impact fracture behavior of side plate material of 35 ton class FRP ship, which are composed by glass fiber and unsaturated polyester resin, were investigated. Impact fracture toughness of GF/PE composites displayed maximum value when the temperature of specimen is room temperature and $50^{\circ}C$, and with decrease in temperature of specimen, impact fracture toughness decreased. Impact fracture energy of GF/EP composites decreased with increase in initial crack length of specimen, and this value decreased rapidly when the temperature of specimen is lowest, $-25^{\circ}C$,. It is believed that sensitivity of notch on impact fracture energy were increased with decrease in temperature of specimen. As the GF/EP composites exposed in low temperature, impact fracture toughness of composites decreased gradually owing to the decrease of interface bonding strength caused by difference of thermal expansion coefficient between the glass fiber/polyester resin. Further, decrease of interface bonding strength of composites with decrease in specimen temperature was ascertained by SEM photograph of impact fracture surface.

• 센서학회지
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• 제18권2호
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• pp.147-153
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• 2009

A thermal flow sensor has been fabricated and characterized, consisting of a center resistive heater surrounded by two upstream and one downstream temperature sensing resistors. The heater and temperature sensing resistors are fabricated from nitrogen-doped(n-type) polycrystalline silicon carbide(poly-SiC) deposited by LPCVD(low pressure chemical vapor deposition) on LPCVD silicon nitride films on a Si substrate. Cavities were etched into the Si substrate from the front side to create suspended silicon nitride membranes carrying the poly-SiC elements. One upstream sensor is located $50{\mu}m$ from the heater and has a sensitivity of $0.73{\Omega}$/sccm with ${\sim}15\;ms$ rise time in a dynamic range of 1000 sccm. N-type poly-SiC has a linear negative temperature coefficient and a TCR(temperature coefficient of resistance) of $-1.24{\times}10^{-3}/^{\circ}C$ from room temperature to $100^{\circ}C$.

• 대한조선학회논문집
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• 제48권3호
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• pp.189-199
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• 2011

Austenite stainless steel(ASS), aluminum alloy and nickel steel alloy are the most widely used in many cryogenic applications due to superior mechanical properties at low temperature. The Face-Centered Cubic(FCC) and Hexagonal Close-Packed(HCP) materials are used for the primary and secondary insulation barrier of Liquefied Natural Gas(LNG) carrier tank and various kinds of LNG applications currently. In this study, tensile tests of ASS, aluminum alloy and nickel steel alloy were carried out for the acquisition of quantitative mechanical properties under the cryogenic environment. The range of thermal condition was room temperature to $-163^{\circ}C$ and strain rate range was 0.00016/s to 0.01/s considering the dependencies of temperatures and strain rates. The comprehensive test data were analyzed in terms of the characteristics of mechanical behavior for the development of constitutive equation and its application.

• Journal of Welding and Joining
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• 제31권5호
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• pp.59-63
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• 2013

A bendable electronic module has been developed for a mobile application by using a low-cost roll-to-roll manufacturing process. In flexible embedded electronic module, a thin silicon chip was embedded in a polymer-based encapsulating adhesive between flexible copper clad polyimide layers. To confirm reliability and durability of prototype bendable module, the following tests were conducted: Moisture sensitivity level, thermal shock test, high temperature & high humidity storage test, and pressure cooker tester. Those experiments to induce failure of the module due to temperature variations and moisture are the experiment to verify the reliability. Failure criterion was 20% increase in bump resistance from the initial value. The mechanism of the increase of the bump resistance was analyzed by using non-destructive X-ray analysis and scanning acoustic microscopy. During the pressure cooker test (PCT), delamination occurred at the various interfaces of the bendable embedded modules. To investigate the failure mechanism, moisture diffusion analysis was conducted to the pressure cooker's test. The hygroscopic characteristics of the encapsulating polymeric materials were experimentally determined. Analysis results have shown moisture saturation process of flexible module under high temperature/high humidity and high atmosphere conditions. Based on these results, stress factor and failure mechanism/mode of bendable embedded electronic module were obtained.

• 한국표면공학회:학술대회논문집
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• 한국표면공학회 2018년도 춘계학술대회 논문집
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• pp.83-83
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• 2018

최근 의료, 보건, 헬스케어 분야에 대한 관심이 증가함에 따라 질병의 조기 진단 연구가 각광 받고 있다. 특히 표면증강 라만 산란 (Surface Enhancement Raman scattering)은 고분자 검출을 위해 가장 유용한 물리 화학적 기법으로 SERS를 활용한 특정물질 검출 기술 개발에 대한 연구가 많이 이루어지고 있다. 나노구조의 국부적 표면 플라즈몬의 공명조건 (Surface Plasmon Resonance, SPR)으로 유도된 전자기장은 우수한 SERS 신호를 나타낸다. 따라서 표면 플라즈몬 공명 효과는 귀금속 나노입자의 종류, 크기 및 형태, 기판의 형상 및 구조 등에 의해서 달라지게 되므로 이들을 조절하여 보다 민감한 SERS 신호를 얻을 수 있다. 본 연구에서는 고감도 SERS-Active 기판을 제작하기 위해 SERS 기판 표면의 나노구조를 최적화 하였다. SERS 기판 표면을 제어하기 위해 공정파워, 공정압력, 기판의 온도 등의 증착공정 변수에 변화를 주어 표면의 나노구조를 형성하였다. 이를 분석하기 위해 SEM 분석을 통해 피라미드형 실리콘 기판 표면의 Au 나노구조 금속 박막을 확인하였고, XRD를 이용하여 결정성 및 결정크기를 확인하였다. Rhodamine 6G를 이용한 라만 분석을 통해 SERS 신호의 강도를 알 수 있었다. 금속 나노구조의 형태, 온도 제어를 통해 SERS 신호강도가 우수한 나노구조 기판을 제조 할 수 있었다.

• 한국안전학회지
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• 제19권3호
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• pp.51-56
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• 2004

Conductive polymer blends and composites are widely used for different safety application such as electrostatic charge dissipation(ESD), electromagnetic interference(EMI) shielding, electrostatic prevention and safety chemical sensor. In order to prepare a impedance-type humidity sensor that is durable at high humidities and high temperature, electically conductive polymer blends based on diallyldimethylammonium chloride(DADMAC) and epoxy were prepared in this study. The polymer blends type conductive ionomer exhibits reaction each other DADMAC and epoxy in FT-IR and DSC analysis. The blends material was traced by new peak at 1600cm-1 and appeard improvement of thermal resistance by melting point shift. Alumina substrate was deposited a pair of gold electrodes by screen printing. The blend material were spin-coated with a thin film type on the surface of alumina substrate. The polymer bleld type sensor exhibits a linear impedance increasing better than DADMAC coated humidity sensor. Also it shows good sensitivity, low hysteresis and durability against high humidity.

• Nuclear Engineering and Technology
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• 제47권1호
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• pp.66-73
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• 2015

Background: A numerical simulation was carried out to investigate the difference between internal and external heat-flux distributions at the reactor vessel wall under in-vessel retention through external reactor vessel cooling (IVR-ERVC). Methods: Total loss of feed water, station blackout, and large break loss of coolant accidents were selected as the severe accident scenarios, and a transient analysis using the element-birth-and-death technique was conducted to reflect the vessel erosion (vessel wall thickness change) effect. Results: It was found that the maximum heat flux at the focusing region was decreased at least 10% when considering the two-dimensional heat conduction at the reactor vessel wall. Conclusion: The results show that a higher thermal margin for the IVR-ERVC strategy can be achieved in the focusing region. In addition, sensitivity studies revealed that the heat flux and reactor vessel thickness are dominantly affected by the molten corium pool formation according to the accident scenario.

• 한국압력기기공학회 논문집
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• 제13권1호
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• pp.61-68
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• 2017

Reactor pressure vessel (RPV) under severe accident conditions accompanied by core melting is exposed to direct high-temperature thermal loads. Understanding the creep behavior of the material is one of the most important factors for evaluating the structural integrity at these conditions. While damage evaluation studies have been conducted on critical structures of nuclear power plants through finite element (FE) analyses considering creep behavior, for accurate creep damage evaluation, constitutive equations considered in the FE analyses may have different results depending on the time hardening and strain hardening models as well as the tertiary creep consideration. The purpose of this study is to evaluate the creep damage under severe accident conditions by using FE method for a representative domestic RPV material, SA508 Gr.3. The effect of material hardening models and constitutive equations which are the main variables were also investigated.

• 설비공학논문집
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• 제15권10호
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• pp.879-887
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• 2003

Buildings with heating and cooling systems have been increased, since the requirement of thermal comfort for residents is grown. Heating and cooling systems, have been changed from two separate systems to one multi-function system which includes both heating and cooling. Especially, heat pump heating and cooling system has been adopted for general classrooms in schools since education environment improvement project has been launched. This research suggests the best option for the heat pump heating and cooling system in educational buildings through economic assessments for four alternative systems based on electric heat pump (EHP) and gas engine driven heat pump (GHP), which are most widely used for elementary, middle and high schools. The model buildings are in the Y high school which has 24 classes of new construction building, which will be built soon. Annual energy consumption for alternative systems uses BECS 3.10, which can be used for system simulation.