• Title/Summary/Keyword: Thermal Aging

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A study on Au-Sn alloy plating layer improving reliability of electrical contacts (전자부품 커넥터의 접속 신뢰성 향상을 위한 Au-Sn 합금 도금층 연구)

  • Choi, Jong Hwan;Son, Injoon
    • Journal of the Korean institute of surface engineering
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    • v.55 no.6
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    • pp.408-416
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    • 2022
  • In this study, the effect of Au-Sn alloy coating on reliability of electrical contacts was investigated via comparison with Au-Co alloy coating. The results show that Au-Sn alloy exhibited lower contact resistance and higher solder spreadability than those of Au-Co alloy after thermal aging. In the case of Au-Co alloy plating, the underlying Ni element diffused into Au-Co layer to form Ni oxides on surface during thermal aging, leading to increased contact resistance and decreased solder spreadability. Meanwhile, for Au-Sn alloy plating, Au-Ni-Sn metallic compound was formed at the interface between Au-Sn layer and underlying Ni layer. This compound acted as a diffusion barrier, thereby inhibiting the diffusion of Ni to Au-Sn layer during thermal aging. Consequently, Au-Sn alloy layer showed better contact reliability than that of Au-Co alloy layer.

Effects of Thermal Aging on the Fracture Characteristic in the Dissimilar Welds (CF8M과 SA508 용접재의 열화에 따른 파괴특성 평가)

  • Woo, Seung-Wan;Kwon, Jae-Do;Choi, Sung-Jong;Choi, Young-Hwan
    • Proceedings of the KSME Conference
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    • 2004.04a
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    • pp.72-77
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    • 2004
  • In a primary reactor cooling system(RCS), a dissimilar weld zone exists between cast stainless steel(CF8M) in a pipe and low-alloy steel(SA508 cl.3) in a nozzle. Thermal aging is observed in CF8M as the RCS is exposed for a long period of time to a reactor operating temperature between 290 and $330^{\circ}C$, while no effect is observed in SA508 cl.3. The specimens are prepared by an artificially accelerated aging technique maintained for 300, 1800 and 3600 hrs at $430^{\circ}C$, respectively. The specimens for elastic-plastic fracture toughness tests are prepared one type, which notch is created in the heat affected zone(HAZ) of CF8M. And, the specimens for fatigue crack growth tests are prepared in three classes, which notches are created at the center of deposited zone, the HAZ of CF8M, and the HAZ of SA508 cl.3. From the experiments, the J-integral values with the increase of aging time decrease, and the differences of the fatigue crack growth behaviors are relatively small in the three classes specimens.

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Evaluation of Bond Strength of Isothermally Aged Plasma Sprayed Thermal Barrier Coating (플라즈마 용사 열차폐 코팅의 열화에 따른 접착강도 평가)

  • Kim, Dae-Jin;Lee, Dong-Hoon;Koo, Jae-Mean;Song, Sung-Jin;Seok, Chang-Sung;Kim, Mun-Young
    • Transactions of the Korean Society of Mechanical Engineers A
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    • v.32 no.7
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    • pp.569-575
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    • 2008
  • In this study, disk type of thermal barrier coating system for gas turbine blade was isothermally aged in the furnace changing exposure time and temperature. For each aging condition, bond tests for three samples were conducted for evaluating degradation of adhesive or cohesive strength of thermal barrier coating system. For as-sprayed condition, the location of fracture in the bond test was in the middle of epoxy which have bond strength of 57 MPa. As specimens are degraded by thermal aging, bond strength gradually decreased and the location of failure was also changed from within top coat at the earlier stage of thermal aging to the interface between top coat and TGO at the later stage due to the delamination in the coating.

A Comparative Study on the Characteristics of Accelerated aging at Low and High Temperatures of the Fluorocarbon Rubber Composites (불소 고무복합체의 저온과 고온촉진노화 특성에 대한 비교 연구)

  • Park, JeongBae;Lee, BeomCheol;Jeong, YoonSeok;Park, SungHan
    • Proceedings of the Korean Society of Propulsion Engineers Conference
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    • 2017.05a
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    • pp.915-922
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    • 2017
  • The study on the thermal and oil resistance rubber composite, 2016. [6] predicted the lifetime of Fluorocarbon Rubber by accelerating aging at high temperature ($150^{\circ}C$, $175^{\circ}C$, $200^{\circ}C$). general rubber products are likely to exhibit different properties depending on the degradation factors such as temperature, humidity, ozone, light, emulsion, mechanical and electrical stress. To solve these problems, We compared the rate of change about tensile strength, elongation rate, volume change rate, weight change rate, thickness change rate, thermal conductivity in low temperature promoting aging on the basis of predictive lifetime of high temperature promoting aging. As a result of the review, the required life expectancy was satisfied, but there was a slight difference in the rate of change between the high-temperature promoted aging life result and the low temperature promoted aging life result. The cause was a reduction in "tensile strength / elongation" and an increase in "volume / weight / thickness" caused by the main chain decomposition of fluorine rubber due to aging at high temperature promoting aging. However, the low temperature promoting aging was caused by the curing reaction of fluorine rubber at $80^{\circ}C$. The tensile strength / elongation and volume / weight / thickness changes were small.

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Analysis of Degradation Characteristics for Oil-Paper Insulation using Tan Delta Measurement (Tan Delta 측정을 이용한 유침 절연지의 열화특성 분석)

  • Kim, Jeong-Tae;Kim, Woo-Bin
    • The Transactions of The Korean Institute of Electrical Engineers
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    • v.65 no.9
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    • pp.1518-1523
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    • 2016
  • In this study, in order to understand the degradation characteristics of oil-paper insulation for power transformers and OF cables, tan delta was measured using cable model specimens with long-term accelerated thermal and electrical aging. In addition, to find out the degradation level due to the accelerated aging, tensile strengths of aged papers were measured. As a result, tan ${\delta}$ showed the characteristics of slight decrease at the first stage and then increase with the aging time, which could be analyzed due to the evaporation of remaining moisture and the change of aging rate with time. Also, the trend of tensile strengths with aging temperature and time was appeared to be exponentially decreased and by use of these data equivalent calculated lifetimes and accelerated aging factors were derived for each aging temperatures. After then, tan ${\delta}$ was analyzed with the equivalent operating years. For all different aging temperatures, the aged data were very well fit to the equivalent operating years and it is shown that tan ${\delta}$ was increased with the decrease of tensile strength.

Analysis of Activation Energy of Thermal Aging Embrittlement in Cast Austenite Stainless Steels (주조 오스테나이트 스테인리스강의 열취화 활성화에너지 분석)

  • Gyeong-Geun Lee;Suk-Min Hong;Ji-Su Kim;Dong-Hyun Ahn;Jong-Min Kim
    • Transactions of the Korean Society of Pressure Vessels and Piping
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    • v.20 no.1
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    • pp.56-65
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    • 2024
  • Cast austenitic stainless steels (CASS) and austenitic stainless steel weldments with a ferrite-austenite duplex structure are widely used in nuclear power plants, incorporating ferrite phase to enhance strength, stress relief, and corrosion resistance. Thermal aging at 290-325℃ can induce embrittlement, primarily due to spinodal decomposition and G-phase precipitation in the ferrite phase. This study evaluates the effects of thermal aging by collecting and analyzing various mechanical properties, such as Charpy impact energy, ferrite microhardness, and tensile strength, from various literature sources. Different model expressions, including hyperbolic tangent and phase transformation equations, are applied to calculate activation energy (Q) of room-temperature impact energies, and the results are compared. Additionally, predictive models for Q based on material composition are evaluated, and the potential of machine learning techniques for improving prediction accuracy is explored. The study also examines the use of ferrite microhardness and tensile strength in calculating Q and assessing thermal embrittlement. The findings provide insights for developing advanced prediction models for the thermal embrittlement behavior of CASS and the weldments of austenitic steels, contributing to the safety and reliability of nuclear power plant components.

Accelerated Aging Characteristics of Electroconductive Paper (탄소섬유를 첨가한 전도성 종이의 강제열화 특성)

  • Kim, Bong-Yong
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.43 no.2
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    • pp.24-30
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    • 2011
  • The accelerated aging characteristics of electroconductive papers manufactured with a mixture of carbon fiber were investigated by heating in dry oven. By accelerated aging time, the tensile strength, tensile stretch of the papers were decreased more slowly with increase of carbon fiber content, but the electrical conductivity was more rapidly decreased in case of high carbon fiber content. The weight loss of papers by thermal analysis were reduced as increasing the carbon fiber content. These results were indicated that the electrical conductivity of carbon fiber was diminished easily by heat aging, but thermal characteristic of carbon fiber was much better than that of wood pulp.

Effect of Aging on Adhesive Strength of Rubber-steel Cord Composite and Tire-endurance (고무-스틸 코드 접착력과 타이어 내구력에 미치는 노화의 영향)

  • Lim, Won-Woo
    • Journal of Adhesion and Interface
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    • v.3 no.2
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    • pp.40-44
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    • 2002
  • We invested effect of the keeping-time of uncured composite and thermal aging, of cured composite on adhesive strength for rubber-brass coated steel cord composite in this study. We also evaluated how the adhesive strength affects to tire endurance. Using PAD adhesion specimen, peel adhesive strength was measured. The uncured composite was kept for several days up to 35 days in factory. Cured composite was also kept for 5 and 10 days at $85^{\circ}C$ in dry oven. Peel adhesive strength was decreased with increasing keeping-time and showed lower value with increasing thermal aging time. The lower peel adhesive strength, the lower tire-endurance. This fact was caused by the humidity and thermal aging which affected in the decrease of adhesive strength of the rubber-steel cord composite and resulted in interface fracture between rubber and steel cord. This phenomenon was confirmed from SEM investigation and tire-endurance. It was just known that corrosion of steel cord's surface and aging of adhesive layer strongly affected to decrease of adhesive strength. This resulted in directly decreasing tire-endurance.

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Effect of Thermal Aging on Microstructure and Mechanical Properties of China Low-Activation Martensitic Steel at 550℃

  • Wang, Wei;Liu, Shaojun;Xu, Gang;Zhang, Baoren;Huang, Qunying
    • Nuclear Engineering and Technology
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    • v.48 no.2
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    • pp.518-524
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    • 2016
  • The thermal aging effects on mechanical properties and microstructures in China low-activation martensitic steel have been tested by aging at $550^{\circ}C$ for 2,000 hours, 4,000 hours, and 10,000 hours. The microstructure was analyzed by scanning and transmission electron microscopy. The results showed that the grain size and martensitic lath increased by about $4{\mu}m$ and $0.3{\mu}m$, respectively, after thermal exposure at $550^{\circ}C$ for 10,000 hours. MX type particles such as TaC precipitated on the matrix and Laves-phase was found on the martensitic lath boundary and grain boundary on aged specimens. The mechanical properties were investigated with tensile and Charpy impact tests. Tensile properties were not seriously affected by aging. Neither yield strength nor ultimate tensile strength changed significantly. However, the ductile-brittle transition temperature of China low-activation martensitic steel increased by $46^{\circ}C$ after aging for 10,000 hours due to precipitation and grain coarsening.

The Study of Long-Term Performance Evaluation of Vacuum Insulation Panel(VIP) with Accelerated Aging Test (가속노화 시험을 통한 진공단열패널(VIP)의 장기성능 평가 연구)

  • Kim, Jin-Hee;Kim, Jun-Tae
    • Journal of the Korean Solar Energy Society
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    • v.37 no.4
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    • pp.35-47
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    • 2017
  • Energy efficiency solutions are being pursued as a sustainable approach to reducing energy consumption and related gas emissions across various sectors of the economy. Vacuum Insulation Panel (VIP) is an energy efficient advanced insulation system that facilitates slim but high-performance insulation, based on a porous core material evacuated and encapsulated in a barrier envelope. Although VIP has been applied in buildings for over a decade, it wasn't until recently that efforts have been initiated to propose and adopt a global standard on characterization and testing of VIP. One of the issues regarding VIP is its durability and aging due to pressure and moisture dependent increase of the initial low thermal conductivity with time; more so in building applications. In this paper, the aging of commercially available VIP was investigated experimentally; thermal conductivity was tested in accordance with ISO 8302 standard (guarded hot box method) and long-term durability was estimated based on a non-linear pressure-humidity dependent equation based on study of IEA/ECBCS Annex 39, with the aim of assessing durability of VIP for use in buildings. The center-of-panel thermal conductivity after 25 years based on initial 90% fractile with a confidence level of 90 % for the thermal conductivity (${\lambda}90/90$) ranged from 0.00726-0.00814 (W/m K) for silica core VIP. Significant differences between manufacturer-provided data and measurements of thermal conductivity and internal pressure were observed.