• Title/Summary/Keyword: Tensile strength test

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Synthesis and Characterization of HEMA-PCL Macromer Grafted onto Starch (옥수수전분에 HEMA-PCL Macromer를 그래프팅시킨 공중합체의 합성 및 특성)

  • 공원석;진인주;김말남;김수현;윤진산
    • Polymer(Korea)
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    • v.24 no.2
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    • pp.141-148
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    • 2000
  • Polycaprolactone (PCL) was blended with corn starch to produce biodegradable compost films and the biodegradability and mechanical properties were investigated. As the compatibilizer for the immiscible PCL/starch blend, 2-hydroxyethylmethacrylate (HEMA)-PCL macromer was grafted onto starch by initially grafting HEMA to starch and then grafting of PCL onto HEMA via ring opening polymerization of $\varepsilon$-caprolactone. When biodegradability of the PCL grafted starch-g-DEMA copolymers was compared with that of starch by the modified Sturm test, graft copolymers degraded at much slower rates due to the presence of the non-degradable HEMA. With the addition of the graft copolymer up to 5 wt% to the blend, the elongation-at-break of the starch/PCL blend increased substantially, while the tensile strength and modulus did not change much. SEM observation of the blend containing 2 wt% copolymer clearly indicated that the interfacial adhesion between the starch and PCL was strengthened by the copolymer.

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An Experimental Research to Evaluate Structural Capacity of Pre-stressed Concrete Beam connected with Embedded Steel Plate (강판으로 접합된 프리스트레스트 콘크리트보의 구조성능 평가를 위한 실험연구)

  • Lee, Kyoung-Hun;Kim, Jeom-Han
    • Journal of the Korean Society of Hazard Mitigation
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    • v.10 no.5
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    • pp.27-33
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    • 2010
  • In this study, a monotonic loading test to estimate structural capacity of 12 meter long full scale precast pre-stressed concrete beam specimen was performed with a 2,000 kN dynamic actuator. A couple of embedded steel plate was installed at the ends of the beam and specimens were connected to steel girder frame with high tension bolts. Nominal compressive strength of pre-stressed concrete beam and slab were 50 MPa and 24 MPa respectively. Two HD25 tensile steel reinforcements were welded on vertical plate of embedded steel plate. Pre-stressed concrete beam specimen was loaded by displacement control method with a certain loading pattern which was repeated loading and unloading with 10mm increment displacement. About 88.34%, 86.97% and 66.83% of displacement restoration ratios were evaluated at elastic, inelastic and plastic behavior region of specimen respectively.

Acrylamide Polymerization on ceramic Powders(I) : The Process Control of Si2N4 Gelcasting by Polymerization of Acrylamicde (세라믹분체 표면에서 아크릴아마이드 중합(제1보) : 아마이드 고분자중합에 의한 질화규소 겔캐스팅 공정제어)

  • 류병환;김은영;이재도
    • Journal of the Korean Ceramic Society
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    • v.36 no.2
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    • pp.178-185
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    • 1999
  • For the process control of silicon nitride gelcasting, the composition effect of acryamide system on the viscosity of slip and mechanical property of gelcast green body were investigated. The slip was prepared by ball milling of silicon nitride suspension prepared with acrylamide monomer and polyelectrolyte dispersant after premixing them by attritor. The slip mixed with initiator was vacuum deaired and cast into molds, and then polymerized. The consolidated green body was obtained by drying the gelated slip. The viscosity measument and the diametral compression test was done to evaluate the rheological behaviro of slip and mechanical property of gelcast body, respectively. Experimental results showed that the high solid loading of silicon nitride slip was obtained up to 46 vol% with a low viscosity. The mechanical property of gelcast body mainly increased with increasing the concentration of monomer. The gelcast body was machinable above the ∼3 MPa of tensile strength. The relative density of pressured-sintered body was 98.5% at 1760$^{\circ}C$, 3 h.

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Development of Thin, Transparent Oxo-Biodegradable Film with Antibacterial and Freshness Agent (항균, 신선도 기능을 부여한 투명 산화생분해 필름 개발)

  • Choi, Sung-Wook;Lee, Kun-Woo;Yu, Ji-Ye;You, Young-Sun
    • KOREAN JOURNAL OF PACKAGING SCIENCE & TECHNOLOGY
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    • v.23 no.3
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    • pp.133-141
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    • 2017
  • This article described the development of transparent antimicrobial oxo-biodegradable (AOB) film with the function of enhanced freshness of food by employing oxo-biodegradable masterbatch (MB) and antimicrobial MB together with organic metal salt, organic acid, or unsaturated fatty acid. Antibacterial test of the AOB film with the different contents of the antimicrobial MB resulted in the significant freshness extension of plum. Tensile strength and elongation rate of the AOB films before UV treatment were similar to those of polyethylene films used as control. The reduced mechanical properties of AOB film after UV treatment (340 nm) suggested that the AOB film could be degraded by oxo biodegradation. The developed AOB films can effectively prevent decomposition of food by providing antibacterial function and preserving freshness.

Effect of NbC Carbide Addition on Mechanical Properties of Matrix-Type Cold-Work Tool Steel (매트릭스(matrix)형 냉간금형강의 기계적 특성에 미치는 NbC 탄화물 첨가의 영향)

  • Kang, Jun-Yun;Kim, Hoyoung;Son, Dongmin;Lee, Jae-Jin;Yun, Hyo Yun;Lee, Tae-Ho;Park, Seong-Jun;Park, Soon Keun
    • Journal of the Korean Society for Heat Treatment
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    • v.28 no.5
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    • pp.239-249
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    • 2015
  • Various amount of NbC carbide was intentionally formed in a matrix-type cold-work tool steel by controlled amount of Nb and C addition. And the effect of NbC addition on the mechanical properties was investigated. Four alloys with different Nb and C contents were cast by vacuum induction melting, then hot forging and spheroidizing annealing were conducted. The machinability of the annealed specimens was examined with 3 different cutting tools. And tensile tests at room temperature were conducted. After quenching and tempering, hardness and impact toughness were measured, while wear resistance was evaluated by disk-on-plate type wear test. The increasing amount of NbC addition resulted in degraded machinability with increased strength, whereas the absence of NbC also led to poor machinability due to high toughness. After quenching and tempering, the additional NbC improved wear resistance with increasing hardness, whereas it deteriorated impact toughness. Therefore, it could be found that a moderate addition of NbC was desirable for the balanced combination of mechanical properties.

Field Application of Hydraulic Rock Splitting Technique to Biotite Granite (흑운모화강암 지역에 대한 수압암반절개기술의 현장 적용)

  • Park, Jongoh;Lee, Dal-Heui;Woo, Ik
    • Tunnel and Underground Space
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    • v.27 no.5
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    • pp.263-270
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    • 2017
  • Hydraulic rock splitting is a technique which leads to failure of rockmass by means of water injection with a pressure higher than the tensile strength of rockmass, using straddle packer installed in boreholes drilled from free surface. Field tests were conducted in this study for several slopes of biotite granite according to various designs for borehole layout and water injection. Test results showed that new cracks were generated to connect to adjacent holes or that pre-existed cracks were propagated by injection, finally leading to failure. In particular, this study suggests the possibility of controlling the direction of generated cracks with guide slot, since new cracks were generated parallel to the guide slots carved on a borehole wall before injection. Various types of borehole layout and injection methods should be further developed for the practical uses, considering the factors influencing on crack generation.

Longitudinal Elongation of Slender Reinforced Concrete Beams Subjected to Cyclic Loading (주기하중을 받는 세장한 철근콘크리트 보의 길이방향 인장변형)

  • Eom, Tae-Sung;Park, Hong-Gun
    • Journal of the Korea Concrete Institute
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    • v.20 no.6
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    • pp.785-796
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    • 2008
  • Longitudinal elongation develops in reinforced concrete beams that exhibit flexural yielding during cyclic loading. The longitudinal elongation can decrease the shear strength and deformation capacity of the beams. In the present study, nonlinear truss model analysis was performed to study the elongation mechanism of reinforced concrete beams. The results showed that residual tensile plastic strain of the longitudinal reinforcing bar in the plastic hinge is the primary factor causing the member elongation, and that the shear-force transfer mechanism of diagonal concrete struts has a substantial effect on the magnitude of the elongation. Based on the analysis results, a simplified method for evaluating member elongation was developed. The proposed method was applied to test specimens with various design parameters and loading conditions.

자동차용 강판의 온도에 따른 기계적 특성

  • Hyeon, Ju-Sik;Lee, Bo-Ryong;Mun, Man-Bin
    • Proceedings of the Materials Research Society of Korea Conference
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    • 2010.05a
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    • pp.39.1-39.1
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    • 2010
  • 겨울철 혹한지방에서의 차량운행 또는 여름철 혹서지방에서의 장시간 차량 운행시 차체를 구성하고 있는 강판에는 약 $-50^{\circ}C{\sim}150^{\circ}C$의 온도환경에 처하게 된다. 따라서 이러한 저온 고온 환경하에서 차체 충돌상품성 예측 및 충돌안전 설계를 위해 온도에 따른 차체 강판의 기계적 물성평가가 요구된다. 이를 위해 본 연구에서는 자동차용 충돌부재에 주로 쓰이는 HS440MPa, HS590MPa급 냉연 고장력 강판에 대해 $-60^{\circ}C{\sim}200^{\circ}C$의 온도범위로 저온 고온 인장시험을 수행 하였다. 각각의 인장시험 결과로부터 온도 별 항복강도, 인장강도, 연신율, 가공경화지수 등 기계적 물성 변화를 평가하였다. 저온 고온 인장시험은 ZWICK Z250 만능재료시험기를 사용하였고 KS5호 규격의 인장시편을 사용하였으며, 시편에 충분한 온도를 가하기 위하여 목표온도 도달 후 20분간 유지한 뒤 인장시험을 수행하였다. 인장시험결과 HS440MPa, HS590MPa급 두 강종 모두 온도가 낮아질수록 강도 및 연신율 등이 증가하였고, 온도가 증가할수록 강도 및 연신율 등 기계적 물성이 저하 되었다. 즉, 우리가 주로 평가해왔던 상온($25^{\circ}C$)에 비해 저온 고온 환경하에서는 강판의 기계적 물성 변화가 큰 것을 알 수 있다. 따라서 혹한 또는 혹서 지방 등 온도차이가 큰 운행환경하에서의 차체 강도 및 충돌안전성 확보를 위해 온도에 따른 강판의 정확한 물성평가가 필요하고 차체 설계시 온도에 따른 강도변화를 충분히 고려하여야 한다.

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Carbon Nanotubes Reinforced Poly(ethylene terephthalate) Nanocomposites (탄소나노튜브로 강화시킨 Poly(ethylene terephthalate) 나노복합재료)

  • Choi, Soohee;Jeong, Youngjin
    • Polymer(Korea)
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    • v.38 no.2
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    • pp.240-249
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    • 2014
  • Multi-walled carbon nanotube (MWNT) reinforced poly(ethylene terephthalate) (PET) composites are studied. To increase the interfacial interactions between PET and MWNTs, the MWNTs are functionalized with bishydroxy-ethylene-terephthalate (BHET). The functionalized MWNTs are melt blended into PET matrix using a twin screw extruder. The amount of MWNTs loaded in PET matrix ranges from 0.5 to 2.0 wt%. After compounding and spinning, the filaments are post-drawn and annealed. To verify the chemical modifications of carbon nanotubes, Raman, $^1H$ NMR, XPS, TGA and FE-SEM are used. The nanocomposites are also analyzed with DSC, TGA, and UTM. These tests show that crystallization temperature and thermal degradation temperature increase due to the functionalized MWNTs. Also, tensile test shows that yield strength and toughness increase more than 30% with addition of only 1 wt% of MWNTs. These results show that the introduction of BHET onto the MWNTs is a very effective way in manufacturing MWNT/PET composite.

A Study on the Characteristics of Natural Preservative Agent-treated Fabrics for Textile Cultural Properties Preservation (섬유문화재 보존에 활용하기 위한 천연보존제로 처리한 직물의 특성연구)

  • Baek, Young-Mee
    • Journal of Conservation Science
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    • v.25 no.2
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    • pp.197-206
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    • 2009
  • Natural preservative agents are generally made of antibiotic substances that are extracted from plants. They are used mainly to keep in an original good state food, natural cosmetic goods and medicines which are likely to get rotten. The purpose of this study is to investigate whether natural preservative agents can be applied to fabrics for the preservation of textile cultural properties. For the purpose, this researcher experimented with a certain natural preservative agent which was developed to preserve natural cosmetic goods. The study found that when treated with the foresaid natural preservative agent whose ratio to water was 1%, fabrics showed little changes in color and tensile strength, almost neutral pH, high antibiosis and anti-fungus and high resistance to Bacillus cereus that is much detrimental to silk fabrics. As a part of the study, a preliminary test on the possibility of using natural preservative agents to preserve textile cultural properties, found that when kept covered up with the 1% natural preservative agent-treated fabrics for 72 hours, excavated textile relics showed a dramatic decrease in microbial growth.

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