• Elastomers and Composites
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• 제38권4호
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• pp.342-353
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• 2003

본 연구는 폴리에스터 가소제를 이용한 내제트유성 PVC계 실란트 개발에 관한 것이다. PVC 공중합체에 아디프산 글리콜 폴리에스터 가소제(Songcizer P-3000) 또는 DOP를 배합하여 연료유 함침 전후의 칩입도 변화, 용해도, 흐름성 및 인장 접착 신율을 측정하였다. 연료유 함침 전후 칩입도 변화 및 용해도를 측정한 결과 폴리에스터 가소제의 내제트유성이 DOP 가소제를 사용한 것 보다 작은 것으로 나타났다. PVC 공중합체에 Songcizer P-3000의 배합비를 중량비로 500 phr로 고정하고 접착성 향상제인 DCDP (dicyclopentadiene)계 석유수지를 400 phr까지 배합한 결과 첨가량에 비례하여 접착 신율이 감소하였다. 탄산칼슘은 연료유의 확산을 방지하였고 Songcizer P-3000을 사용한 경우 용해도를 감소시키는 결과를 얻었다.

• Corrosion Science and Technology
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• 제13권5호
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• pp.186-194
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• 2014

Establishment of adhesion strength measurement procedure for marine epoxy coatings was conducted in order to ensure reliability of the test results. It was found that (1) the increase in thickness of the substrates would induce increase of pull-off strength. Especially, the increase in adhesion strength with the substrate thickness increment was attributed to the transition of stress mode to the pure tensile mode excluding bending effect. (2) The longer curing time, the higher pull-off strength. It may be due to higher cross-linking density of the coating (3) The pull-off strength increases as coating thickness increases due to the diminishment of bending effect (4) The longer drying time after water immersion, the higher pull-off strength. It may be due to the evaporation of water molecule at the coating-substrate interface.

• 대한기계학회:학술대회논문집
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• 대한기계학회 2003년도 춘계학술대회
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• pp.1104-1110
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• 2003

There are many applications of nanostructures, have been suggested by lots of researchers. It is highly required to measure the properties of nano-sized materials for design and fabrication of the nanostructures. In this paper, several techniques for measuring the mechanical properties of nano-structures are presented laying emphasis on the activity of Nano Property Measurement Team in KIMM. Some advanced applications of nano-indenter are described for measuring elastic, visco-elastic, frictional and adhesive properties as well as the standard methods of it. Micro-tensile test technique with accurate in-plane strain measurement method is also presented and its role in the property measurement of nanostructures is discussed.

• Elastomers and Composites
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• 제49권3호
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• pp.245-252
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• 2014

폴리올, 이소시아네이트, 2-HEMA 및 기타 아크릴레이트 단량체들로부터 제조된 폴리우레탄 접착제의 FT-IR측정과 물성을 검토하였다. 폴리우레탄 접착제의 연화점, 점도, 접착강도 및 기계적 물성들이 각각 링과볼법, Brookfield 점도계 및 만능시험기를 이용하여 검토되었다. 실험 결과에 의하면 PPG 함량 및 부틸아크릴레이트 함량이 증가함에 따라 연화점, 접착강도, 인장강도 및 100% modulus 값 등은 감소하는 것을 보여준다. 하지만 2-HEMA 및 MDI량이 증가할수록 인장강도 및 100% modulus값 등은 증가하였으며 점도와 NCO함량 등도 또한 증가하였다.

• 한국복합재료학회:학술대회논문집
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• 한국복합재료학회 2005년도 춘계학술발표대회 논문집
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• pp.42-45
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• 2005

Interfacial evaluation of various combinations of both Flax and Hemp fibers/polypropylene were performed by using micromechanical test and nondestructive acoustic emission (AE). It can be because interfacial adhesion between the natural fiber surface and matrix plays an important role in controlling the overall mechanical properties of polymer composite materials by transferring the stress from the matrix to the fiber. It is necessary to characterize the interphase and the level of adhesion to understand the performance of the composites properly. Microfailure mechanism of single Flax fiber bundles were investigated using the combination of single fiber tensile test and nondestructive acoustic emission. Microfailure modes of the different natural fiber/polypropylene systems were observed using optical microscope and determined indirectly by AE and their FFT analysis.

• 한국건축시공학회:학술대회논문집
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• 한국건축시공학회 2023년도 봄 학술논문 발표대회
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• pp.41-42
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• 2023

Test results for a total of four types of complex waterproofing methods were analyzed. In the case of the A method, the stress generated by high-viscosity compounds adhering to the base test body during the behavior of the test body was transferred to the sheet surface layer. In the case of the B method and the C method, the properties of the waterproof sheet consisting of a non-hardened seal based and a non-hardened seal are well reflected and stress absorption in the non-hardened seal layer acts strongly, rapidly reducing stress transfer to the surface of the waterproof sheet. In the case of the D method, slip occurs due to repeated behavior, and the stress on the attachment surface is reduced, and the stress transfer to the surface is greatly reduced. As a result, four types of composite waterproofing methods resulted in changing the stress transfer mechanism caused by behavior on the concrete surface due to the physical properties of the internal constituent material of the waterproof sheet.

• 한국염색가공학회지
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• 제27권1호
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• pp.18-26
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• 2015

para-aramid fibers were treated by atmosphere air plasma to improve the interfacial adhesion. The wettability of plasma-treated aramid fiber was observed by means of dynamic contact angle surface free energy measurement. Surface roughness were investigated with the help of scanning electron microscopy and atomic force microscopy. The tensile test of aramid fiber roving was carried out to determine the effect of plasma surface treatments on the mechanical properties of the fibers. A pull-out force test was carried out to observe the interfacial adhesion effect with matrix material. It was found that surface modification and a chemical component ratio of the aramid fibers improved wettability and adhesion characterization. After oxygen plasma, it was indicated that modified the surface roughness of aramid fiber increased mechanical interlocking between the fiber surface and vinylester resin. Consequently the oxygen plasma treatment is able to improve fiber-matrix adhesion through excited functional group and etching effect on fiber surface.

• 한국도로학회논문집
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• 제3권4호
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• pp.117-126
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• 2001

본 연구는 일반 콘크리트와 SBR 라텍스 개질 콘크리트의 부착강도 특성을 분석하고자 신 구 콘크리트로 구성된 직접인장 시험체를 제작하여 부착강도를 측정하였다. 이때, 시험체와 측정기의 연결장치가 $360^{\circ}$ 회전이 가능하도록 시험장비를 개선하여 시험체의 편심이 부착강도 측정에 미치는 영향을 최소화였다. 주요 실험변수로는 라텍스 혼입율, 표면 처리상태, 표면 함수상태로 정하였으며 실험결과는 다음과 같다; 라텍스 혼입률이 증가함에 따라 부착강도도 증가하였으며, 혼입률 15%에서 37%의 증진을 보였다. 이것은 라텍스가 골재와 시멘트 페이스트 사이에 충전되어 필름 막을 형성하고 부착력을 증진시켰기 때문인 것으로 판단된다. 표면처리에 따라 부착강도의 변화를 고찰한 결과, 샌드 그라인딩과 와이어 부러쉬에 의해 표면처리를 하였을 경우 부착강도는 단순 절단한 경우보다 약 49% 증가하였다. 표면함수 상태에 따른 영향을 고찰한 결과, 부착강도는 기존 콘크리트 표면이 건조하였을 경우에 가장 작게 나타났고, 자유수가 표면에 있을 때가 그 다음을 나타냈으며, 표면건조포화상태에선 37% 증가하여 가장 크게 나타났다. 따라서 부착강도를 증진시키기 위해서는 적절한 표면처리와 표면함수상태의 유지가 필수적임을 알 수 있었다.

• 한국지반공학회논문집
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• 제24권8호
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• pp.43-52
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• 2008

본 연구에서는 단철근 네일과 다철근 네일의 인장강도를 조사하기 위해 단철근과 다철근 네일의 극한인발시험과 크리프시험을 수행하였다. 철근과 시멘트 그라우트의 부착력과 인장하중에 의해 유발된 마찰력, 하중전이 특성을 조사하였다. 단철근과 다철근 네일의 현장인발시험과 유한차분해석 프로그램의 하나인 $FLAC^{2D}$를 이용하여 얻은 결과를 분석하고 비교하였다. 다철근 네일의 현장인발시험결과 단철근 네일에 비해 인발파괴하중이 크고 하중전이가 큼을 알 수 있다.

• 열처리공학회지
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• 제15권3호
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• pp.118-126
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• 2002

TiCN thin films were deposited on tool steels at $510^{\circ}C$ by PECVD from a $TiCl_4+N_2+CH_4+H_2+Ar$ gaseous mixture. The microstructures and preferred orientation were investigated. The micro-scratch tests were performed using a system equipped with an acoustic emission sensor. Critical loads were determined to evaluate the adhesion of TiCN to substrate. The influences of the microstructures of substrates, double layered coatings, and coatings after nitriding(duplex coating) were investigated. The experimental results showed that the microstructures of substrates and double layered coating did not affect the critical loads considerably. By the duplex coating, critical loads were not always increased. In some cases, duplex coatings decreased critical loads significantly despite of absence of black layer. In this study, we tried to relate the results of scratch test to the residual stress analysis. Nitriding before the coating reduces the tensile residual stress in the film, which gives rise to low critical load in scratch test.