• Journal of the Korean Wood Science and Technology
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• 제39권3호
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• pp.206-212
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• 2011

라디에타 소나무(Pinus radiata D.Don)를 이용하여 압체 온도와 시간에 따른 압밀화 목재의 경도와 치수안 정성을 조사하였다. 압체 온도가 상승함에 따라 표면경도도 함께 증가하였다. 열압체 시간 30분을 기준으로 압체 온도 $70^{\circ}C$에서는 경도 값이 5.0 N/$mm^2$, $220^{\circ}C$에서 15.6 N/$mm^2$으로 312% 향상되었으며, 60분에서는 313%, 90분에서는 224% 향상되는 것으로 나타났다. 치수회복실험 결과 열압체 온도가 상승함에 따라 치수고정효과는 상승한 반면 압체 시간의 증가에 의한 치수고정효과는 미약하였다. 접촉각 측정결과 압체 온도와 시간의 증가와 함께 접촉각도 증가했으며 압체 온도 $220^{\circ}C$에서는 $90^{\circ}$ 이상의 접촉각을 나타내어 표면이 소수성을 나타냄을 알 수 있었다.

• 한국건축시공학회:학술대회논문집
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• 한국건축시공학회 2005년도 춘계 학술기술논문발표대회 논문집
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• pp.77-80
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• 2005

The surface of concrete tiles is weak in moisture that it occurrenced efflorescence, but in the former study we found that it is possible to ensure moisture stability of concrete surface by autoclaving. So this study is to discuss the moisture stability and Physical Properties of high-strength glossy concrete according to time and temperature of autoclave curing. As the results, by increasing time and temperature of autoclave curing, compressive strength and surface hardness increased and glossiness decreased. In the case to 3 hour and $180^{\circ}C$ of autoclave curing, there is not effloescences in mosture stability test.

• 한국전기전자재료학회:학술대회논문집
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• 한국전기전자재료학회 1998년도 추계학술대회 논문집
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• pp.215-218
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• 1998

The thermal stability of polyaniline-camphorsulfonic acid(PANI-CSA) film was studied as a function of temperature and time. A decrease in electrical conductivity of PANI-CSA film occurred when PANI-CSA film is subjected to temperature above 60$^{\circ}C$. From the result of thermogravimetry (TG), it was thought that the deterioration in electrical conductivity of PANI-CSA film was due to evaporation of water and residual solvent.

• Composites Research
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• 제28권6호
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• pp.395-401
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• 2015

본 연구에서는 자가손상보수에 적용되는 Grubbs' catalyst의 열안정성과 자가치료제와의 반응성을 조사하였다. 이를 위해 제조사에서 공급된 4종류를 고려하였으며 제조사에서 공급받은 상태와 기계적으로 분쇄시킨 상태로 시험하였다. 자가치료제는 Dicyclopentadiene (DCPD)과 5-ethylidene-2-norbonene (ENB)을 적절한 비율로 혼합한 4종류를 고려하였다. 촉매의 열안정성을 조사하기 위해 시차주사 열량측정장치를 통해 온도에 따른 열흐름 변화를 측정하였다. 자가치료제와의 반응성을 평가하기 위해 촉매와 혼합된 자가치료제의 반응열을 측정하였다. 이때 촉매는 자가치료제와 반응할 때의 최대온도와 최대온도 도달시간을 고려하여 Fluka Chemika Grubbs' catalyst를 적용하였다. 연구결과에 따르면 촉매는 제조사에 따라 다른 형상을 나타내며 입자의 크기가 작은 촉매가 자가치료제와 높은 반응성을 나타내었다. ENB의 혼합비가 높은 자가치료제가 촉매와 혼합되면 최대온도는 증가하고 최대온도 도달시간은 빨라졌다. 또한 촉매의 양이 많을수록 최대온도는 높아지고 최대온도 도달시간은 빨라졌다. 촉매의 열안정성과 자가치료제와의 반응성을 고려할 때 0.5 wt% 촉매와 D3E1 자가치료제가 자가손상보수를 위한 최적 조건임을 알 수 있었다. 마지막으로 노출된 분위기 온도에 따라 촉매에 열분해가 발생할 수 있기 때문에 촉매가 열안정성을 갖는 온도보다 높은 온도에 노출되지 않도록 하여야 한다.

• 한국염색가공학회지
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• 제30권4호
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• pp.264-274
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• 2018

Immobilization of lysozyme on chitosan non-woven using glutaraldehyde(GA) was investigated. For this, 100 % chitosan non-woven was prepared as novel support for the enzyme immobilization. In addition, free lysozyme activity was examined depending on various pH and temperature by measuring time. Moreover, the optimum immobilization conditions depending on various pH, temperature, immobilization time and lysozyme concentration was evaluated. In addition, thermal stability and storage stability of immobilized lysozyme were measured. The characteristics of immobilized lysozyme was examined by FT-IR, surface morphology, and MTT assay. The results are follows: the optimal immobilization of lysozyme were pH 7.0, $25^{\circ}C$, lysozyme concentration 1.5 mg/ml, immobilization time 240 min. The immobilized lysozyme showed higher thermal stability than the free trypsin. The immobilized lysozyme activity was retained 80 % of its initial activity at $4^{\circ}C$ over 30 days of storage. The lysozyme was immobilized effectively on chitosan non-woven by observation of surface morphology.

• Journal of Pharmaceutical Investigation
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• 제33권4호
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• pp.293-298
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• 2003

This study was attempted to develop the physicochemical ad morphological stability test methods for the cream and lotion formulations among the cosmetic foundations and to provide the guidance for the stability methods with respect to basic emulsions and creams. With these developed stability test methods, we can evaluate the expired date or life time of the available basic cosmetics, especially basic lotions ad creams. Also, the stability test methods established in this study can be used as a guideline to test physical and morphological stability of cosmetics in the future. Thus, we selected two types of basic cosmetics such as lotions and creams made by four different cosmetic companies ad applied them to the stability test methods depending on the temperature changes such as temperature cycling and freezing-thawing cycling test. After the temperature changes, the conductivity, turbidity, particle size, creaming ratio and pH changes of the creams and lotions were evaluated and morphological changes such as crystal formation, odor, color and feeling of the creams and lotions were also tested. As the results of the stability tests, all the tested creams and lotions except for one lotion were stable. Therefore, it may be concluded that these short-term accelerated stability tests as physical stability test depending on the temperature change study were suitable for the stability testing methods for the basic cosmetics and may be useful for the establishment of the guideline for the stability test of cosmetics.

• 한국산학기술학회논문지
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• 제10권11호
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• pp.3494-3499
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• 2009

소화성 궤양의 치료에 일반적으로 병용되어 사용되는 소염진통제인 록소프로펜 또는 알칼리화제인 탄산수소나트륨을 함유한 수용액 중에서 소화성 궤양의 치료에 사용되는 오메프라졸의 안정성에 대한 영향이 실온상태에서 실험하였다. 록소프로펜과 탄산수소나트륨 각각 60 mg을 오메프라졸(600 ${\mu}g$/ml) 용액에 혼합한 후 그 용액을 실온 상태로 80시간 보존하면서 그 분해정도를 원래의 오메프라졸의 농도와 비교하여 각각의 소실 농도를 산출하였다. 오메프라졸의 농도와 크로마토그램의 면적비는 5 - 160 ${\mu}g$/ml 농도에서 상호 직선성을 나타내었고 상대 표준 편차는 3.05 %이하로서 분석이 제대로 이루어졌음을 확인할 수 있었으며 함유 약물과 시간에 따른 오메프라졸의 분해 양상은 가상의 일차 직선 속도식을 나타내는 것을 알 수 있었다. 결론적으로 오메프라졸은 탄산수소나트륨 또는 록소프로 펜과의 병용 투여에 의해 그 안정성이 영향을 받을 수 있다는 것을 확인할 수 있었다.

• 한국가구학회지
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• 제20권6호
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• pp.560-565
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• 2009

It is known that heat treatment decreases the hygroscopicity of wood. Thus heat-treated wood is good for outdoor construction due to its improved dimensional stability. This study is to investigate the hygroscopicity and discoloration of spruce and birch boards heat-treated above $190^{\circ}C$. The equilibrium moisture contents (EMCs) at all relative humidities decreased with the increase of heat treatment temperature and/or time for both spruce and birch. It was revealed that heat-treatment temperature affected more on the hygroscopicity thaan heat-treatment time. The average basic densities decreased for the spruce specimens, but increased for the birch specimens with an increase of the treatment time and/or temperature. The same heat treatment condition (190-8) made the birch specimens darker than the spruce specimens.

• 대한수학회보
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• 제61권1호
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• pp.93-115
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• 2024

In this paper, the Gauge-Uzawa methods for the Darcy-Brinkman equations driven by temperature and salt concentration (DBTC) are proposed. The first order backward difference formula is adopted to approximate the time derivative term, and the linear term is treated implicitly, the nonlinear terms are treated semi-implicit. In each time step, the coupling elliptic problems of velocity, temperature and salt concentration are solved, and then the pressure is solved. The unconditional stability and error estimations of the first order semi-discrete scheme are derived, at the same time, the unconditional stability of the first order fully discrete scheme is obtained. Some numerical experiments verify the theoretical prediction and show the effectiveness of the proposed methods.

• 대한한의학회지
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• 제30권2호
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• pp.127-132
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• 2009

Objectives: This study aimed to investigate the stability of a decoction using three herbal plants and their major components according to the storage conditions and periods. Materials and Methods: A three-herb mixture (1:1:1) of Glycyrrhiza uralensis Fischer, Artemisia capillaris Thunberg, and Poncirus trifoliata Rafinesqui was decocted and kept at room temperature ($25{\pm}2^{\circ}C$) or cold temperature ($4^{\circ}C$) for 0, 2, 4 or 8 weeks in liquid form in a plastic pack under dark conditions. At time points given, they were lyophilized. 200 mg of powdered samples were dissolved in 1 mL of 90% methanol and then applied to a high performance thin layer chromatography (HPTLC) with glycyrrhizin, 6,7-dimethoxycoumarin or poncirin for quantitative or qualitative analysis. Results: There were no gross changes in HPTLC-based compositional band-patterns of the three herbal mixture according to the storage conditions and period. The major components of each herb, glycyrrhizin, 6,7-dimethoxycoumarin and poncirin, showed slight time-dependent reduction in their contents both at room and cold temperature for 8 weeks. Conclusion: We could conclude that the current herbal decoction is generally safe for the stability at both RT or CT for at least 8 weeks. Nevertheless, we proposed that further advanced studies are required for more multiple herbal mixtures and longer storage periods.