• Title/Summary/Keyword: Temperature hardening

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Hardening properties in MMA monomer using UP and EPS in addition hardener (경화제의 첨가에 따른 UP와 EPS 혼입 MMA 수지의 경화특성)

  • Lee, Jung-Hui;Song, Hun;Chu, Yong-Sik;Lee, Jong-Kyu
    • Proceedings of the Korea Concrete Institute Conference
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    • 2008.11a
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    • pp.445-448
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    • 2008
  • The unsaturated polyester(UP) and epoxy resin have a superior material properties and a chemical resistance using sewerage pipes rehabilitation. However, UP and epoxy have not a low temperatures harding, the requirement $8{\sim}11$ hours long times harding and heating system used by reinforcement liner. This study is to evaluate the effects of low temperature harding properties methyl methacrylate(MMA) monomer using expanded polystyrene(EPS) and UP in addition of initiator and promoters. From the test result, viscosity tends to increase with increasing EPS and UP contents. However, harding time change of the MMA resins which it follows in addition of the initiator and promoter.

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Work Softening Behavior of Zn-15%Al alloy (Zn-15%Al 합금의 가공연화 거동)

  • Jun, Joong-Hwan;Seong, Ki-Duk;Kim, Jeong-Min;Kim, Ki-Tae;Jung, Woon-Jae
    • Journal of the Korean Society for Heat Treatment
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    • v.18 no.1
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    • pp.18-23
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    • 2005
  • Effect of cold rolling on microstructural changes has been investigated for a Zn-15%Al alloy to elucidate the reason for its work softening behavior. Fully annealed microstructure of the Zn-15%Al alloy is characterized by ${\eta}$ grains and (${\eta}+{\alpha}$) lamellar colonies, where ${\eta}$ and ${\alpha}$ are Zn-rich HCP and Al-rich FCC phases, respectively. The hardness decreases continuously with increasing cold rolling degree, exhibiting work softening behavior. It is revealed that during the cold rolling, (${\eta}+{\alpha}$) lamellar colonies gradually change into equiaxed ${\eta}$ and ${\alpha}$ grains due to dynamic recrystallization at room temperature, while pre-existing ${\eta}$ grains are only deformed without recrystallization. Furthermore, cold rolling causes the precipitation of dissolved Al solutes in ${\eta}$ grains. In view of these results, change of (${\eta}+{\alpha}$) phases from lamellar to equiaxed morphology, which results in structural softness and increase in equiaxed ${\eta}/{\alpha}$ grain boundaries with higher mobility, and deterioration of solution hardening by precipitation of Al solutes from ${\eta}$ grains, are thought to contribute to the work softening of Zn-15%Al alloy.

Modeling the Present Probability of Urban Woody Plants in the face of Climate Change (기후변화에 따른 도시 수종의 기후 적합성 평가모델 - 서울시를 대상으로 -)

  • Kim, Yoon-Jung;Lee, Dong-Kun;Park, Chan
    • Journal of the Korean Society of Environmental Restoration Technology
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    • v.16 no.1
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    • pp.159-170
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    • 2013
  • The effect of climate change on urban woody plants remains difficult to predict in urban areas. Depending on its tolerances, a plant species may stay and survive or stay with slowly declining remnant populations under a changing climate. To predict those vulnerabilities on urban woody plants, this study suggests a basic bioclimatic envelop model of heat requirements, cold tolerance, chilling requirements and moisture requirements that are well documented as the 'climatic niche'. Each component of the 'climatic niche' is measured by the warmth index, the absolute minimum temperature, the number of chilling weeks and the water balance. Regarding the utility of the developed model, the selected urban plant's present probabilities are suggested in the future climate of Seoul. Both Korea and Japan's thermal thresholds are considered for a plant's optimal climatic niche. By considering the thermal thresholds of these two regions for the same species, the different responses observed will reflect the plant's 'hardening' process in a rising climate. The model illustrated that the subpolar plants Taxus cuspidata and Ulmus davidiana var. japonica are predicted to have low suitability in Seoul. The temperate plants Zelkova serrata and Pinus densiflora, which have a broad climatic niche, exhibited the highest present probability in the future. The subtropical plants Camellia japonica and Castanopsis cuspidata var. sieboldii may exhibit a modest growth pattern in the late 21C's future climatic period when an appropriate frost management scheme is offered. The model can be used to hypothesize how urban ecosystems could change over time. Moreover, the developed model can be used to establish selection guidelines for urban plants with high levels of climatic adaptability.

Determining the Proportions of Bone and Cartilage Growth in the Crucian Carp (carassius auratus) Using the Modified Simultaneous Differential Staining Technique

  • Lee, Jin-Heon
    • Journal of Environmental Health Sciences
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    • v.36 no.4
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    • pp.337-341
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    • 2010
  • The modified simultaneous differential staining technique, which enables double staining of cartilage and bones, needs to be improved to prevent soft tissues from being damaged during the staining process. Key factors influencing the extent to which soft tissues are damaged include the fixative used, macerating time, potassium hydroxide concentration, incubation temperature and the removal of skin from specimens. Here we describe a protocol that enables the hardening of tissues during bleaching and maceration. We also describe a method for objectively measuring rates of cartilage and bone growth. The use of formalin as a fixative rendered soft tissues more rigid due to the resulting chemical bonds formed between proteins. Blotted specimens were immersed in 1% potassium hydroxide (KOH) and incubated at $37^{\circ}C$ for 1 day (smaller specimens) or 2-3 days (larger specimens). The 1% KOH solution was also used as the diluent solution for the subsequent immersion in a graded series of 30%, 50%, 70%, 90%, 100% glycerol solutions, a procedure that made soft tissues even more transparent and hardened. It was not necessary to remove the skin of specimens shorter than 2 cm, since the macerating solution could easily penetrate their thin skin layer and continuously remove those pigments hindering visibility. Since excessive osmosis is another factor that can damage soft tissues in the macerating process by causing the rupture of those cells not able to withstand the osmotic pressure, here it was minimized by balancing the salt concentration between the interior and exterior of cells with the addition of 0.9% sodium chloride (NaCl) in the macerating solution. Finally, to determine the proportions of cartilage and bone growth, photographs of the stained specimens were taken with a dissecting microscope and sections corresponding to the cartilage and bones were cut out from the printed pictures and weighed. Our results show that this method is suitable for the objective evaluation of bone and cartilage growth.

Nonlinear forced vibration of FG-CNTs-reinforced curved microbeam based on strain gradient theory considering out-of-plane motion

  • Allahkarami, Farshid;Nikkhah-bahrami, Mansour;Saryazdi, Maryam Ghassabzadeh
    • Steel and Composite Structures
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    • v.26 no.6
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    • pp.673-691
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    • 2018
  • The main goal of this research is to examine the in-plane and out-of-plane forced vibration of a curved nanocomposite microbeam. The in-plane and out-of-plane displacements of the structure are considered based on the first order shear deformation theory (FSDT). The curved microbeam is reinforced by functionally graded carbon nanotubes (FG-CNTs) and thus the extended rule of mixture is employed to estimate the effective material properties of the structure. Also, the small scale effect is captured using the strain gradient theory. The structure is rested on a nonlinear orthotropic viscoelastic foundation and is subjected to concentrated transverse harmonic external force, thermal and magnetic loads. The derivation of the governing equations is performed using energy method and Hamilton's principle. Differential quadrature (DQ) method along with integral quadrature (IQ) and Newmark methods are employed to solve the problem. The effect of various parameters such as volume fraction and distribution type of CNTs, boundary conditions, elastic foundation, temperature changes, material length scale parameters, magnetic field, central angle and width to thickness ratio are studied on the frequency and force responses of the structure. The results indicate that the highest frequency and lowest vibration amplitude belongs to FGX distribution type while the inverse condition is observed for FGO distribution type. In addition, the hardening-type response of the structure with FGX distribution type is more intense with respect to the other distribution types.

Grain Refinement and Mechanical Properties of AM60 Mg Alloy by $CaCN_2$ Addition (Ca$CN_2$ 첨가에 의한 AM60 마그네슘 합금의 결정립 미세화 및 기계적 성질)

  • Eom, Jeong-Pil;Jeong, Seong-Kyu;Lim, Su-Geun;Shin, Hee-Taek;Jeong, Deuk-Soo
    • Journal of Korea Foundry Society
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    • v.18 no.4
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    • pp.383-388
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    • 1998
  • Effects of $CaCN_2$ addition on the grain refinement in the AM60 magnesium ingots were investigated. The effects of the $CaCN_2$ are estimated with different inoculation temperatures, inoculation contents, and holding time to find out the optimum condition. AM60 alloy was melted in the low carbon steel crucible by cylindrical electric furnace under an argon atmosphere. The melting and casting apparatus is specially designed for magnesium alloys. The grain size of AM60 magnesium alloy decreased significantly with an increase in $CaCN_2$ content and, at 0.8 wt% $CaCN_2$ or more, grain size becomes constant at about $85 {\mu}m$. The optimum condition was obtained in the 0.8 wt% $CaCN_2$ for holding molten metal of 30 min. at the temperature of $710^{\circ}C$. The tensile properties of AM60 magnesium alloys were improved due to grain refinement by addition of $CaCN_2$. In the optimum condition, the yield strength, tensile strength and elongation were ${\sigma}_{0.2}=107 MPa$, ${\sigma}_{T.S}=234 MPa$ and e=14.2%. The variation of stress with strain obeyed the relationship of the ${\sigma}=K{\varepsilon}^n$. The strain-hardening exponent, n and strength coefficient, K obtained in the 0.8 wt% $CaCN_2$ added AM 60 magnesium alloy were n=0.21 and K=390 MPa.

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THE EFFECTS OF HEAT TREATMENT ON MECHANICAL PROPERTIES AND METAL RELEASE FROM HEAT-TREATED ORTHODONTIC ARCHWIRES (열처리한 교정용 호선의 기계적 성질과 금속유리에 대한 연구)

  • Choi, Chul Min;Rhee, Byung Tae
    • The korean journal of orthodontics
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    • v.20 no.2
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    • pp.381-390
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    • 1990
  • The purpose of this study was to evaluate the effects of heat treatment on mechanical properties in $0.016^{{\prime}{\prime}}{\times}0.022^{{\prime}{\prime}}$ blue Elgiloy wires and to measure the amounts of nickel and chromium released from the wires in artificial saliva. Ultimate tensile strength, yield strength and elongation were measured with universal testing machine (Instron). and the amounts of nickel and chromium released from the sample were measured with atomic absorption spectrophotometer after one week immersion in the artificial saliva. Ultimate tensile strength and yield strength were progressively increased below $1000^{\circ}F$, but elongation was decreased. And the results were reversed above $1100^{\circ}F$. After heat treatment of the sample for 9 minutes at $1000^{\circ}F$, the maximum tensile strength and yield strength were $213.6kg/mm^2$, $140.1kg/mm^2$, respectively. Both tensile strength and yield strength were decreased progressively above $1100^{\circ}F$. Elongation was appeared the minimum value (8.6%) after heat treatment for 9 minutes and 12 minutes at $1000^{\circ}F$. There was a pronounced increase in nickel and chromium liberation with increasing time and temperature. The maximum amounts of nickel and chromium released form the sample were $4.947{\mu}m/cm^2$, $3.088{\mu}g/cm^2$, respectively after heat treatment for 12 minutes at $1300^{\circ}F$. Heat treatment is applied to orthodontic wires, especially cobalt-chromium alloys, for the purpose of stress-relievning and hardening. When the heat-treatment of orthodontic wires, the heating procedure should be well controlled in order to have no effect on corrosion resistance and mechanical properties.

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Effect of Strain Aging on the Tensile Properties of an API X70 Linepipe Steel (API X70 라인파이프강의 인장 특성에 미치는 변형 시효의 영향)

  • Lee, Seung-Wan;Lee, Sang-In;Hwang, Byoungchul
    • Korean Journal of Materials Research
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    • v.27 no.10
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    • pp.524-529
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    • 2017
  • The effect of strain aging on the tensile properties of API X70 linepipe steel was investigated in this study. The API X70 linepipe steel was fabricated by controlled rolling and accelerated cooling processes, and the microstructure was analyzed using optical and scanning electron microscopes and electron backscatter diffraction. Strain aging tests consisting of 1 % pre-strain and thermal aging at $200^{\circ}C$ and $250^{\circ}C$ were conducted to simulate U-forming, O-forming, Expansion(UOE) pipe forming and anti-corrosion coating processes. The API X70 linepipe steel was composed of polygonal ferrite, acicular ferrite, granular bainite, and bainitic ferrite whose volume fraction was dependent on the chemical composition and process conditions. As the thermal aging temperature increased, the steel specimens showed more clearly discontinuous type yielding behavior in the tensile stress-strain curve due to the formation of a Cottrell atmosphere. After pre-strain and thermal aging, the yield and tensile strengths increased and the yield-to-tensile strength ratio decreased because yielding and aging behaviors significantly affected work hardening. On the other hand, uniform and total elongations decreased after pre-strain and thermal aging since dislocation gliding was restricted by increased dislocation density after a 1 % pre-strain.

Differences in Cold Rolling Workability and Mechanical Properties between Al-Mg-Si and Al-Mg-Zn System Alloys with Cold Rolling (냉간압연가공에 따른 Al-5.5Mg-2.9Si계와 Al-7Mg-0.9Zn계 합금의 압연가공성 및 기계적 특성 차이)

  • Yang, Ji-Hun;Lee, Seong-Hee
    • Korean Journal of Materials Research
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    • v.26 no.11
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    • pp.628-634
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    • 2016
  • The cold rolling workability and mechanical properties of two new alloys, designed and cast Al-5.5Mg-2.9Si and Al-7Mg-0.9Zn alloys, were investigated in detail. The two alloy sheets of 4 mm thickness, 30 mm width and 100 mm length were reduced to a thickness of 1 mm by multi-pass rolling at ambient temperature. The rolling workability was better for the Al-7Mg-0.9Zn alloy than for the Al-5.5Mg-2.9Si alloy; in case of the former alloy, edge cracks began to occur at 50% rolling reduction, and their number and length increased with rolling reduction; however, in the latter alloy, the sheets did not have any cracks even at higher rolling reduction. The mechanical properties of tensile strength and elongation were also better in the Al-7Mg-0.9Zn alloy than in Al-5.5Mg-2.9Si alloy. Work hardening ability after cold rolling was also higher in the Al-7Mg-0.9Zn alloy than in the Al-5.5Mg-2.9Si alloy. At the same time, the texture development was very similar for both alloys; typical rolling texture developed in both alloys. These differences in the two alloys can primarily be explained by the existence of precipitates of $Mg_2Si$. It is concluded that the Al-7Mg-0.9Zn alloy is better than the Al-5.5Mg-2.9Si alloy in terms of mechanical properties.

Study on the Disbonding of Stainless Steel Overlay Welded Metal(Report 2) - A Metallurgical Study on PWHT of Overlaid Austenitic Stainless Steel Weld Metals - (스테인레스강 Overlay 용접부의 Disbonding 에 관한 연구(2) - 오스테나이트계 스테인레스강 오버레이 용접금속의 PWHT에 관한 야금학적 고찰 -)

  • 이영호;윤의박
    • Journal of Welding and Joining
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    • v.2 no.1
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    • pp.4-17
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    • 1984
  • Overlaid weld metals of austenitic stainless steel in a pressure vessel of power reactor are usually post-weld heated for a long period of time after welding. The PWHT is considered as a kind of sensitizing and it is important to check the soundness of the weld metal after PWHT, especially about the precipitation of carbides. The purpose of this report is to obtain information on the relation between the change of microstructure and Post-Weld Heat Treatment in the overlaid weld metals. Metallurgical aspects of the problem on austenitic stainless steel heated at $625^{\circ}C$, $670^{\circ}C$, $720^{\circ}C$ and $760^{\circ}C$ for 3, 10, 30, 100 and 300 hours have been investigated by means of optical-micrography, micro-hardness measurement, scanning electron microscope and electron-probe micro analysis. From the results obtained, the following conclusions are drawn; 1) The PWHT above $625^{\circ}C$ for a long time causes a diffusion of carbon atoms from low alloy steel into stainless steel, and consequently carbon is highly concentrated at the boundary layer of stainless steel. 2) C in ferritic steel migrated to austenitic steel and carbides precipitated in austenitic steel along fusion line. At higher temperatures, the ferrite grains coarsened in the decarburized zone. 3) In the change of microstructure of stainless steel overlaid weld metal, the width of carbides precipitated zone and decarburized zone increased with increase of PWHT temperature and time. 4) At about $625^{\circ}C$ to $760^{\circ}C$, chromium carbides, mainly $M_{23} C_6$, precipitate very closely in the carburized layer with remarkable hardening. 5) Precipitation of delta ferrite from molten weld metal depends on solidification phenomenon. There was a small of ferrite near the bond in which the local solidification time was short, comparing with after parts of weld metal. Shape and amount of ferrite were not changed by Post-Weld Heat Treatment after solidification.

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